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1. 发明授权

US11267930B2 Antimicrobial thermoplastic polyuethanes 有权
公开(公告)号：US11267930B2
公开(公告)日：2022-03-08
申请号：US16481268
申请日：2018-01-30
申请人： Lubrizol Advanced Materials, Inc.
发明人： Hua Zhang , Roger W. Day , Richard Woofter , Umit G. Makal , Kiara L. Smith
IPC分类号： C08G18/76 , C08G18/32 , C08K5/31 , C09D5/16 , C09D175/04
摘要： The disclosed technology provides thermoplastic polyurethane compositions having non-leaching antimicrobial properties while still maintaining good physical properties, methods of making the same, and articles, including medical devices, made from such compositions. The disclosed technology includes a process of making an antimicrobial polymer composition, where the process includes mixing an antimicrobial additive into a polymeric material; wherein said polymeric material comprises a polymeric backbone made up of urethane linkages derived from a polyisocyanate and a polyol; and wherein said mixing occurs under conditions that result in the breaking of a minority of said urethane bonds resulting in reactive isocyanate groups; and wherein two or more of said reactive isocyanate groups react with said antimicrobial additive to covalently bond said antimicrobial additive into the polymeric backbone of said polymeric material; resulting in an antimicrobial polymer composition.

2. 发明授权

US10184023B2 Thermoplastic Polyurethane with high heat resistance 有权
公开(公告)号：US10184023B2
公开(公告)日：2019-01-22
申请号：US15329767
申请日：2015-08-11
申请人： Lubrizol Advanced Materials, Inc.
发明人： Umit G. Makal
IPC分类号： C08G18/76 , C08G18/32 , C08G18/44 , C08G18/48 , C09J175/08
摘要： The present invention relates to novel thermoplastic polyurethane (TPU) compositions that contain alkylene substituted spirocyclic compounds as chain extender and polycarbonate polyol. The present invention provides for TPUs which exhibit high temperature resistance.

3. 发明授权

US09650477B2 Crosslinkable thermoplastic polyurethane 有权
公开(公告)号：US09650477B2
公开(公告)日：2017-05-16
申请号：US14519275
申请日：2014-10-21
申请人： Lubrizol Advanced Materials, Inc.
发明人： Umit G. Makal , George H. Loeber , Louis J. Brandewiede
IPC分类号： C08J5/00 , C08G18/68 , C08G18/67 , C08G18/66 , B29C71/04 , H01B3/30 , H01B7/295 , H01B13/14 , B29K75/00 , B29K105/24
CPC分类号： C08J5/00 , B29C71/04 , B29K2075/00 , B29K2105/24 , B29K2995/0016 , C08G18/6607 , C08G18/676 , C08G18/68 , C08J2375/08 , H01B3/302 , H01B7/295 , H01B13/148
摘要： The TPU of this invention contains unsaturation in its polymeric backbone. The unsaturation can be present in the soft segment or in the hard segment or in both the soft and hard segments of the TPU. The TPU can be molded like a thermoplastic, and can be subsequently crosslinked by exposure to electron beam irradiation into thermoset articles having excellent chemical resistance, dimensional stability, set properties, heat resistance, oxidative resistance, and creep resistance. In one embodiment, the TPUs of this invention are the reaction product (1) a hydroxyl terminated intermediate, (2) a polyisocyanate, (3) a saturated glycol chain extender, and (4) a glycol chain extender containing carbon-carbon double bonds, such as the allyl moieties present in trimethylolpropane monoallyl ether. In another embodiment of this invention, the thermoplastic polyurethane which is crosslinkable by e-beam irradiation is comprised of the reaction product of (1) a saturated hydroxyl terminated intermediate, (2) an unsaturated hydroxyl terminated intermediate, wherein the unsaturated hydroxyl terminated intermediate contains carbon-carbon double bonds, (3) a polyisocyanate, and (4) a saturated glycol chain extender.

4. 发明申请

US20150148514A1 METHOD FOR IDENTIFYING BIOABSORBABLE POLYMERS 审中-公开
标题翻译：识别生物可溶性聚合物的方法
公开(公告)号：US20150148514A1
公开(公告)日：2015-05-28
申请号：US14407660
申请日：2013-06-24
申请人： Lubrizol Advanced Materials, Inc.
发明人： Umit G. Makal , Roger W. Day
IPC分类号： G06F19/00 , C08G18/32 , C08G18/72
CPC分类号： G16C20/30 , C08G18/08 , C08G18/3203 , C08G18/4277 , C08G18/664 , C08G18/72 , C08G2230/00 , F04C2270/041 , G16C20/40
摘要： A system and method for producing a bioabsorbable thermoplastic polyurethane tailored to a medical application are provided. The method includes identifying suitable thermoplastic polyurethane properties based on the medical application. The thermoplastic polyurethane comprises units derived from a diol chain extender, a diisocyanate, and a polyol. The thermoplastic polyurethane properties include a biodegradation rate and at least one physical property. The method includes identifying a base thermoplastic polyurethane and altering at least one parameter of the base thermoplastic polyurethane which relates to the desired thermoplastic polyurethane properties to generate a candidate thermoplastic polyurethane. The altering may be performed iteratively until the suitable range of thermoplastic polyurethane properties based on the medical application is met.
摘要翻译：提供了一种用于制造适于医疗应用的生物可吸收热塑性聚氨酯的系统和方法。该方法包括基于医疗应用鉴定合适的热塑性聚氨酯性质。热塑性聚氨酯包含衍生自二醇增链剂，二异氰酸酯和多元醇的单元。热塑性聚氨酯性质包括生物降解速率和至少一种物理性质。该方法包括鉴定基础热塑性聚氨酯并改变与所需热塑性聚氨酯性质相关的基础热塑性聚氨酯的至少一个参数以产生候选的热塑性聚氨酯。可以迭代地进行改变，直到满足基于医疗应用的热塑性聚氨酯特性的合适范围。

5. 发明申请

US20210163672A1 Melt Processable Thermoplastic Polyurethane-Urea Elastomers 有权
公开(公告)号：US20210163672A1
公开(公告)日：2021-06-03
申请号：US17172144
申请日：2021-02-10
申请人： Lubrizol Advanced Materials, Inc.
发明人： Umit G. Makal , George H. Loeber , Lalith B. Suragani Venu
IPC分类号： C08G18/76 , C08G18/44 , C08G18/66 , C08G18/08 , B29B9/06 , C08G18/32 , C08G18/42 , C08G18/48 , C08J3/12
摘要： The present invention relates to a melt processable thermoplastic polyurethane-urea composition formed by a continuous bulk process without the presence of solvent using a polyol component, an isocyanate component, and chain extender component comprising a hindered aromatic diamine.

6. 发明申请

US20200332117A1 Thermoplastic Polyurethane Composition 审中-公开
公开(公告)号：US20200332117A1
公开(公告)日：2020-10-22
申请号：US16919143
申请日：2020-07-02
申请人： Lubrizol Advanced Materials, Inc.
发明人： Romina Marin Bernabe , Umit G. Makal , Qwei Lu
IPC分类号： C08L75/04 , C08G18/66 , C08G18/75 , C08G18/32 , C08G18/42
摘要： The present invention relates to novel thermoplastic polyurethane (TPU) compositions that contain alkylene substituted spirocyclic compounds as chain extender, aliphatic polyisocyanate, and polyester polyol. The present invention provides for TPUs which exhibit high temperature and chemical resistance.

7. 发明申请

US20190270840A1 THERMOPLASTIC POLYURETHANES WITH REDUCED TACKINESS 审中-公开
公开(公告)号：US20190270840A1
公开(公告)日：2019-09-05
申请号：US16308497
申请日：2017-06-15
申请人： LUBRIZOL ADVANCED MATERIALS, INC.
发明人： Umit G. Makal , Romina Marin Bernabe , Chetan M. Makadia
IPC分类号： C08G18/66 , C08G18/73 , C08G18/42 , C08G18/32 , C08G18/28
摘要： The present invention relates to novel thermoplastic polyurethane (TPU) compositions that have crystalline chain ends. The TPU compositions of the invention can provide improved resiliency, lower surface free energy, and/or reduced stickiness, while maintaining other desirable physical properties. The TPU compositions of the present invention are made from the reaction product of an aliphatic polyisocyanate, a polycaprolactone polyester polyol, an optional chain extender component, and a chain terminator component, which comprises a short chain crystalline compound containing a single functional group capable of terminating the chain of the thermoplastic polyurethane.

8. 发明申请

US20150141567A1 ALLOY COMPRISING POLYOLEFIN AND THERMOPLASTIC POLYURETHANE 有权
标题翻译：合金包含聚烯烃和热塑性聚氨酯
公开(公告)号：US20150141567A1
公开(公告)日：2015-05-21
申请号：US14402511
申请日：2013-05-17
申请人： Lubrizol Advanced Materials, Inc. , Coloplast A/S
发明人： Carsten Hoej , Niels Joergen Madsen , Umit G. Makal
IPC分类号： C08L75/04 , C08L23/12 , C08L23/06
CPC分类号： C08L75/04 , C08G18/10 , C08G18/48 , C08G18/4854 , C08G18/76 , C08L23/06 , C08L23/12 , C08L75/08 , C08L23/08 , C08G18/3206
摘要： This invention relates to an alloy comprising polyurethane and polyolefin. It has now surprisingly been found that a specific composition of polyolefin and polyurethane has surprising mechanical properties and at the same time has transparent characteristics and/or appearance. The present invention provides an alloy with remarkable mechanical properties. The phases do not macro-phase separate. Thus, this stable and potentially broad interface is very effective in stress transfer when the alloy is strained. As one might expect, the hardness values for the alloys are in between the hardness values of each component but the other physical properties are no adjusted. In this way, when considering the hardness and mechanical values, these alloys behave like two compatible polymers.
摘要翻译：本发明涉及包含聚氨酯和聚烯烃的合金。现在令人惊奇地发现，聚烯烃和聚氨酯的特定组合物具有惊人的机械性能，同时具有透明特性和/或外观。本发明提供具有显着机械性能的合金。这些阶段不是宏相分离的。因此，当合金应变时，这种稳定和潜在的宽界面在应力传递中非常有效。可以预期的是，合金的硬度值在每个组分的硬度值之间，但其他物理性能没有调整。以这种方式，当考虑硬度和机械值时，这些合金表现得像两种相容的聚合物。

9. 发明申请

US20150034361A1 Crosslinkable Thermoplastic Polyurethane 审中-公开
标题翻译：可交联热塑性聚氨酯
公开(公告)号：US20150034361A1
公开(公告)日：2015-02-05
申请号：US14519275
申请日：2014-10-21
申请人： Lubrizol Advanced Materials, Inc.
发明人： Umit G. Makal , George H. Loeber , Louis J. Brandewiede
IPC分类号： C08J5/00 , B29C71/04 , H01B13/14 , H01B3/30 , H01B7/295
CPC分类号： C08J5/00 , B29C71/04 , B29K2075/00 , B29K2105/24 , B29K2995/0016 , C08G18/6607 , C08G18/676 , C08G18/68 , C08J2375/08 , H01B3/302 , H01B7/295 , H01B13/148
摘要： The TPU of this invention contains unsaturation in its polymeric backbone. The unsaturation can be present in the soft segment or in the hard segment or in both the soft and hard segments of the TPU. The TPU can be molded like a thermoplastic, and can be subsequently crosslinked by exposure to electron beam irradiation into thermoset articles having excellent chemical resistance, dimensional stability, set properties, heat resistance, oxidative resistance, and creep resistance. In one embodiment, the TPUs of this invention are the reaction product (1) a hydroxyl terminated intermediate, (2) a polyisocyanate, (3) a saturated glycol chain extender, and (4) a glycol chain extender containing carbon-carbon double bonds, such as the allyl moieties present in trimethylolpropane monoallyl ether. In another embodiment of this invention, the thermoplastic polyurethane which is crosslinkable by e-beam irradiation is comprised of the reaction product of (1) a saturated hydroxyl terminated intermediate, (2) an unsaturated hydroxyl terminated intermediate, wherein the unsaturated hydroxyl terminated intermediate contains carbon-carbon double bonds, (3) a polyisocyanate, and (4) a saturated glycol chain extender.
摘要翻译：本发明的TPU在其聚合物主链中含有不饱和键。该不饱和度可以存在于TPU的软段或硬链段或软段和硬区两者中。 TPU可以像热塑性塑料一样成型，并且随后可以通过电子束照射进入具有优异的耐化学性，尺寸稳定性，凝固性，耐热性，耐氧化性和抗蠕变性的热固性制品中而交联。在一个实施方案中，本发明的TPU是反应产物（1）羟基封端的中间体，（2）多异氰酸酯，（3）饱和的乙二醇增链剂，和（4）含有碳 - 碳双键的二醇链延长剂，例如存在于三羟甲基丙烷单烯丙基醚中的烯丙基部分。在本发明的另一个实施方案中，通过电子束照射可交联的热塑性聚氨酯由（1）饱和羟基封端的中间体，（2）不饱和羟基封端的中间体的反应产物组成，其中不饱和羟基封端的中间体包含碳 - 碳双键，（3）多异氰酸酯，和（4）饱和二醇增链剂。

10. 发明申请

US20220153917A1 Antimicrobial Thermoplastic Polyuethanes 有权
公开(公告)号：US20220153917A1
公开(公告)日：2022-05-19
申请号：US17588980
申请日：2022-01-31
申请人： Lubrizol Advanced Materials, Inc.
发明人： Hua Zhang , Roger W. Day , Richard Woofter , Umit G. Makal , Kiara L. Smith
IPC分类号： C08G18/76 , C08G18/32 , C08K5/31 , C09D5/16 , C09D175/04
摘要： The disclosed technology provides thermoplastic polyurethane compositions having non-leaching antimicrobial properties while still maintaining good physical properties, methods of making the same, and articles, including medical devices, made from such compositions. The disclosed technology includes a process of making an antimicrobial polymer composition, where the process includes mixing an antimicrobial additive into a polymeric material; wherein said polymeric material comprises a polymeric backbone made up of urethane linkages derived from a polyisocyanate and a polyol; and wherein said mixing occurs under conditions that result in the breaking of a minority of said urethane bonds resulting in reactive isocyanate groups; and wherein two or more of said reactive isocyanate groups react with said antimicrobial additive to covalently bond said antimicrobial additive into the polymeric backbone of said polymeric material; resulting in an antimicrobial polymer composition.

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