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1. 发明授权

US4472341A Polyurethane process using polysiloxane mold release agents 失效
标题翻译：聚氨酯工艺采用聚硅氧烷脱模剂
公开(公告)号：US4472341A
公开(公告)日：1984-09-18
申请号：US510791
申请日：1983-07-05
申请人： Louis M. Alberino , Dale F. Regelman , George H. Temme
发明人： Louis M. Alberino , Dale F. Regelman , George H. Temme
IPC分类号： C08G18/00 , B29C33/64 , C08G18/08 , C08L75/00 , C08L75/04 , B28B1/24 , C08G18/14
CPC分类号： C08G18/08 , B29C33/64 , C08L75/04 , Y10S264/83
摘要： Disclosed is an improved process for the production of organic polyisocyanate based molded polymers prepared from at least one organic polyisocyanate and at least one polyol in the presence of an internal release agent wherein the improvement comprises employing as said agent a polysiloxane having at least one unit of the formula ##STR1## wherein R is selected from the group consisting of lower-alkyl and aryl, R.sup.1 is a divalent hydrocarbon radical, and R.sup.2 is selected from the group consisting of lower-alkoxy, aryloxy, particular hydroxyalkyleneoxy, alkoxyalkyleneoxy, amino, and hydroxyalkylamino radicals.The molding process can be repeated in many cycles before the molds require cleaning or treatment with release agent. The ease and rapidity with which the present process can be carried out makes it particularly suited to RIM production methods.
摘要翻译：公开了一种改进的制备由至少一种有机多异氰酸酯和至少一种多元醇在内部脱模剂存在下制备的有机多异氰酸酯基模制聚合物的方法，其中改进包括使用作为所述试剂的聚硅氧烷，所述聚硅氧烷具有至少一个单元其中R选自低级烷基和芳基，R1是二价烃基，R2选自低级烷氧基，芳氧基，特别是羟基亚烷基氧基，烷氧基亚烷基氧基，氨基和羟烷基氨基。在模具需要清洁或用脱模剂处理之前，可以在许多周期内重复模制过程。可以轻松快捷地实现本流程，使其特别适合RIM生产方式。

2. 发明授权

US4216322A Process for making triethylene diamines 失效
标题翻译：制备三亚乙基二胺的方法
公开(公告)号：US4216322A
公开(公告)日：1980-08-05
申请号：US956109
申请日：1978-10-30
申请人： George H. Temme
发明人： George H. Temme
IPC分类号： C07D487/08 , C08G18/20
CPC分类号： C07D487/08 , C07C255/00 , C08G18/2063
摘要： There is disclosed a novel process for the preparation of 1,4-diazabicyclooctane dihydrohalides having the formula ##STR1## wherein each R is independently selected from the group consisting of hydrogen, lower alkyl, aryl, aralkyl, and cycloalkyl, and X is chlorine or bromine, said process comprising heating at a temperature of at least about 100.degree. C. and in a dipolar aprotic solvent certain novel dihaloalkylene diamines. Neutralization of the dihydrohalides provides the corresponding 1,4-diazabicyclooctane free bases.Also disclosed are certain novel 1,4-diazabicyclooctane diammonium dihalides formed as intermediates in the above process and a process for their conversion to the 1,4-diazabicyclooctane dihydrohalides and free bases thereof.The 1,4-diazabicyclo compounds produced in accordance with the invention find particular utility as catalysts in the preparation of polyurethanes from organic polyols and polyisocyanates.
摘要翻译：公开了一种制备具有式“IMAGE”的1,4-二氮杂双环辛烷二氢卤化物的新方法，其中每个R独立地选自氢，低级烷基，芳基，芳烷基和环烷基，X是氯或溴，所述方法包括在至少约100℃的温度和在偶极非质子溶剂中加热某些新的二卤代亚烷基二胺。二氢卤化物的中和提供相应的1,4-二氮杂双环辛烷游离碱。还公开了在上述方法中形成作为中间体的某些新的1,4-二氮杂双环辛烷二卤化二铵及其转化为1,4-二氮杂双环辛烷二氢卤化物及其游离碱的方法。根据本发明制备的1,4-二氮杂双环化合物在从有机多元醇和多异氰酸酯制备聚氨酯中特别有用。

3. 发明授权

US4226958A Process for preparing organo-arsenic derivatives of polystyrene and related polymers 失效
标题翻译：制备聚苯乙烯和相关聚合物的有机砷衍生物的方法
公开(公告)号：US4226958A
公开(公告)日：1980-10-07
申请号：US69764
申请日：1979-08-27
申请人： Curtis P. Smith , George H. Temme
发明人： Curtis P. Smith , George H. Temme
IPC分类号： C08F8/00 , C07C67/00 , C07C241/00 , C07C267/00 , C08F8/42 , C08F8/22 , C08F8/24
CPC分类号： C08F8/42
摘要： A process is described for the preparation of a polymer having a recurring unit of the formula: ##STR1## where R is hydrogen or methyl, C.sub.n H.sub.2n is lower-alkylene, R.sub.1 and R.sub.2 are aryl or lower-alkyl, and x is 0 or 1. A polymer having a recurring unit of the formula: ##STR2## where X is chloro, bromo, iodo, chloroalkyl, bromoalkyl or iodoalkyl, is reacted with the appropriate aryl or alkyl chloride or bromide and arsenic trichloride, arsenic tribromide or arsenic trioxide in the presence of sodium, magnesium, or lithium metal. The resulting polymer is an intermediate in the preparation, by oxidation, of the corresponding As-oxide which polymer is useful as a catalyst for the conversion of isocyanates to the corresponding carbodiimides.
摘要翻译：描述了制备具有下式的重复单元的聚合物的方法：其中R是氢或甲基，C n H 2n是低级亚烷基，R 1和R 2是芳基或低级烷基，x是0或1 将具有下式的重复单元的聚合物：其中X是氯，溴，碘，氯烷基，溴烷基或碘代烷基，与合适的芳基或烷基氯化物或溴化物，三氯化砷，三溴化砷或三氧化二砷反应存在钠，镁或锂金属。所得聚合物是通过氧化制备相应的As-氧化物的中间体，该聚合物可用作将异氰酸酯转化为相应的碳二亚胺的催化剂。

4. 发明授权

US4223111A Process for preparing arylarsine substituted polystyrene 失效
标题翻译：制备芳胂取代聚苯乙烯的方法
公开(公告)号：US4223111A
公开(公告)日：1980-09-16
申请号：US069763
申请日：1979-08-27
申请人： Curtis P. Smith , George H. Temme
发明人： Curtis P. Smith , George H. Temme
IPC分类号： C08F8/42 , C08F8/22 , C08F8/24
CPC分类号： C08F8/42
摘要： A process is described for the preparation of a polymer having a recurring unit of the formula: ##STR1## where R is hydrogen or methyl, C.sub.n H.sub.2n is lower-alkylene, R.sub.1 and R.sub.2 are aryl and x is 0 or 1. A polymer having a recurring unit of the formula: ##STR2## where X is chloro, bromo, iodo, chloroalkyl, bromoalkyl or iodoalkyl, is reacted with a triarylarsine in the presence of lithium or sodium-potassium alloy. The resulting polymer is an intermediate in the preparation, by oxidation, of the corresponding As-oxide. The latter is useful as a catalyst for the conversion of isocyanates to the corresponding carbodiimides.
摘要翻译：描述了制备具有下式的重复单元的聚合物的方法：其中R是氢或甲基，C n H 2n是低级亚烷基，R 1和R 2是芳基，x是0或1.具有在锂或钠 - 钾合金存在下，其中X是氯，溴，碘，氯烷基，溴烷基或碘代烷基的重复单元与三芳基胂反应。所得聚合物是通过氧化制备相应的As-氧化物的中间体。后者可用作将异氰酸酯转化成相应的碳二亚胺的催化剂。

5. 发明授权

US06858282B2 Textured graphite sheet infused with a sealant 有权
标题翻译：纹理石墨片注入密封剂
公开(公告)号：US06858282B2
公开(公告)日：2005-02-22
申请号：US10111627
申请日：2000-12-14
申请人： George H. Temme
发明人： George H. Temme
IPC分类号： B32B3/26 , B32B9/00 , C04B41/48 , C04B41/83 , H01M8/02 , B32B3/24
CPC分类号： B32B9/00 , B32B3/06 , B32B3/26 , B32B2305/026 , B32B2457/18 , C04B41/009 , C04B41/483 , C04B41/83 , C04B2111/00853 , H01M8/0213 , H01M8/0226 , H01M8/0234 , H01M8/0239 , H01M8/0271 , Y10T428/24273 , Y10T428/24322 , Y10T428/24331 , Y10T428/24339 , Y10T428/24347 , Y10T428/249955 , Y10T428/249956 , Y10T428/249994 , Y10T428/30 , C04B41/457 , C04B35/522
摘要： A method for sealing flexible graphite sheets formed from exfoliated graphite particles is provided. A textured surface is provided onto the graphite sheet to facilitate the infusion of a sealant into the internal pores of the sheet.
摘要翻译：提供了一种用于密封由剥离石墨颗粒形成的柔性石墨片的方法。在石墨片上提供有纹理的表面，以便于将密封剂浸入片材的内部孔中。

6. 发明授权

US4570010A Product 失效
标题翻译：产品
公开(公告)号：US4570010A
公开(公告)日：1986-02-11
申请号：US478128
申请日：1983-03-23
申请人： Fred A. Stuber , George H. Temme
发明人： Fred A. Stuber , George H. Temme
IPC分类号： C07F7/08 , C08G18/61 , C08G77/388 , C08G77/392 , C07F7/10
CPC分类号： C08G77/388 , C07F7/0854 , C08G18/61 , C08G77/392 , C08G2120/00 , C08G2125/00 , Y10S264/83
摘要： Disclosed is an improved process for the production of organic polyisocyanate-based molded polymers prepared from at least one organic polyisocyanate and at least one polyol wherein there is employed an internal mold release agent comprising an amino-polysiloxane having at least one group of the formulaRNH-alkylene--O--bonded to a silicon atom of a polysiloxane, wherein R is selected from the group consisting of hydrogen, lower-alkyl, cycloalkyl, and ECHR"CHR'-- wherein E is an electron withdrawing group and R' and R" are independently selected from the group consisting of hydrogen and methyl.The molding process can be repeated many times before the mold surfaces must be cleaned or treated with release agent. The ease of release of the molded polyurethanes makes the process particularly suitable for RIM production methods.
摘要翻译：公开了一种用于生产由至少一种有机多异氰酸酯和至少一种多元醇制备的有机多异氰酸酯基模制聚合物的改进方法，其中使用内部脱模剂，其包含具有至少一个式RNH的氨基 - 聚硅氧烷 - 亚烷基-O-键合到聚硅氧烷的硅原子上，其中R选自氢，低级烷基，环烷基和ECHR'CHR'，其中E是吸电子基团，R'和R “独立地选自氢和甲基。在模具表面必须用脱模剂清洁或处理之前，可以重复成型过程多次。模制聚氨酯的易释放使得该方法特别适用于RIM生产方法。

7. 发明授权

US07305884B1 In situ monitoring of reactive material using ultrasound 失效
标题翻译：使用超声波原位监测反应性物质
公开(公告)号：US07305884B1
公开(公告)日：2007-12-11
申请号：US11107832
申请日：2005-04-18
申请人： Gregory T. Schueneman , George H. Temme
发明人： Gregory T. Schueneman , George H. Temme
IPC分类号： G01N29/00
CPC分类号： G01N29/07 , G01N29/0645 , G01N29/4445 , G01N2291/011 , G01N2291/044 , G01N2291/101
摘要： The present invention provides a device and method of non-destructively monitoring reactive material through a substrate for changes in material properties that designate the condition of the reactive material during cure and service life. A transducer is placed on a portion of the substrate generally parallel to an interface of the substrate to the reactive material. The ultrasonic waves generated via the transducer are used to detect reflected sound waves upon encountering the interfaces, where the interfaces consist of changes in material properties across the substrate.
摘要翻译：本发明提供了一种通过基材非破坏性地监测反应性材料的装置和方法，用于在固化和使用寿命期间指示反应性材料的状态的材料性质的变化。传感器放置在基板的大致平行于基板与反应性材料的界面的部分上。通过传感器产生的超声波用于在遇到界面时检测反射的声波，其中界面由穿过基底的材料性质的变化组成。

8. 发明授权

US4764330A Process for the production of organic polyisocyanate-based molded polymers 失效
标题翻译：用于生产有机多异氰酸酯的模塑聚合物的方法
公开(公告)号：US4764330A
公开(公告)日：1988-08-16
申请号：US794989
申请日：1985-11-04
申请人： Fred A. Stuber , George H. Temme
发明人： Fred A. Stuber , George H. Temme
IPC分类号： C07F7/08 , C08G18/61 , C08G77/388 , C08G77/392 , B29C45/00
CPC分类号： C07F7/0854 , C08G18/61 , C08G77/388 , C08G77/392 , C08G2120/00 , C08G2125/00
摘要： An improved process for the production of organic polyisocyanate-based molded polymers prepared from at least one organic polyisocyanate and at least one polyol wherein there is employed an internal mold release agent comprising an amino-polysiloxane having at least one group of the formulaRNH-alkylene-O-bonded to a silicon atom of a polysiloxane, wherein R is selected from the group consisting of hydrogen, lower-alkyl, cycloalkyl, and ECHR"CHR'- wherein E is an electron withdrawing group and R' and R" are independently selected from the group consisting of hydrogen and methyl. The molding process can be repeated many times before the mold surfaces must be cleaned or treated with release agent. The ease of release of the molded polyurethanes makes the process particularly suitable for RIM production methods.
摘要翻译：一种用于生产由至少一种有机聚异氰酸酯和至少一种多元醇制备的有机多异氰酸酯基模制聚合物的改进方法，其中使用内部脱模剂，其包含具有至少一个式RNH-亚烷基的氨基 - 聚硅氧烷 -O-键合到聚硅氧烷的硅原子上，其中R选自氢，低级烷基，环烷基和ECHR'CHR'，其中E是吸电子基团，R'和R“ 独立地选自氢和甲基。在模具表面必须用脱模剂清洁或处理之前，可以重复成型过程多次。模制聚氨酯的易释放使得该方法特别适用于RIM生产方法。

9. 发明授权

US4284775A 1,4-Diazabicyclooctane di-N,N'-quaternized compounds 失效
标题翻译： 1,4-二氮杂双环辛烷二-N，N'-季化合物
公开(公告)号：US4284775A
公开(公告)日：1981-08-18
申请号：US117860
申请日：1980-02-04
申请人： George H. Temme
发明人： George H. Temme
IPC分类号： C07D487/08 , C08G18/20 , C07D471/08
CPC分类号： C07D487/08 , C07C255/00 , C08G18/2063
摘要： There is disclosed a novel process for the preparation of 1,4-diazabicyclooctane dihydrohalides having the formula ##STR1## wherein each R is independently selected from the group consisting of hydrogen, lower alkyl, aryl, aralkyl, and cycloalkyl, and X is chlorine or bromine, said process comprising heating at a temperature of at least about 100.degree. C. and in a dipolar aprotic solvent certain novel dihaloalkylene diamines. Neutralization of the dihydrohalides provides the corresponding 1,4-diazabicyclooctane free bases.Also disclosed are certain novel 1,4-diazabicyclooctane diammonium dihalides formed as intermediates in the above process and a process for their conversion to the 1,4-diazabicyclooctane dihydrohalides and free bases thereof.The 1,4-diazabicyclo compounds produced in accordance with the invention find particular utility as catalysts in the preparation of polyurethanes from organic polyols and polyisocyanates.
摘要翻译：公开了一种制备具有式“IMAGE”的1,4-二氮杂双环辛烷二氢卤化物的新方法，其中每个R独立地选自氢，低级烷基，芳基，芳烷基和环烷基，X是氯或溴，所述方法包括在至少约100℃的温度和在偶极非质子溶剂中加热某些新的二卤代亚烷基二胺。二氢卤化物的中和提供相应的1,4-二氮杂双环辛烷游离碱。还公开了在上述方法中形成作为中间体的某些新的1,4-二氮杂双环辛烷二卤化二铵及其转化为1,4-二氮杂双环辛烷二氢卤化物及其游离碱的方法。根据本发明制备的1,4-二氮杂双环化合物在从有机多元醇和多异氰酸酯制备聚氨酯中特别有用。

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