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    • 6. 发明授权
    • Method of manufacturing silicided silicon microtips for scanning probe
microscopy
    • 制造用于扫描探针显微镜的硅化硅微尖头的方法
    • US6139759A
    • 2000-10-31
    • US256261
    • 1999-02-23
    • Lambert A. DoezemaPhilip V. KaszubaLeon MoszkowiczJames M. NeverJames A. Slinkman
    • Lambert A. DoezemaPhilip V. KaszubaLeon MoszkowiczJames M. NeverJames A. Slinkman
    • C25F3/08G01B7/34G01R31/02
    • G01Q60/40B82Y35/00G01Q60/30Y10S977/879
    • A micromechanical sensor probe for a scanned-probe tool comprising a silicon probe and a coating of a refractory metal silicide formed at least on the tip of the probe. Titanium silicide is preferred. A method for manufacturing such a probe includes the steps of, first, providing a silicon cantilever and tip combination and, second, forming a refractory metal silicide on at least the tip of the cantilever and tip combination. This second step of the method includes removing any remnant oxide from the tip, stabilizing the cantilever and tip combination on a carrier, depositing a refractory metal on the silicon tip, heating the cantilever and tip combination in an ambient free of oxygen to react chemically the refractory metal on and the silicon of the tip, selectively etching any unreacted refractory metal from the tip, and annealing the cantilever and tip combination in an ambient free of oxygen. The method may also include, as a final step, removing any unreacted refractory metal from the tip.
    • 一种用于扫描探针工具的微机械传感器探针,其包括硅探针和至少形成在探针尖端上的难熔金属硅化物的涂层。 硅化钛是优选的。 用于制造这种探针的方法包括以下步骤:首先提供硅悬臂和尖端组合,其次,在悬臂和尖端组合的至少尖端上形成难熔金属硅化物。 该方法的第二步骤包括从尖端去除任何残余氧化物,将悬臂和尖端组合稳定在载体上,将难熔金属沉积在硅尖端上,在不含氧的环境中加热悬臂和尖端组合以化学反应 难熔金属和尖端的硅,从尖端选择性地蚀刻任何未反应的难熔金属,并且在没有氧的环境中退火悬臂和尖端组合。 作为最后的步骤,还可以包括从尖端去除任何未反应的难熔金属。