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1. 发明申请

US20100311577A1 CaO Based Carbon Dioxide Absorbent and Method of Making 审中-公开
标题翻译： CaO基二氧化碳吸收剂及其制备方法
公开(公告)号：US20100311577A1
公开(公告)日：2010-12-09
申请号：US12479320
申请日：2009-06-05
申请人： Liyu Li , David L. King , Jun Liu , Kake Zhu , Zimin Nie , Christopher J. Howard
发明人： Liyu Li , David L. King , Jun Liu , Kake Zhu , Zimin Nie , Christopher J. Howard
IPC分类号： B01J20/04 , B01J20/30
CPC分类号： B01J20/3078 , B01D53/62 , B01D2251/402 , B01D2251/404 , B01D2257/504 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/30 , B01J20/3433 , B01J20/3483 , B82Y30/00 , Y02A50/2342 , Y02C10/04
摘要： A method for making a class of relatively stable porous carbon dioxide absorbents by mixing inert nanoparticles with a CaO precursor followed by high temperature calcination. In the preferred embodiments of this invention this process takes place in the essential absence of nitrates. In some embodiments of the invention the method further includes forming the inert nanoparticles-doped porous CaO material by decomposing a mixture of inert particles and CaO precursor material.
摘要翻译：通过将惰性纳米颗粒与CaO前体混合并进行高温煅烧来制备一类相对稳定的多孔二氧化碳吸收剂的方法。在本发明的优选实施方案中，该方法基本上不存在硝酸盐。在本发明的一些实施方案中，该方法还包括通过分解惰性颗粒和CaO前体材料的混合物来形成惰性纳米颗粒掺杂的多孔CaO材料。

2. 发明授权

US07608238B2 Nanosheets of MgO processing the 111 plane 有权
标题翻译： MgO纳米片加工111平面
公开(公告)号：US07608238B2
公开(公告)日：2009-10-27
申请号：US11356314
申请日：2006-02-17
申请人： Ryan Richards , Kake Zhu , Christian Kubel
发明人： Ryan Richards , Kake Zhu , Christian Kubel
IPC分类号： C01F5/02 , C01F5/06
CPC分类号： C01F5/02 , B01J21/10 , B82Y30/00 , C01P2002/72 , C01P2002/78 , C01P2002/82 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/20 , C01P2004/62 , C01P2004/64 , C07C45/74 , H01M4/9016 , H01M8/1011 , Y02E60/523 , Y02P70/56 , C07C49/796
摘要： Periclase MgO having a nanosheet structure. The distance of the lattice planes in HRTEM is −0.24 nm-0.25 nm. Method of preparing periclase MgO having a nanosheet structure including preparation of Mg(OCH3)2 in methanol solution. 4-methoxy benzy alcohol (MBZ) or 4-nitro benzyl alcohol (NBZ) or a mixture thereof is added in a ration of Mg to MBZ and/or NBZ of at least 1. Water/methanol mixture is added to the system. Solvent removal and calcinations in air is performed of the mixture.
摘要翻译： Periclase MgO具有纳米片结构。 HRTEM中晶格面的距离为-0.24nm-0.25nm。制备具有包括在甲醇溶液中制备Mg（OCH 3）2）的纳米片结构的微晶玻璃的方法。以至少为1的Mg至MBZ和/或NBZ的比例加入4-甲氧基苄醇（MBZ）或4-硝基苄醇（NBZ）或其混合物。将水/甲醇混合物加入到该体系中。在混合物中进行空气中的溶剂去除和煅烧。

3. 发明授权

US07417008B2 Supported polyoxometalates and process for their preparation 失效
标题翻译：负载型多金属氧酸盐及其制备方法
公开(公告)号：US07417008B2
公开(公告)日：2008-08-26
申请号：US11443683
申请日：2006-05-31
申请人： Ryan M. Richards , Ulrich Kortz , Lihua Bi , Kake Zhu
发明人： Ryan M. Richards , Ulrich Kortz , Lihua Bi , Kake Zhu
IPC分类号： B01J23/00 , C01G41/02 , C07C45/00 , C07C27/00
CPC分类号： B01J27/188 , B01J23/6527 , B01J23/888 , C01G1/00 , C01G41/006 , C01G49/009 , C01G53/006 , C01P2002/52
摘要： The invention relates to supported polyoxometalates represented by the formula (An)m+ [M4(H2O)10(XW9O33)2]m− or solvates thereof, wherein A represents a cation, n is the number of cations, m is the charge of the polyoxoanion, M is a transition metal, and X is an element selected from the group consisting of As, Sb, Bi, Se and Te, characterized in that the polyoxometalate is supported on a solid support selected from the group consisting of Al2O3, MgO, TiO2, ZrO2, SiO2, mesoporous silica, active carbon, diatomite, clays, zeolites, polyoxometalate salts and mixtures thereof, with the proviso that the polyoxometalate salt supports are different from the supported polyoxometalates defined by the above formula, a process for their preparation and their use for the catalytic oxidation of organic molecules.
摘要翻译：本发明涉及由式（Ⅳ）表示的负载型多金属氧酸盐：[M n O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O ）10 （XW 9 O 33）其中m - 或其溶剂化物其中A表示阳离子，n为阳离子数，m为多氧阴离子的电荷，M为过渡金属，X为选自As，Sb，Bi，Se和Te的元素，其特征在于其中所述多金属氧酸盐负载在选自由Al 2 O 3，MgO，TiO 2，ZrO 2，Na 2 O 3， > 2，SiO 2，介孔二氧化硅，活性炭，硅藻土，粘土，沸石，多金属氧酸盐及其混合物，条件是多金属氧酸盐载体不同于负载的多金属氧酸盐定义通过上式，其制备方法及其用于有机分子的催化氧化。

4. 发明申请

US20080014140A1 Fabrication of hierarchical zeolites 有权
标题翻译：分层沸石的制造
公开(公告)号：US20080014140A1
公开(公告)日：2008-01-17
申请号：US11819444
申请日：2007-06-27
申请人： Claus Christensen , Kake Zhu , Marina Kustova , Kresten Egeblad
发明人： Claus Christensen , Kake Zhu , Marina Kustova , Kresten Egeblad
IPC分类号： B01J29/00
CPC分类号： C01B37/02 , C01B39/02 , C01B39/04 , C01B39/24 , C01B39/36 , C01B39/365 , C01B39/38 , C01B39/40
摘要： A method for producing zeolite or zeotype crystals with a hierarchical pore system having both pores with average diameter between 0.3-2 nm and pores with an average diameter size larger than 4 nm in diameter, comprising the steps of applying a carbohydrate or a carbohydrate solution onto a zeolite precursor material or into a zeolite precursor composition, partly or fully decomposing the carbohydrate, crystallizing the zeolite, removing the partly or fully decomposed carbohydrate by calcination or combustion.
摘要翻译：一种生产沸石或沸石晶体的方法，其分级孔系统具有平均直径在0.3-2nm之间的孔和直径大于4nm的平均直径尺寸的孔，包括以下步骤：将碳水化合物或碳水化合物溶液施加到沸石前体材料或沸石前体组合物，部分或全部分解碳水化合物，使沸石结晶，通过煅烧或燃烧除去部分或完全分解的碳水化合物。

5. 发明申请

US20070196266A1 Nanosheets of MgO processing the 111 plane and method of manufacturing the same 有权
标题翻译： MgO纳米片加工111平面及其制造方法
公开(公告)号：US20070196266A1
公开(公告)日：2007-08-23
申请号：US11356314
申请日：2006-02-17
申请人： Ryan Richards , Kake Zhu , Christian Kubel
发明人： Ryan Richards , Kake Zhu , Christian Kubel
IPC分类号： C01F5/14
CPC分类号： C01F5/02 , B01J21/10 , B82Y30/00 , C01P2002/72 , C01P2002/78 , C01P2002/82 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/20 , C01P2004/62 , C01P2004/64 , C07C45/74 , H01M4/9016 , H01M8/1011 , Y02E60/523 , Y02P70/56 , C07C49/796
摘要： Periclase MgO having a nanosheet structure. The distance of the lattice planes in HRTEM is −0.24 nm-0.25 nm. Metod of preparing periclase MgO having a nanosheet structure including preparation of Mg(OCH3)2 in methanol solution. 4-methoxy benzy alcohol (MBZ) or 4-nitro benzyl alcohol (NBZ) or a mixture thereof is added in a ration of Mg to MBZ and/or NBZ of at least 1. Water/methanol mixture is added to the system. Solvent removal and calcinations in air is performed of the mixture.
摘要翻译： Periclase MgO具有纳米片结构。 HRTEM中晶格面的距离为-0.24nm-0.25nm。制备具有包括在甲醇溶液中制备Mg（OCH 3）2）的纳米片结构的玻璃化酶MgO的方法。以至少为1的Mg至MBZ和/或NBZ的比例加入4-甲氧基苄醇（MBZ）或4-硝基苄醇（NBZ）或其混合物。将水/甲醇混合物加入到该体系中。在混合物中进行空气中的溶剂去除和煅烧。

6. 发明授权

US07824657B2 Fabrication of hierarchical zeolites 有权
标题翻译：分层沸石的制造
公开(公告)号：US07824657B2
公开(公告)日：2010-11-02
申请号：US11819444
申请日：2007-06-27
申请人： Claus Hviid Christensen , Kake Zhu , Marina Kegnaes , Kresten Egeblad
发明人： Claus Hviid Christensen , Kake Zhu , Marina Kegnaes , Kresten Egeblad
IPC分类号： C01B39/02 , C01B33/02
CPC分类号： C01B37/02 , C01B39/02 , C01B39/04 , C01B39/24 , C01B39/36 , C01B39/365 , C01B39/38 , C01B39/40
摘要： A method for producing zeolite or zeotype crystals with a hierarchical pore system having both pores with average diameter between 0.3-2 nm and pores with an average diameter size larger than 4 nm in diameter, comprising the steps of applying a carbohydrate or a carbohydrate solution onto a zeolite precursor material or into a zeolite precursor composition, partly or fully decomposing the carbohydrate, crystallizing the zeolite, removing the partly or fully decomposed carbohydrate by calcination or combustion.
摘要翻译：一种生产沸石或沸石晶体的方法，其分级孔系统具有平均直径在0.3-2nm之间的孔和直径大于4nm的平均直径尺寸的孔，包括以下步骤：将碳水化合物或碳水化合物溶液施加到沸石前体材料或沸石前体组合物，部分或全部分解碳水化合物，使沸石结晶，通过煅烧或燃烧除去部分或完全分解的碳水化合物。

7. 发明申请

US20070282138A1 Supported polyoxometalates and process for their preparation 失效
标题翻译：负载型多金属氧酸盐及其制备方法
公开(公告)号：US20070282138A1
公开(公告)日：2007-12-06
申请号：US11443683
申请日：2006-05-31
申请人： Ryan M. Richards , Ulrich Kortz , Lihua Bi , Kake Zhu
发明人： Ryan M. Richards , Ulrich Kortz , Lihua Bi , Kake Zhu
IPC分类号： C07F7/18 , C07C27/00
CPC分类号： B01J27/188 , B01J23/6527 , B01J23/888 , C01G1/00 , C01G41/006 , C01G49/009 , C01G53/006 , C01P2002/52
摘要： The invention relates to supported polyoxometalates represented by the formula (An)m+ [M4(H2O)10(XW9O33)2]m− or solvates thereof, wherein A represents a cation, n is the number of cations, m is the charge of the polyoxoanion, M is a transition metal, and X is an element selected from the group consisting of As, Sb, Bi, Se and Te, characterized in that the polyoxometalate is supported on a solid support selected from the group consisting of Al2O3, MgO, TiO2, ZrO2, SiO2, mesoporous silica, active carbon, diatomite, clays, zeolites, polyoxometalate salts and mixtures thereof, with the proviso that the polyoxometalate salt supports are different from the supported polyoxometalates defined by the above formula, a process for their preparation and their use for the catalytic oxidation of organic molecules.
摘要翻译：本发明涉及由式（Ⅳ）表示的负载型多金属氧酸盐：[M n O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O ）10 （XW 9 O 33）其中m - 或其溶剂化物其中A表示阳离子，n为阳离子数，m为多氧阴离子的电荷，M为过渡金属，X为选自As，Sb，Bi，Se和Te的元素，其特征在于其中所述多金属氧酸盐负载在选自由Al 2 O 3，MgO，TiO 2，ZrO 2，Na 2 O 3， > 2，SiO 2，介孔二氧化硅，活性炭，硅藻土，粘土，沸石，多金属氧酸盐及其混合物，条件是多金属氧酸盐载体不同于负载的多金属氧酸盐定义通过上式，其制备方法及其用于有机分子的催化氧化。

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