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    • 2. 发明申请
    • Process and apparatus for producing a pressurized product by low-temperature fractionation of air
    • 用于通过空气的低温分馏来生产加压产品的方法和装置
    • US20010052244A1
    • 2001-12-20
    • US09819951
    • 2001-03-29
    • LINDE AKTIENGESELLSCHAFT
    • Dietrich RottmannChristian Kunz
    • F25J003/00
    • F25J3/0429F25J3/04018F25J3/04024F25J3/04145F25J3/04187F25J3/04193F25J3/04303F25J3/04466F25J2200/06F25J2235/50F25J2245/40
    • For producing a pressurized product by low-temperature producing a pressurized product by low-temperature fractionation of air in a rectification system which has a high-pressure column (13) and a low-pressure column (14), a first feed airstream (12) is introduced into the high-pressure column (13), and an oxygen-rich fraction (38) from the low-pressure column (14) is brought (39) to pressure in the liquid state and introduced (41) into a mixing column (16). A second feed airstream (6, 15) is introduced into the lower region of the mixing column (16) and brought into countercurrent contact with the oxygen-rich fraction (41). The mixing column (16) is operated at a pressure (PM1S) which is lower than the operating pressure (pHDS) of the high-pressure column (13). A total airstream (1) which comprises the first and second feed airstreams is compressed (2) to a first pressure (p1) which is lower than the operating pressure (pHDS) of the high-pressure column (13) and is purified (3) at about this first pressure (p2) . The purified total airstream (4) is divided into the first (5) and the second (6) feed airstream. The first feed airstream (5) is further compressed (8) separately from the second feed airstream to a second pressure (P2) which is at least equal to the operating pressure (PHDS) of the high-pressure column (13).
    • 为了通过在具有高压塔(13)和低压塔(14)的精馏系统中低温分馏空气来低温生产加压产物来生产加压产品,第一进料气流(12 )引入高压塔(13)中,将来自低压塔(14)的富氧馏分(38)带入(39)至液态压力,并将其引入(41) 列(16)。 将第二进料气流(6,15)引入混合塔(16)的下部区域并与富氧部分(41)逆流接触。 混合塔(16)在低于高压塔(13)的操作压力(pHDS)的压力(PM1S)下操作。 包括第一和第二进料气流的总气流(1)被压缩(2)到低于高压塔(13)的操作压力(pHDS)的第一压力(p1)并被纯化(3 )在约第一压力(p2)下。 纯化的总气流(4)分为第一(5)和第二(6)进料气流。 第一进料气流(5)与第二进料气流分开进一步压缩(8)至至少等于高压塔(13)的操作压力(PHDS)的第二压力(P2)。
    • 3. 发明申请
    • Process and device for obtaining a compressed product by low temperature separation of air
    • 通过低温分离空气获得压缩产品的方法和装置
    • US20030051504A1
    • 2003-03-20
    • US10217329
    • 2002-08-13
    • LINDE AKTIENGESELLSCHAFT
    • Horst CorduanDietrich RottmannChristian Kunz
    • F25J003/00
    • F25J3/04218F25J3/04084F25J3/0409F25J3/042F25J3/04303F25J3/0446F25J3/04672F25J2200/06F25J2200/94F25J2215/50F25J2235/50
    • The process and device are used to obtain a compressed product by low temperature separation of air in a rectification system which has a pressure column and a low pressure column. A first flow of compressed and purified feedstock air is cooled in a main heat exchanger system and is fed into the pressure column. At least one fraction from the pressure column is expanded and fed into the low pressure column. An oxygen-rich fraction from the low pressure column is liquid-pressurized and delivered to a mixing column. A heat exchange medium is fed into the lower area of the mixing column and is brought into countercurrent contact with the oxygen-rich fraction. A gaseous top product is removed from the upper area of the mixing column. A product fraction is removed from the rectification system, liquid-pressurized, vaporized in indirect heat exchange with the gaseous top product of the mixing column and is withdrawn as the compressed product. Indirect heat exchange is carried out for vaporization of the liquid-pressurized product fraction in the main heat exchanger system.
    • 该方法和装置用于通过在具有压力塔和低压塔的精馏系统中低温分离空气来获得压缩产物。 压缩和净化的原料空气的第一流在主热交换器系统中冷却并进料到压力塔中。 来自压力塔的至少一个馏分膨胀并进入低压塔。 来自低压塔的富氧部分被液体加压并输送到混合塔。 将热交换介质送入混合塔的下部区域,与富氧级分逆流接触。 从混合塔的上部区域除去气态顶部产物。 将产物馏分从精馏系统中除去,液体加压,与混合塔的气态顶部产物间接热交换蒸发,并作为压缩产物取出。 进行间接热交换以在主热交换器系统中的液体加压产物馏分的蒸发。
    • 4. 发明申请
    • Air fractionation process and installation with mixing column and krypton-xenon recovery
    • 空气分馏过程和安装与混合柱和氪 - 氙气回收
    • US20040007016A1
    • 2004-01-15
    • US10601875
    • 2003-06-24
    • LINDE AKTIENGESELLSCHAFT
    • Dietrich RottmannChristian Kunz
    • F25J003/00
    • F25J3/04745C01B13/0248C01B2210/0046C01B2210/0084C01B2210/0085F25J3/04303F25J3/04466F25J3/04872F25J3/04969F25J2200/06F25J2200/34F25J2200/92F25J2200/94F25J2235/50F25J2245/50
    • A process and apparatus for low-temperature fractionation of air in a distillation column system for nitrogen-oxygen separation (5, 6) introduces into first feed air stream (4) into a distillation column system for nitrogen-oxygen separation. An oxygen-rich fraction (22) from the distillation column system for nitrogen-oxygen separation is pressurized (23) in liquid form and is added (25) to a mixing column (26). A heat transfer medium stream is introduced into the lower region of the mixing column (26) and is brought into countercurrent contact with the oxygen-rich fraction (22, 25). Gaseous top product (260) from the upper region of the mixing column (26) is introduced into an additional column (27). A liquid (38, 39, 40, 41) from the lower or middle region of the mixing column is introduced into the distillation column system. A krypton- and xenon-containing oxygen stream (44, 46, 47, 48) from the distillation column system is introduced into a krypton-xenon enriching column (36) from which a krypton- and xenon-enriched fraction (51) is obtained. A krypton- and xenon-depleted top fraction (28) is obtained from the upper region of the additional column (27).
    • 在用于氮 - 氧分离的蒸馏塔系统(5,6)中低温分馏空气的方法和装置将第一进料空气流(4)引入到用于氮 - 氧分离的蒸馏塔系统中。 来自用于氮 - 氧分离的蒸馏塔系统的富氧馏分(22)以液体形式加压(23)并加入到混合塔(26)中。 将传热介质流引入混合塔(26)的下部区域,并与富氧部分(22,25)逆流接触。 将来自混合塔(26)的上部区域的气态顶部产物(260)引入另外的塔(27)中。 将来自混合塔的下部或中部区域的液体(38,39,40,41)引入蒸馏塔系统。 将来自蒸馏塔系统的含氪和氙的氧气流(44,46,47,48)引入氪 - 氙浓缩塔(36)中,从其中获得富含氪和氙的馏分(51) 。 从附加柱(27)的上部区域获得氪和氙耗尽的顶部馏分(28)。
    • 6. 发明申请
    • Three-column system for the low-temperature fractionation of air
    • 三柱系统用于空气的低温分馏
    • US20020121106A1
    • 2002-09-05
    • US10058218
    • 2002-01-29
    • LINDE AKTIENGESELLSCHAFT
    • Dietrich RottmannChristian KunzHorst Corduan
    • F25J003/00
    • F25J3/04884F25J3/0406F25J3/04084F25J3/0409F25J3/04212F25J3/0423F25J3/04296F25J3/04303F25J3/04351F25J3/04393F25J3/04448F25J3/04454F25J3/04678F25J3/04709F25J2200/20F25J2200/32F25J2200/40F25J2205/30F25J2220/42F25J2235/50F25J2235/52F25J2245/02F25J2245/42F25J2245/50F25J2250/42F25J2250/50F25J2250/52
    • The process and the apparatus are used for the low-temperature fractionation of air in a three-column system which has a high-pressure column (5), a low-pressure column (7) and a medial column (6). Charge air (1, 2, 4) is introduced into the high-pressure column (5), where it is separated into a first oxygen-enriched liquid and a first nitrogen fraction (16). At least a part (19) of the first nitrogen fraction (16) is condensed in a first condenser/evaporator (8) to form a first liquid nitrogen fraction (20). A first oxygen-enriched fraction (22) from the high-pressure column (5) is introduced into the medial column (6), where it is separated into a second oxygen-enriched liquid and a second nitrogen fraction (24). At least a part of the second nitrogen fraction (24) is condensed in a second condenser/evaporator (25) to form a second liquid nitrogen fraction (26) and is added as reflux to one of the columns of the three-column system and/or is obtained as liquid product (64). A second oxygen-enriched fraction (29, 31) from the high-pressure column or from the medial column (6) is introduced into the low-pressure column (7), where it is separated into a third oxygen-enriched liquid and a third nitrogen fraction. Liquid reflux nitrogen (54, 60), which has not been formed in the second condenser/evaporator (25), is introduced into the medial column (6).
    • 该方法和装置用于具有高压塔(5),低压塔(7)和内侧柱(6)的三塔系统中的空气的低温分馏。 将加压空气(1,2,4)引入高压塔(5)中,在其中分离成第一富氧液体和第一氮气馏分(16)。 第一氮馏分(16)的至少一部分(19)在第一冷凝器/蒸发器(8)中冷凝以形成第一液氮馏分(20)。 将来自高压塔(5)的第一富氧馏分(22)引入到内侧柱(6)中,在其中将其分离成第二富氧液体和第二氮气馏分(24)。 第二氮馏分(24)的至少一部分在第二冷凝器/蒸发器(25)中冷凝以形成第二液氮馏分(26),并作为回流加入到三塔系统的一个塔中, /或作为液体产物(64)获得。 将来自高压塔或内侧柱(6)的第二富氧馏分(29,31)引入低压塔(7)中,将其分离成第三富氧液体, 第三氮分数。 未在第二冷凝器/蒸发器(25)中形成的液体回流氮(54,60)被引入到内侧柱(6)中。
    • 7. 发明申请
    • Process for obtaining gaseous nitrogen
    • 获得气态氮的方法
    • US20010052242A1
    • 2001-12-20
    • US09810708
    • 2001-03-19
    • Linde Aktiengesellschaft
    • Dietrich RottmannChristian Kunz
    • F25J003/00
    • F25J3/044F25J3/04321F25J3/04351
    • For obtaining gaseous nitrogen by low-temperature separation from air, a distillation column system has a single column (4). Compressed air (1) is cooled in a main heat exchanger (2) and fed (3) to single column (4). A nitrogen-rich fraction (5, 7, 8) is drawn off from the distillation column system and compressed at least in part in a circulation compressor (9, 1063). A first part (12, 13) of nitrogen-rich fraction (5, 7, 8) is fed downstream from circulation compressor (9) to the liquefaction chamber of a condenser-evaporator (14) and is condensed under a pressure higher than the operating pressure of single column (4), so to form nitrogen-rich liquid (15, 16). A liquid oxygen-enriched fraction (231) from the distillation column system is at least partially evaporated in the evaporation chamber of condenser-evaporator (14). A first oxygen-enriched gas (234, 533) formed in the evaporation chamber of condenser-evaporator (14), is introduced into single column (4). A second portion (19, 20, 1064) of the nitrogen-rich fraction (5, 7, 8) is drawn off at least at times as gaseous nitrogen product. A second oxygen-enriched gas (221, 521) is removed from the evaporation chamber of condenser-evaporator (14), work expanded (23), and heated in main heat exchanger (2).
    • 为了通过与空气进行低温分离获得气态氮,蒸馏塔系统具有单柱(4)。 压缩空气(1)在主热交换器(2)中冷却,并将(3)供给单塔(4)。 将富氮馏分(5,7,8)从蒸馏塔系统中排出并至少部分压缩在循环压缩机(9,1063)中。 将富氮馏分(5,7,8)的第一部分(12,13)从循环压缩机(9)的下游供给到冷凝器 - 蒸发器(14)的液化室,并在高于 单塔(4)的操作压力,从而形成富氮液体(15,16)。 来自蒸馏塔系统的液体富氧馏分(231)在冷凝器 - 蒸发器(14)的蒸发室中至少部分蒸发。 形成在冷凝器 - 蒸发器(14)的蒸发室中的第一富氧气体(234,533)被引入单塔(4)中。 至少有时作为气态氮产物排出富氮馏分(5,7,8)的第二部分(19,20,1046)。 第二富氧气体(221,521)从冷凝器 - 蒸发器(14)的蒸发室中移出,工作膨胀(23),并在主热交换器(2)中加热。