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1. 发明授权

US4022811A Preparation of alkyl perbromates 失效
标题翻译：制备烷基过溴酸盐
公开(公告)号：US4022811A
公开(公告)日：1977-05-10
申请号：US650829
申请日：1976-01-21
申请人： Kurt Baum , Charles D. Beard , Vitautas Grakaukas
发明人： Kurt Baum , Charles D. Beard , Vitautas Grakaukas
IPC分类号： C01B7/09 , C07C409/00 , C07C71/00
CPC分类号： C07C409/00 , C01B7/09
摘要： Derivatives of perbromic acid of the formula: XBrO.sub.4 wherein X is Ag, H.sub.3).sub.2 CH, or (CH.sub.3).sub.2 C.sub.2 H.sub.3 prepared by a synthesis of silver perbromate through the reaction of dilute aqueous perbromic acid with silver oxide at a temperature from 0.degree. to 50.degree. C, followed by a removal of water and by a synthesis of isopropyl or isobutyl perbromate through the reaction of anhydrous silver perbromate suspended in a fluid selected from the class consisting of carbon tetrachloride, cyclohexane, and 1,1,2-trichlorotrifluoroethane with an alkyl bromide at a temperature from -25.degree. to 0.degree. C. Isopropyl and isobutyl perbromates are useful as oxidizing agents for alcohols.
摘要翻译：通式为：XBrO4的过溴酸衍生物，其中X为Ag，（CH 3）2 CH或（CH 3）2 C 2 H 3），其通过在0℃至50℃的温度下通过稀水溶液与氧化银的反应合成过溴酸银制备然后除去水，并通过悬浮在选自四氯化碳，环己烷和1,1,2-三氯三氟乙烷的流体中的无水过溴化银反应合成异丙基或异丁基溴化铵，烷基溴在-25℃至0℃的温度下进行。异丙基和异丁基过溴酸盐可用作醇的氧化剂。

2. 发明授权

US4165332A Preparation of aliphatic perchlorates and of trifluoromethane sulfonates 失效
标题翻译：脂肪族高氯酸盐和三氟甲烷磺酸盐的制备
公开(公告)号：US4165332A
公开(公告)日：1979-08-21
申请号：US647395
申请日：1976-01-08
申请人： Charles D. Beard , Kurt Baum
发明人： Charles D. Beard , Kurt Baum
IPC分类号： C07C303/26 , C07C309/65 , C07C409/00 , C07C71/00
CPC分类号： C07C409/00 , C07C303/26
摘要： The formation of predominantly primary aliphatic perchlorates and trifluoethanesulfonates by reacting the corresponding silver salt with primary aliphatic halides in benzene at a temperature from about 5.degree. C. to about 50.degree. C. Primary aliphatic perchlorates and trifluoromethanesulfonates are excellent alkylating agents for amines, alcohols, and nitroalcohols.
摘要翻译：在约5℃至约50℃的温度下，通过使相应的银盐与伯脂肪族卤化物在苯中反应，主要形成主要的脂族高氯酸盐和三氟甲磺酸盐。初级脂族高氯酸盐和三氟甲磺酸盐是用于胺，醇，和硝基醇。

3. 发明授权

US4611061A 2'-hydroxy-5'-(hydroxyalkyl)phenyl-2H-benzotriazoles 失效
标题翻译： 2'-羟基-5' - （羟基烷基）苯基-2H-苯并三唑
公开(公告)号：US4611061A
公开(公告)日：1986-09-09
申请号：US592764
申请日：1984-03-26
申请人： Charles D. Beard , Namassivaya Doddi , Akira Yamada
发明人： Charles D. Beard , Namassivaya Doddi , Akira Yamada
IPC分类号： C08F20/36 , C08K5/3475 , G02B1/04 , C07D249/18
CPC分类号： G02B1/04 , C08F20/36 , C08K5/3475 , G02B1/043
摘要： The compounds 2'-hydroxy-5'-(hydroxyalkyl)phenyl-2H-benzotriazoles are useful as intermediate alcohols in the preparation of corresponding 2'-hydroxy-5'-acrylyloxyphenyl-2H-benzotriazole monomers, which in turn are copolymerizable with ethylenically unsaturated monomers, particularly acrylic monomers, to impart ultraviolet absorbing properties to the resulting copolymers.
摘要翻译：化合物2'-羟基-5' - （羟基烷基）苯基-2H-苯并三唑在制备相应的2'-羟基-5'-丙烯酰氧基苯基-2H-苯并三唑单体时可用作中间体醇，它们又可与烯键式不饱和单体，特别是丙烯酸单体，以赋予所得共聚物紫外线吸收性能。

4. 发明授权

US4528311A Ultraviolet absorbing polymers comprising 2-hydroxy-5-acrylyloxyphenyl-2H-benzotriazoles 失效
标题翻译：包含2-羟基-5-丙烯酰氧基苯基-2H-苯并三唑的紫外吸收聚合物
公开(公告)号：US4528311A
公开(公告)日：1985-07-09
申请号：US512860
申请日：1983-07-11
申请人： Charles D. Beard , Akira Yamada , Namassivaya Doddi
发明人： Charles D. Beard , Akira Yamada , Namassivaya Doddi
IPC分类号： C08F20/36 , C08K5/3475 , G02B1/04 , C08F120/26 , C08F120/36
CPC分类号： G02B1/04 , C08F20/36 , C08K5/3475 , G02B1/043
摘要： Ultraviolet light absorbing polymer compositions comprising copolymers of 2-Hydroxy-5-acrylyloxyphenyl-2H-benzotriazoles with one or more other monomers copolymerizable therewith, particularly acrylic monomers are useful in the manufacture of occular devices, particularly intraoccular lenses and contact lenses. Polymers of the disclosed benzotriazoles may be added to other organic materials to impart ultraviolet absorbing properties thereo.
摘要翻译：包含2-羟基-5-丙烯酰氧基苯基-2H-苯并三唑与一种或多种与其可共聚的其它单体，特别是丙烯酸单体的共聚物的紫外光吸收聚合物组合物可用于制造眼部装置，特别是眼内透镜和隐形眼镜。所公开的苯并三唑的聚合物可以加入到其它有机材料中以赋予其紫外线吸收性能。

5. 发明授权

US4111999A Cleavage of silylated carboranes and method for preparing meta-carborane employing same 失效
标题翻译：甲硅烷基化的碳硼烷的切割以及使用其制备偏碳硼烷的方法
公开(公告)号：US4111999A
公开(公告)日：1978-09-05
申请号：US865893
申请日：1977-12-30
申请人： Charles D. Beard , Robert B. Moffitt, III
发明人： Charles D. Beard , Robert B. Moffitt, III
IPC分类号： C07F5/02 , C07F7/08
CPC分类号： C07F7/082 , C07F5/027
摘要： A highly selective method is disclosed for cleaving carboranyl carbon-silicon bonds which comprises contacting either silylated monomeric carboranes or polymers thereof with a nucleophilic cleavage agent and, if desired, in the presence of a protic reagent and recovering the carborane cage intact. This technique is employed in a method for producing the useful meta-carborane in bulk which includes the steps of isomerizing a silylated derivative of ortho-carborane using known techniques to produce the corresponding meta-carborane derivative and then cleaving the carboranyl carbon-silicon bond to form meta-carborane.
摘要翻译：公开了用于裂解碳硼烷基碳 - 硅键的高选择性方法，其包括使甲硅烷基化的单体碳硼烷或其聚合物与亲核裂解剂接触，并且如果需要，在质子试剂存在下接触并回收完整的碳硼烷笼。该技术用于本体生产有用的偏碳硼烷的方法，其包括使用已知技术异构化邻 - 碳硼烷的甲硅烷基化衍生物以产生相应的间 - 碳硼烷衍生物，然后将碳硼烷基碳 - 硅键断开的步骤形成元碳硼烷。

6. 发明授权

US4803254A Vinylsilylalkoxy arylbenzotriazole compounds and UV absorbing compositions made therefrom 失效
标题翻译：乙烯基磺酰基烷氧基芳基苯并三唑化合物和由其制成的UV吸收组合物
公开(公告)号：US4803254A
公开(公告)日：1989-02-07
申请号：US24638
申请日：1987-03-11
申请人： Gary B. Dunks , Akira Yamada , Namassivaya Doddi , Charles D. Beard
发明人： Gary B. Dunks , Akira Yamada , Namassivaya Doddi , Charles D. Beard
IPC分类号： G02C7/00 , A61F2/16 , A61L27/18 , C07D249/20 , C07F7/08 , C07F7/10 , C07F7/12 , C08G77/00 , C08G77/26 , C08G77/28 , C08G77/388 , C08G77/42 , C08G77/452 , C09K3/00 , G02B1/04 , G02C7/04 , C08F283/12 , C08F30/08
CPC分类号： C08G77/388 , A61F2/16 , A61L27/18 , C07F7/0812 , C07F7/0818 , C08G77/04 , G02B1/043
摘要： Vinylsilylalkoxy arylbenzotriazol monomers such as 2-[3'-t-butyl-5'-(3-"-dimethylvinylsilylpropoxy)-2'-hydroxy-phenyl]-5-methoxybenzotriazole are disclosed. These monomers can be incorporated in optically clear silicone polymers to form intraocular lenses, contact lenses, and the like, which have UV absorbing properties.

7. 发明授权

US4716234A Ultraviolet absorbing polymers comprising 2-(2'-hydroxy-5'-acryloyloxyalkoxyphenyl)-2H-benzotriazole 失效
标题翻译：包含2-（2'-羟基-5'-丙烯酰氧基苯氧基苯基）-2H-苯并三唑的紫外吸收聚合物
公开(公告)号：US4716234A
公开(公告)日：1987-12-29
申请号：US937171
申请日：1986-12-01
申请人： Gary B. Dunks , Akira Yamada , Charles D. Beard , Namassivaya Doddi
发明人： Gary B. Dunks , Akira Yamada , Charles D. Beard , Namassivaya Doddi
IPC分类号： G02C7/04 , C07D249/20 , C08F20/34 , C08F20/36 , C08F220/36 , C08L57/12 , C08L101/00 , C09K3/00 , G02B1/04 , G02B5/22 , C07D249/16 , C08F120/36 , C08F232/08
CPC分类号： C07D249/20 , C08F20/36
摘要： Ultraviolet light absorbing compositions comprising 2-(2'-hydroxy-5'-acryloyloxyalkoxyphenyl(-2H-benzotrizoles, and copolymers thereof with one or more other monomers copolyermizable therewith, particularly acrylic monomers, are useful in the manufacture of ocular devices, particularly intraocular lenses and contact lenses.

8. 发明授权

US4153672A Synthesis of tetradecahydroundecaborate (-1) from borohydride ion 失效
标题翻译：从硼氢化物离子合成十四氢十硼酸盐（{31 1）
公开(公告)号：US4153672A
公开(公告)日：1979-05-08
申请号：US926757
申请日：1978-07-21
申请人： Gary B. Dunks , Charles D. Beard
发明人： Gary B. Dunks , Charles D. Beard
IPC分类号： C01B6/10 , C01B35/00 , C01B35/18 , C07F5/02
CPC分类号： C01B35/00
摘要： The tetradecahydroundecaborate(-1) anion is synthesized from a metal borohydride by heating a suspension of the borohydride ion in a solvent, such as diglyme, with agitation at a temperature of from 85.degree. C. to about 135.degree. C. and adding an alkyl halide. The B.sub.11 H.sub.14.sup.- anion obtained is useful in the synthesis of decaborane, an intermediate in formation a carborane-based polymers.
摘要翻译： {PG，1]通过在溶剂例如二甘醇二甲醚中加热硼氢化物离子的悬浮液，在85（20℃至约20℃）的温度下，从金属硼氢化合物合成十四氢十硼酸盐（{31 1） 135 {20 {0℃并加入烷基卤化物。 B {HD 11 {L H {HD 14 {HU {31 {L阴离子获得可用于合成十硼烷，形成中间体为碳硼烷基聚合物。

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