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1. 发明授权

US5153066A Temperature-sensitive color-changeable composite fiber 失效
标题翻译：温度敏感的可变色复合纤维
公开(公告)号：US5153066A
公开(公告)日：1992-10-06
申请号：US555608
申请日：1990-07-23
申请人： Kazuhiko Tanaka , Masao Kawamoto , Kenji Hiramatsu , Tsutomu Kito , Kuniyuki Senga
发明人： Kazuhiko Tanaka , Masao Kawamoto , Kenji Hiramatsu , Tsutomu Kito , Kuniyuki Senga
IPC分类号： D01F1/06 , D01F1/04 , D01F8/04 , D01F8/06 , D01F8/12 , D01F8/14
CPC分类号： D01F1/04 , D01F8/04 , Y10S428/913 , Y10T428/2929
摘要： A temperature-sensitive color-changeable composite fiber wherein (A) a thermally color-changeable polymer phase (phase A) composed essentially of a thermally color-changeable material and a thermoplastic polymer having a melting point or a softening point of 230.degree. C. or lower, the content of the thermally color-changeable material being 0.5 to 90% by weight and (B) a protective polymer (phase B) composed essentially of a fiber-forming thermoplastic polymer are brought into contact with each other, (i) the protective polymer phase (phase B) occupying at least 60% of the fiber surface area, and (ii) the protective polymer phase (phase B) occupying 20 to 95% by weight relative to the overall fiber. The composite fiber of this invention has reversibly thermally color-changeable performance of excellent temperature-sensitive color-changeability, color vividness, washing durability and light resistance.

2. 发明授权

US5721059A Temperature-dependent color/transparency storing resin composition and laminate member employing the same 失效
标题翻译：储存树脂组合物的温度依赖性颜色/透明度和采用该组合物的层压构件
公开(公告)号：US5721059A
公开(公告)日：1998-02-24
申请号：US705148
申请日：1996-08-29
申请人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
发明人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
IPC分类号： B41M5/337 , B32B27/18 , B32B27/28 , B32B27/30 , B41M5/36 , C08K5/00 , C08K5/05 , C08K5/07 , C08K5/09 , C08K5/10 , C08K5/16 , C08K5/34 , C08K5/3435 , C08L27/00 , C08L27/06 , C09K9/02 , B32B27/08
CPC分类号： C08K5/0008 , B41M5/305 , Y10S428/913 , Y10T428/31928 , Y10T428/31935
摘要： A temperature-dependent color/transparency storing resin layer is composed by dispersing and fixing a mutually dissolved homogeneous composition consisting of (A) an electron-donating color-developing organic compound, (B) a compound having a phenolic hydroxyl radical, and (C) a compound selected from alcohols, esters, ketones and carboxylic acids, in vinyl chloride-vinyl acetate-copolymer matrix resin, as small particles, and capable of exhibiting reversible change in color and in transparency in response to a temperature variation with hysteresis, and selectively storing a state developed above the high trigger temperature and a state developed below the low trigger temperature in a temperature range between the high and low trigger temperatures, wherein the transparency is improved by blending vinyl chloride-vinyl acetate-vinyl alcohol copolymer and/or vinyl chloride-vinylidene chloride copolymer as an agent for improving the transparency in said matrix resin so as to regulate the transparency and to conspicuously improve the transparency especially exhibited in a temperature range above the high trigger temperature, so as to constitute a laminate member to be applied in various fields.
摘要翻译：通过分散和固定由（A）给电子显色性有机化合物（B）具有酚羟基的化合物和（C）的（C）化合物组成的相互溶解的均匀组合物来构成温度依赖的颜色/透明度储存树脂层）选自醇，酯，酮和羧酸的化合物，在氯乙烯 - 乙酸乙烯酯共聚物基质树脂中作为小颗粒，并且能够响应于滞后的温度变化而呈现可逆的颜色变化和透明度，以及选择性地存储在高触发温度之上发展的状态和在低触发温度和低触发温度之间的温度范围内低于低触发温度发展的状态，其中透明度通过混合氯乙烯 - 乙酸乙烯酯 - 乙烯醇共聚物和/或氯乙烯 - 偏二氯乙烯共聚物作为改善所述基体树脂透明度的试剂，以调节t 透明性，并显着提高特别是在高触发温度以上的温度范围内显示的透明性，从而构成应用于各种领域的层叠构件。

3. 发明授权

US5585425A Thermochromic opaque/transparent composition, laminate member employing the same, and three-dimensional member employing said laminate member and capable of concealing and revealing the interior 失效
标题翻译：热变色不透明/透明组合物，使用其的层合构件和采用所述层压构件并能够隐藏和露出内部的三维构件
公开(公告)号：US5585425A
公开(公告)日：1996-12-17
申请号：US409057
申请日：1995-03-23
申请人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
发明人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
IPC分类号： B41M5/337 , B44F1/08 , C09B67/08 , C09B67/46 , C09K9/02 , C08K5/13
CPC分类号： B44F1/08 , C09K9/02 , Y10T428/31928 , Y10T428/31935
摘要： A thermochromic opaque/transparent composition is capable of exhibiting change in transparency together with change in color in response to temperature variation, a laminate member employing the same, and a three-dimensional article capable of concealing and revealing the interior, utilizing the laminate member. A thermochromic opaque/transparent composition is composed of dispersion, in vinyl chloridevinyl acetate copolymer matric resin, which has been obtained by blending with hindered amine compound selected from piperidine derivatives within a particle size range of 0.1 to 2.0 .mu.m, of a reversible thermochromic material consisting of (a) an electron-donating color-developing organic compound, (b) a compound having a phenolic hydroxyl radical, and (c) a homogeneous fused composition containing a compound selected from alcohols, esters, ketones and carboxylic acids, and capable of exhibiting reversible change in transparency together with change in color in response to temperature variation, with hysteresis with a temperature difference of 10.degree. C. to 50.degree. C. between the low and high trigger temperatures.
摘要翻译：热变色不透明/透明组合物能够随着温度变化而显示出透明度的变化以及颜色的变化，使用该组合物的层压构件和能够利用层压构件隐藏和露出内部的三维制品。热变色不透明/透明组合物由在氯乙烯醋酸乙烯酯共聚物树脂中的分散体组成，其通过与选自0.1至2.0μm的粒度范围的哌啶衍生物的受阻胺化合物共混获得可逆热变色材料包括（a）给电子显色有机化合物，（b）具有酚羟基的化合物，和（c）含有选自醇，酯，酮和羧酸的化合物的均相熔融组合物，表现出透明度的可逆变化以及响应于温度变化的颜色变化，在低和高触发温度之间具有10℃至50℃的温度差的滞后。

4. 发明授权

US5490956A Thermochromic opaque composition, laminate member employing the same, and three-dimensional member employing said laminate member and capable of concealing and revealing the interior 失效
标题翻译：热变色不透明组合物，使用其的层压构件和采用所述层压构件并能够隐藏和露出内部的三维构件
公开(公告)号：US5490956A
公开(公告)日：1996-02-13
申请号：US139024
申请日：1993-10-21
申请人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
发明人： Tsutomu Kito , Kuniyuki Senga , Hiroyuki Hayashi
IPC分类号： A63H33/22 , B32B7/02 , B32B27/20 , B41M5/337 , B43L13/00 , B44F1/08 , C09K9/02 , G02F1/00 , C08K5/00
CPC分类号： B41M5/305 , B41M5/3335 , B41M5/3372 , B41M5/3375 , B44F1/08 , C09K9/02 , B41M2205/04 , B41M5/327 , B41M5/3275 , Y10S252/962
摘要： There are provided a thermochromic opaque composition capable of exhibiting change in transparency together with change in color in response to temperature variation, a laminate member employing the same, and a three-dimensional article capable of concealing and revealing the interior, utilizing the laminate member. The thermochromic oaque composition is formed by dispersing a thermochromic material, capable of developing and erasing color by an electron donating-accepting reaction, in small particles in vinyl chloride-vinyl acetate matrix resin. The above-mentioned structure realizes reversible change in transparency, together with change in color, in response to temperature variation, with hysteresis with a temperature difference of 10.degree. C. at minimum to 50.degree. C. between the high and low trigger temperatures.
摘要翻译：提供一种热变色不透明组合物，其能够随着温度变化而随着颜色变化而呈现出透明性的变化，使用该变色的层压构件和能够利用层压构件隐藏和露出内部的三维制品。热变色蜡组合物通过在氯乙烯 - 乙酸乙烯酯基质树脂中的小颗粒中分散能够通过给电子接受反应显影和消除颜色的热变色材料形成。上述结构在高和低触发温度之间实现透明度的可逆变化以及响应于温度变化的颜色变化，在10℃的温度差下具有最小至50℃的滞后。

5. 发明授权

US5879443A Temperature-sensitive color-memorizing microencapsulated pigment 失效
标题翻译：温度敏感色记忆微囊化颜料
公开(公告)号：US5879443A
公开(公告)日：1999-03-09
申请号：US867646
申请日：1997-06-02
申请人： Kuniyuki Senga , Tsutomu Kito
发明人： Kuniyuki Senga , Tsutomu Kito
IPC分类号： C08K9/10 , C09B67/02 , C08K5/00
CPC分类号： C08K9/10 , C09B67/0097 , B41M5/305 , Y10S252/962
摘要： A microcapsulated pigment contains, as reaction media one or more specific aliphatic acid alcohol esters obtained from monohydric aliphatic alcohols having odd numbers of carbon atoms and aliphatic carboxylic acids, these reaction media in a homogeneous compatible state with chromatic components are occluded in microcapsules to obtain characteristics of thermochromism with a hysteresis range (segment HG) from 8.degree. C. to 30.degree. C.
摘要翻译：作为反应介质，微胶囊化颜料含有由具有奇数个碳原子的一元脂肪醇和脂肪族羧酸获得的一种或多种特定的脂肪酸醇酯，将这些与有色成分均匀相容的反应介质封闭在微胶囊中以获得特征具有8℃至30℃的滞后范围（段HG）的热致变色

6. 发明授权

US5785746A Preparation method for shear-thinning water-based ball-point pen inks compositions and ball-point pens employing the same 失效
标题翻译：用于剪切稀释水性圆珠笔墨水组合物的制备方法和使用其的圆珠笔
公开(公告)号：US5785746A
公开(公告)日：1998-07-28
申请号：US794091
申请日：1997-02-03
申请人： Tsutomu Kito , Kuniyuki Senga
发明人： Tsutomu Kito , Kuniyuki Senga
IPC分类号： B43K1/08 , C09D11/18
CPC分类号： B43K1/086 , C09D11/18
摘要： A shear-thinning water-based ball-point pen ink composition comprising from 1% by weight to 35% by weight of a colorant, from 2% by weight to 35% by weight of a water-soluble polar solvent, from 1% by weight to 30% by weight of a nonionic surface active agent having an HLB value within the range of from 8 to 12, and the balance being water and adjusting additives, and having a viscosity within the range of from 25 mPa.s to 160 mPa.s (a value at the number of revolution of 100 rpm in an EM type rotational viscometer, 25.degree. C.) and a shear thinning index within the range of from 0.1 to 0.6; the nonionic surface active agent having a mixed phase comprising a phase standing dispersed in the form of fine particles and a phase standing dissolved in a molecular state.
摘要翻译：一种剪切稀释的水性圆珠笔墨水组合物，其包含1重量％至35重量％的着色剂，2重量％至35重量％的水溶性极性溶剂，1重量％重量至30重量％的HLB值在8至12范围内的非离子表面活性剂，余量为水和调节添加剂，粘度范围为25mPa.s至160mPa （EM型旋转粘度计中的旋转次数为100rpm，25℃），剪切稀化指数在0.1〜0.6的范围内; 该非离子表面活性剂具有混合相，该混合相包含以细颗粒形式分散的相和以分子状态溶解的相。

7. 发明申请

US20050014444A1 Reversibly metachromatic toy 有权
标题翻译：可逆的变色玩具
公开(公告)号：US20050014444A1
公开(公告)日：2005-01-20
申请号：US10790773
申请日：2004-03-03
申请人： Hiroki Harata , Kuniyuki Senga , Masanori Takeda
发明人： Hiroki Harata , Kuniyuki Senga , Masanori Takeda
IPC分类号： G09B19/00 , A63H33/22 , A63H33/38 , B32B5/18 , B41M3/00 , B41M5/00 , B41M5/52 , B42D1/00 , B44F1/06 , A63H33/00 , G02F1/01
CPC分类号： B32B5/18 , A63H33/22 , A63H33/38 , B32B7/12 , B32B27/065 , B32B27/304 , B32B27/32 , B32B27/34 , B32B27/36 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2307/4026 , B32B2307/412 , B32B2375/00 , B41M3/001 , B41M5/52 , B44F1/066 , Y10T428/249953
摘要： A reversibly metachromatic toy having a platelike resin foamed substrate, a resin layer provided on both the outer side surfaces of the foamed substrate, and a reversibly metachromatic layer provided on at least one-side resin layer partly or all over the surface.
摘要翻译：一种具有板状树脂发泡基板的可逆变色玩具，设置在发泡基板的两个外表面上的树脂层和在表面上部分或全部至少一侧树脂层上设置的可逆异色层。

8. 发明授权

US07332109B2 Thermally color-developing reversibly thermochromic pigment 有权
标题翻译：热变色可逆热变色颜料
公开(公告)号：US07332109B2
公开(公告)日：2008-02-19
申请号：US10323844
申请日：2002-12-20
申请人： Kuniyuki Senga , Katsuyuki Fujita , Shigehiro Koide
发明人： Kuniyuki Senga , Katsuyuki Fujita , Shigehiro Koide
IPC分类号： G02B5/22 , G02B5/20 , G02F1/01
CPC分类号： B41M5/3375 , B41M5/28 , B41M5/305
摘要： A thermally color-developing reversibly thermochromic pigment which shows a uniform color density in the coloring temperature range and also shows an optimal ΔH value within a range of from 3 to 40° C. Thermally color-developing reversibly thermochromic pigments of a three component system having a ΔH value within a range of from 7 to 40° C. in which at least essential three components including (a) an electron-donating chromic organic compound, (b) a specified compound selected from the gallic acid esters and (c) a reaction medium selected from alcohols, esters, ketones and hydrocarbons; which reversibly generates color reactions of both of the compounds within a specified temperature range and has a melting point of less than 50° C., are microencapsulated, and of a four component system having a ΔH value within a range of from 3 to 25° C. in which a compound (d) selected from monomer compounds having a melting point of 50° C. or more or polymer compounds having a softening point of 70° C. or more is added to the three component system.
摘要翻译：一种热显色可逆热变色颜料，其在着色温度范围内显示均匀的色密度，并且还显示出在3至40℃范围内的最佳ΔH值。具有三组分体系的热显色可逆热变色颜料至少必要的三种组分，包括（a）给电子的铬有机化合物，（b）选自没食子酸酯的特定化合物和（c）a 选自醇，酯，酮和烃的反应介质; 其可以在特定温度范围内可逆地产生两种化合物的显色反应，并且具有低于50℃的熔点，微胶囊化，以及ΔH值在3至25°范围内的四组分体系其中将选自熔点为50℃以上的单体化合物的化合物（d）或软化点为70℃以上的高分子化合物加入到三组分体系中。

9. 发明授权

US06494950B1 Thermochromic microencapsulated pigments 有权
标题翻译：热变色微胶囊化颜料
公开(公告)号：US06494950B1
公开(公告)日：2002-12-17
申请号：US09664062
申请日：2000-09-18
申请人： Katsuyuki Fujita , Kuniyuki Senga
发明人： Katsuyuki Fujita , Kuniyuki Senga
IPC分类号： B41M530
CPC分类号： B41M5/3375 , B41M5/284 , B41M5/305 , C09B67/0097 , C09K9/02 , Y10S252/962 , Y10S428/913 , Y10T428/2984
摘要： Disclosed is a thermochromic microencapsulated pigment which comprises as four essential components (a) an electron-donating chromatic organic compound, (b) an electron-accepting compound, (c) a reaction medium determining the temperatures at which the color reactions of component (a) with component (b) take place, and (d) a color change temperature regulator, the color change temperature regulator (d) comprising one or more compounds selected from the group consisting of esters, alcohols, ketones, acid amides, hydrocarbons, and fatty acids and having a melting point Y (° C.) satisfying the relationship (X+30)° C.≦Y≦200° C., wherein X (° C.) is the melting point of component (c), and the four essential components being microencapsulated.
摘要翻译：公开了一种热变色微胶囊化颜料，其包含四种基本组分（a）给电子有机有机化合物，（b）电子接受性化合物，（c）反应介质，其确定组分（a ）和（d）变色温度调节剂，所述变色温度调节剂（d）包含一种或多种选自酯，醇，酮，酰胺，烃的化合物和脂肪酸，其熔点Y（℃）满足关系式（X + 30）℃。<= Y <= 200℃，其中X（℃）是组分（c）的熔点，，并且四个基本组分被微胶囊化。

10. 发明授权

US07189133B2 Reversibly metachromatic toy 有权
标题翻译：可逆的变色玩具
公开(公告)号：US07189133B2
公开(公告)日：2007-03-13
申请号：US10790773
申请日：2004-03-03
申请人： Hiroki Harata , Kuniyuki Senga , Masanori Takeda
发明人： Hiroki Harata , Kuniyuki Senga , Masanori Takeda
IPC分类号： A63H33/00
CPC分类号： B32B5/18 , A63H33/22 , A63H33/38 , B32B7/12 , B32B27/065 , B32B27/304 , B32B27/32 , B32B27/34 , B32B27/36 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2307/4026 , B32B2307/412 , B32B2375/00 , B41M3/001 , B41M5/52 , B44F1/066 , Y10T428/249953
摘要： A reversibly metachromatic toy having a platelike resin foamed substrate, a resin layer provided on both the outer side surfaces of the foamed substrate, and a reversibly metachromatic layer provided on at least one-side resin layer partly or all over the surface.
摘要翻译：一种具有板状树脂发泡基板的可逆变色玩具，设置在发泡基板的两个外表面上的树脂层和在表面上部分或全部的至少一侧树脂层上设置的可逆异色层。

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