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1. 发明授权

US06617029B2 Nitrogen-containing flame retarding epoxy resin and an epoxy resin composition containing the same 有权
标题翻译：含氮阻燃环氧树脂和含有该阻燃环氧树脂的环氧树脂组合物
公开(公告)号：US06617029B2
公开(公告)日：2003-09-09
申请号：US10035238
申请日：2002-01-04
申请人： Kuen-Yuan Hwang , Hong-Hsing Chen , Chih-Fu Chen , Huan-Chang Chao
发明人： Kuen-Yuan Hwang , Hong-Hsing Chen , Chih-Fu Chen , Huan-Chang Chao
IPC分类号： B32B2738
CPC分类号： C08K5/34922 , H05K1/0326 , Y10T428/31511 , C08L63/00
摘要： The present invention relates to a nitrogen-containing epoxy resin of the following formula: wherein R's are the same or different and each represents a hydrogen atom or —R13—C6-10 aryl-(OR14)p, and the aryl group is optionally substituted with C1-6 alkyl group, in which R13 represents a C1-6 alkylene group or a phenylene —CH2— group optionally substituted with a hydroxy group, R14 represents a glycidyl group, and p is an integer of 1 or 2, provided that at least one R group is not a hydrogen atom; R1 represents a phenyl group or —N(R)2 group in which R is defined as above. The resin is produced from sequentially reacting melamine derivatives with aldehydes, phenolic compounds, and epihalohydrin. The nitrogen-containing epoxy resin, alone or as part of an epoxy resin composition, provides excellent flame-retardant and heat-resistant properties without using halogen or diantimony trioxide; hence, the resin and its composition are favorable as encapsulating materials for semiconductor applications.
摘要翻译：本发明涉及下式的含氮环氧树脂：其中R相同或不同，各自表示氢原子或-R13-C6-10芳基 - （OR14）p，并且芳基任选被取代具有C 1-6烷基，其中R 13表示C 1-6亚烷基或任选被羟基取代的亚苯基-CH 2 - 基，R 14表示缩水甘油基，p表示1或2的整数，条件是在至少一个R基团不是氢原子; R 1表示苯基或-N（R）2基团，其中R如上定义。树脂是通过使三聚氰胺衍生物与醛，酚类化合物和表卤代醇顺序反应制备的。单独或作为环氧树脂组合物的一部分的含氮环氧树脂在不使用卤素或二氧化锑的情况下提供优异的阻燃和耐热性能; 因此，树脂及其组合物作为用于半导体应用的封装材料是有利的。

2. 发明授权

US06576690B1 Phosphorous-containing flame retarding epoxy resin and an epoxy resin composition containing the same 有权
标题翻译：含磷阻燃环氧树脂和含有这种阻燃环氧树脂的环氧树脂组合物
公开(公告)号：US06576690B1
公开(公告)日：2003-06-10
申请号：US10104567
申请日：2002-03-22
申请人： Kuen-Yuan Hwang , Hong-Hsing Chen , Chih-Fu Chen
发明人： Kuen-Yuan Hwang , Hong-Hsing Chen , Chih-Fu Chen
IPC分类号： C08K336
CPC分类号： C08G59/1422 , C08G59/4071 , H05K1/0326
摘要： The present invention relates to a phosphorous-containing flame retarding epoxy resin and their composition comprising the nitrogen-containing flame retarding epoxy resin. More specifically, the present invention relates to a flame retarding epoxy resin having a pendent phosphorous-containing functional group and their composition comprising the nitrogen-containing flame retarding epoxy resin. The flame retarding phosphorous-containing epoxy resin and the epoxy resin composition containing the same of the present invention possess excellent flame retarding property and heat resistance without containing halogen and diantimony trioxide. Therefore they are useful as an encapsulating material in the semiconductor industry and the cured article prepared from the composition exhibits excellent molding ability and excellent reliance.
摘要翻译：本发明涉及含磷阻燃环氧树脂及其组合物，其含有含氮阻燃环氧树脂。更具体地，本发明涉及具有含侧基的含磷官能团的阻燃性环氧树脂及其组合物，其包含含氮阻燃环氧树脂。含有阻燃性含磷环氧树脂和含有本发明的阻燃性含磷环氧树脂的环氧树脂组合物在不含卤素和三氧化二锑的情况下具有优异的阻燃性和耐热性。因此，它们可用作半导体工业中的封装材料，并且由该组合物制备的固化制品表现出优异的模塑能力和优异的依赖性。

3. 发明授权

US07507819B2 Method for preparing amino phosphate compounds 有权
标题翻译：制备氨基磷酸酯化合物的方法
公开(公告)号：US07507819B2
公开(公告)日：2009-03-24
申请号：US11269320
申请日：2005-11-07
申请人： Kuen-Yuan Hwang , An-Bang Duh , Chih-Fu Chen , Cheng-Jung Chiang
发明人： Kuen-Yuan Hwang , An-Bang Duh , Chih-Fu Chen , Cheng-Jung Chiang
IPC分类号： C07D251/54
CPC分类号： C07D251/56
摘要： The present invention relates to a method for preparing amino phosphate flame retardants. Melamine and phosphoric acid substances are used as a starting material, AND then the starting material reacts in the absence of solvents at a temperature ranging from 40 to 200° C. to obtain powdery amino phosphate compounds used as flame retardants. Since the reaction free of solvents is carried out under a condition of lower temperature, the powdery amino phosphate compounds can be obtained without drying steps. Therefore, not only the contaminations caused by solvent volatilization can be avoided, but also the process of preparing the product is simplified and the cost of the product is reduced.
摘要翻译：本发明涉及一种制备氨基磷酸酯阻燃剂的方法。使用三聚氰胺和磷酸物质作为原料，然后起始物质在不存在溶剂的情况下在40〜200℃的温度下反应，得到用作阻燃剂的粉末状氨基磷酸酯化合物。由于没有溶剂的反应在较低温度的条件下进行，所以可以在没有干燥步骤的情况下获得粉状氨基磷酸酯化合物。因此，不仅可以避免由溶剂挥发引起的污染，而且简化了产品的制备过程，降低了产品的成本。

4. 发明申请

US20080054234A1 Flame retardative resin composition 审中-公开
标题翻译：阻燃树脂组合物
公开(公告)号：US20080054234A1
公开(公告)日：2008-03-06
申请号：US11894890
申请日：2007-08-21
申请人： Kuen-Yuan Hwang , An-Pang Tu , Chih-Fu Chen , Gai-Chi Chen
发明人： Kuen-Yuan Hwang , An-Pang Tu , Chih-Fu Chen , Gai-Chi Chen
IPC分类号： C09K21/14
CPC分类号： C09K21/14 , C08G59/68 , C08L63/00 , C08L2666/16
摘要： A nonflammable resin composition comprises (A) at least an epoxy resin with biphenyl unit or naphthyl unit; (B) at least a phenolic resin used as a hardener, wherein the phenolic resin has a skeleton formed by phenyl rings bonding directly each other without interruption, and is in an amount of 30 to 100% by weight based on total hardeners; and (C) a curing catalyst. The said nonflammable resin has an excellent flame retardancy, a good heat resistance, and an improved moldability and reliability.
摘要翻译：不燃性树脂组合物包含（A）至少一种具有联苯单元或萘基单元的环氧树脂; （B）至少一种用作固化剂的酚醛树脂，其中所述酚醛树脂具有由不间断地直接键合的苯环形成的骨架，并且相对于总硬化剂为30〜100重量％和（C）固化催化剂。所述不燃性树脂具有优异的阻燃性，良好的耐热性，并提高了成型性和可靠性。

5. 发明申请

US20070049753A1 Method for preparing amino phosphate compounds 有权
标题翻译：制备氨基磷酸酯化合物的方法
公开(公告)号：US20070049753A1
公开(公告)日：2007-03-01
申请号：US11269320
申请日：2005-11-07
申请人： Kuen-Yuan Hwang , An-Bang Duh , Chih-Fu Chen , Cheng-Jung Chiang
发明人： Kuen-Yuan Hwang , An-Bang Duh , Chih-Fu Chen , Cheng-Jung Chiang
IPC分类号： C07D251/54
CPC分类号： C07D251/56
摘要： The present invention relates to a method for preparing amino phosphate flame retardants. Melamine and phosphoric acid substances are used as a starting material, AND then the starting material reacts in the absence of solvents at a temperature ranging from 40 to 200° C. to obtain powdery amino phosphate compounds used as flame retardants. Since the reaction free of solvents is carried out under a condition of lower temperature, the powdery amino phosphate compounds can be obtained without drying steps. Therefore, not only the contaminations caused by solvent volatilization can be avoided, but also the process of preparing the product is simplified and the cost of the product is reduced.
摘要翻译：本发明涉及一种制备氨基磷酸酯阻燃剂的方法。使用三聚氰胺和磷酸物质作为原料，然后起始物质在不存在溶剂的情况下在40〜200℃的温度下反应，得到用作阻燃剂的粉末状氨基磷酸酯化合物。由于没有溶剂的反应在较低温度的条件下进行，所以可以在没有干燥步骤的情况下获得粉状氨基磷酸酯化合物。因此，不仅可以避免由溶剂挥发引起的污染，而且简化了产品的制备过程，降低了产品的成本。

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