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1. 发明授权

US07977443B2 Copolymer rubber, rubber composition and rubber molded product 有权
标题翻译：共聚橡胶，橡胶组合物和橡胶成型品
公开(公告)号：US07977443B2
公开(公告)日：2011-07-12
申请号：US11990139
申请日：2006-08-09
申请人： Kotaro Ichino , Masao Kunizane , Takashi Hakuta
发明人： Kotaro Ichino , Masao Kunizane , Takashi Hakuta
IPC分类号： C08F236/20 , C08L19/00
CPC分类号： C08L23/16 , C08F210/18 , C08K3/04 , C08K3/22 , C08K3/26 , C08K5/09 , C08L71/00 , C08L2312/00 , C08L2666/22 , C08L2666/02 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/17
摘要： The invention provides a copolymer rubber excellent in processability in kneading and processability in extrusion; rubber compositions containing the rubber; and crosslinked moldings of the compositions excellent in sealing properties and shape retention. A random copolymer rubber of ethylene (A), a C3-20 α-olefin (B) and a nonconjugated polyene (C) which satisfies the following requirements (1) to (5): (1) the structural units (A) and (B) are contained at an (A)/(B) molar ratio of 40/60 to 95/5, (2) the structural unit (C) content is 0.01 to 5% by mole, (3) the limiting viscosity [η] is 1.0 to 5.0 dl/g as determined in decahydronaphthalene at 135°., (4) the Mw/Mn is 1 to 8, and (5) the P value is 0.46 to 1.00 as defined by formula (1): P=Ln(limiting viscosity [η])−5.0×105×η*(10) (1) (wherein Ln is a natural logarithm; and η*(10) is viscosity (Pa·sec) as determined at 190° C. and at 10 rad/sec.
摘要翻译：本发明提供一种挤出加工性优异的挤出加工性的共聚物橡胶，含有橡胶的橡胶组合物; 和密封性能和形状保持性优异的组合物的交联模塑品。（A），C3-20α-烯烃（B）和非共轭多烯（C）的无规共聚物橡胶，其满足以下要求（1）至（5）：（1）结构单元（A）和（A）/（B）摩尔比为40/60〜95/5，（2）结构单元（C）含量为0.01〜5摩尔％，（3）极限粘度[ （10）Mw / Mn为1〜8，（5）如式（1）所定义，P值为0.46〜1.00：（摩尔） P = Ln（特性粘度[eegr]） - 5.0×105×＆eegr *（10）（1）（其中Ln为自然对数;＆eegr; *（10）为粘度（Pa·sec） 190℃和10弧度/秒。

2. 发明申请

US20100144997A1 Copolymer Rubber, Rubber Composition and Rubber Molded Product 有权
标题翻译：共聚橡胶，橡胶组合物和橡胶成型产品
公开(公告)号：US20100144997A1
公开(公告)日：2010-06-10
申请号：US11990139
申请日：2006-08-09
申请人： Kotaro Ichino , Masao Kunizane , Takashi Hakuta
发明人： Kotaro Ichino , Masao Kunizane , Takashi Hakuta
IPC分类号： C08F236/20
CPC分类号： C08L23/16 , C08F210/18 , C08K3/04 , C08K3/22 , C08K3/26 , C08K5/09 , C08L71/00 , C08L2312/00 , C08L2666/22 , C08L2666/02 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/17
摘要： The invention provides a copolymer rubber excellent in processability in kneading and processability in extrusion; rubber compositions containing the rubber; and crosslinked moldings of the compositions excellent in sealing properties and shape retention. A random copolymer rubber of ethylene (A), a C3-20 α-olefin (B) and a nonconjugated polyene (C) which satisfies the following requirements (1) to (5): (1) the structural units (A) and (B) are contained at an (A)/(B) molar ratio of 40/60 to 95/5, (2) the structural unit (C) content is 0.01 to 5% by mole, (3) the limiting viscosity [η] is 1.0 to 5.0 dl/g as determined in decalin at 135° C., (4) the Mw/Mn is 1 to 8, and (5) the P value is 0.46 to 1.00 as defined by formula (1): P=Ln(limiting viscosity [η]−5.0×105×η*(10) (1) (wherein Ln is a natural logarithm; and η*(10) is a viscosity (Pa·sec) as determined at 190° C. and at 10 rad/sec).
摘要翻译：本发明提供一种挤出加工性优异的挤出加工性的共聚物橡胶，含有橡胶的橡胶组合物; 和密封性能和形状保持性优异的组合物的交联模塑品。（A），C3-20α-烯烃（B）和非共轭多烯（C）的无规共聚物橡胶，其满足以下要求（1）至（5）：（1）结构单元（A）和（A）/（B）摩尔比为40/60〜95/5，（2）结构单元（C）含量为0.01〜5摩尔％，（3）极限粘度[ 在135℃下在十氢化萘中测定为1.0〜5.0dl / g，（4）Mw / Mn为1〜8，（5）式（1）定义的P值为0.46〜1.00，：P = Ln（特性粘度[ - eegr]] - 5.0×105×＆eegr *（10）（1）（其中Ln为自然对数，＆eegr * *（10）为粘度（Pa·sec）在190℃和10弧度/秒）。

3. 发明申请

US20090209672A1 Copolymer rubber, rubber composition and rubber molding 审中-公开
标题翻译：共聚橡胶，橡胶组合物和橡胶成型
公开(公告)号：US20090209672A1
公开(公告)日：2009-08-20
申请号：US12314154
申请日：2008-12-04
申请人： Hiroki Ebata , Kotaro Ichino , Masao Kunizane
发明人： Hiroki Ebata , Kotaro Ichino , Masao Kunizane
IPC分类号： C08F136/20 , C08F210/18
CPC分类号： C08F210/18 , C08F4/65908 , C08F2420/02 , C08F4/6592 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/17
摘要： The present invention provides a copolymer rubber which contains only small amounts of impurities and is excellent in kneading processability, extrusion processability and retention of shape and a rubber composition containing the copolymer rubber, and further provides a rubber molded product which is obtained from the rubber composition, is excellent in surface appearance, strength properties, heat aging resistance and weathering resistance and has a low compression set. The copolymer rubber of the present invention comprises structural units derived from [A]ethylene, [B] an α-olefin of 3 to 20 carbon atoms, [C] a non-conjugated polyene having one double bond between adjacent carbon atoms in one molecule, said double bond being capable of polymerization by a metallocene catalyst, and [D] a non-conjugated polyene having two of the above double bonds in one molecule, and the copolymer rubber satisfies specific requirements (1) to (5).
摘要翻译：本发明提供一种仅含有少量杂质，捏合加工性，挤出加工性和保持性的共聚物橡胶和含有共聚物橡胶的橡胶组合物，并且还提供了由橡胶组合物获得的橡胶模制产品，表面外观，强度特性，耐热老化性，耐候性优异，压缩永久变形小。本发明的共聚物橡胶包含衍生自[A]乙烯，[B] 3-20个碳原子的α-烯烃的结构单元，[C]在一个分子中相邻碳原子之间具有一个双键的非共轭多烯所述双键能够通过金属茂催化剂聚合，和[D]在一个分子中具有两个上述双键的非共轭多烯，共聚物橡胶满足特定要求（1）至（5）。

4. 发明申请

US20080188621A1 Rubber Composition and Use Thereof 审中-公开
标题翻译：橡胶组合物及其用途
公开(公告)号：US20080188621A1
公开(公告)日：2008-08-07
申请号：US11587904
申请日：2005-04-28
申请人： Kotaro Ichino , Masao Kunizane , Yuji Ishit , Kunihide Hiraoka , Masaaki Kawasaki , Hidetatsu Murakami , Keiji Okada
发明人： Kotaro Ichino , Masao Kunizane , Yuji Ishit , Kunihide Hiraoka , Masaaki Kawasaki , Hidetatsu Murakami , Keiji Okada
IPC分类号： C08L9/02
CPC分类号： C08L21/00 , B60C1/0016 , C08L9/00 , C08L9/02 , C08L23/16 , C08L53/00 , C08L2666/02 , C08L2666/08
摘要： Provided is a rubber composition which can give a tire excellent in braking performance and fuel consumption and which is excellent in mechanical strength and fatigue resistance, and a use thereof.The rubber composition of the present invention contains a (A) 60 to 0.1 parts by weight of a nonconjugated polyene copolymer, which is a random copolymer containing 96 to 70 mol % of the structural units derived from α-olefin (A1) and 4 to 30 mol % of the structural units derived from a nonconjugated polyene (A2), and has a glass transition temperature (Tg) of −25 to 20° C., (B) 40 to 99.9 parts by weight of a diene rubber and (C) at least one selected from the group consisting of specific polymers.
摘要翻译：提供一种橡胶组合物，其能够赋予制动性能和燃料消耗优异并且机械强度和耐疲劳性优异的轮胎及其用途。本发明的橡胶组合物含有（A）60〜0.1重量份的非共轭多烯共聚物，其是含有96〜70摩尔％的来自α-烯烃（A1）的结构单元和4〜衍生自非共轭多烯（A2）的结构单元的30摩尔％，玻璃化转变温度（Tg）为-25〜20℃，（B）为40〜99.9重量份的二烯系橡胶，（C ）选自由特定聚合物组成的组中的至少一种。

5. 发明申请

US20070219320A1 Process for Producing Rubber Composition, Rubber Composition and use Thereof 审中-公开
标题翻译：生产橡胶组合物，橡胶组合物的方法及用途
公开(公告)号：US20070219320A1
公开(公告)日：2007-09-20
申请号：US11587756
申请日：2005-04-28
申请人： Kotaro Ichino , Masao Kunizane , Yuji Ishii , Kunihide Hiraoka , Masaaki Kawasaki , Hidetatsu Murakami , Keiji Okada
发明人： Kotaro Ichino , Masao Kunizane , Yuji Ishii , Kunihide Hiraoka , Masaaki Kawasaki , Hidetatsu Murakami , Keiji Okada
IPC分类号： C08F8/00
CPC分类号： C08L21/00 , B60C1/0016 , C08K5/0016 , C08L9/00 , C08L23/16 , C08L2666/06 , C08L2666/08
摘要： A process for producing a rubber composition containing a nonconjugated polyene copolymer (A), a softener (B) and a diene rubber (C), comprising: a step of mixing a copolymer composition (I), said copolymer composition (I) comprising 100 parts by weight of a nonconjugated polyene copolymer (A), said nonconjugated polyene copolymer (A) being a random copolymer containing 96 to 70 mol % of the structural units derived from α-olefin (A1) and 4 to 30 mol % of the structural units derived from nonconjugated polyene (A2) and having a glass transition temperature (Tg) of −25 to 20° C., and 1 to 100 parts by weight of the softener (B); the diene rubber (C); and optionally further the softener (B). A tire tread using the rubber composition and a tire having the tire tread.
摘要翻译：一种制备含有非共轭多烯共聚物（A），软化剂（B）和二烯橡胶（C）的橡胶组合物的方法，包括：将共聚物组合物（I），所述共聚物组合物（I）重量份的非共轭多烯共聚物（A），所述非共轭多烯共聚物（A）是含有96-70％（摩尔）衍生自α-烯烃（A1）的结构单元和4-30％（摩尔）结构衍生自非共轭多烯（A2）并且玻璃化转变温度（Tg）为-25至20℃的单元和1至100重量份的软化剂（B）; 二烯橡胶（C）; 和任选地进一步的软化剂（B）。使用橡胶组合物的轮胎胎面和具有轮胎胎面的轮胎。

6. 发明申请

US20110233448A1 COPOLYMER, RUBBER COMPOSITION, CROSS-LINKED RUBBER, CROSS-LINKED FOAM, AND USES THEREOF 有权
标题翻译：共聚物，橡胶组合物，交联橡胶，交联泡沫及其用途
公开(公告)号：US20110233448A1
公开(公告)日：2011-09-29
申请号：US13130746
申请日：2009-11-26
申请人： Hiroki Ebata , Akinori Takehara , Mitsunao Arino , Masao Kunizane , Yoshiharu Kikuchi , Takayuki Kajihara
发明人： Hiroki Ebata , Akinori Takehara , Mitsunao Arino , Masao Kunizane , Yoshiharu Kikuchi , Takayuki Kajihara
IPC分类号： C08F4/6592 , C08L9/00 , C08J9/00 , E04B1/74
CPC分类号： C08L23/16 , C08F4/65908 , C08F4/6592 , C08F210/18 , C08F232/08 , C08F2420/02 , C08J9/04 , C08J2201/026 , C08J2323/16 , C08L2203/14 , C08L2312/00 , C08L2314/06 , C08L2666/08 , C08F210/06 , C08F236/20
摘要： The present invention provides a rubber composition having adequate foamability, uses thereof, a copolymer contained in the rubber composition, a rubber composition capable of providing a cross-linked foam, which has a low specific gravity and an excellent shape-retaining property even when the usage of a nonconjugated polyene is reduced, and a cross-linked rubber and a cross-linked foam, which are produced from the rubber composition. A copolymer (A) according to the present invention is a copolymer including structural units derived from ethylene [A], an α-olefin [B], a nonconjugated polyene [C-1], in which one carbon-carbon double bond (C═C) polymerizable with a metallocene catalyst is present in one molecule, and a nonconjugated polyene [C-2], in which two bonds of C═C polymerizable with the metallocene catalyst are present in one molecule, and being synthesized with the metallocene catalyst, wherein (1) the units derived from the component [B] constitute 10 to 50 percent by mole, (2) the total of the units derived from the component [C-1] and the units derived from the component [C-2] is 1.0 to 6.0 percent by mole, (3) the molar ratio of the units derived from the component [C-1] to the units derived from the component [C-2] is 75/25 to 99.5/0.5, (4) [ML (1+4) 100° C.] is 10 to 200, and (5) 50>activation energy of fluidization (kJ/mol)>35 is satisfied.
摘要翻译：本发明提供一种橡胶组合物，其具有足够的发泡性，其用途，包含在橡胶组合物中的共聚物，能够提供交联泡沫的橡胶组合物，即使在降低了非共轭多烯的使用，以及由橡胶组合物制备的交联橡胶和交联泡沫。根据本发明的共聚物（A）是包含衍生自乙烯[A]，α-烯烃[B]，非共轭多烯[C-1]的结构单元的共聚物，其中一个碳 - 碳双键可用金属茂催化剂聚合的≡C）存在于一个分子中，并且在一分子中存在可与金属茂催化剂聚合的C = C的两个键的非共轭多烯[C-2]，并与茂金属催化剂合成其中（1）衍生自组分[B]的单元构成10至50摩尔％，（2）衍生自组分[C-1]的单元和衍生自组分[C-2 ]为1.0〜6.0摩尔％，（3）[C-1]成分的单元与来自成分[C-2]的单元的摩尔比为75/25〜99.5 / 0.5，（4））[ML（1 + 4）100℃]为10〜200，（5）50>流化活化能（kJ / mol）> 35。

7. 发明授权

US09193856B2 Copolymer, rubber composition, cross-linked rubber, cross-linked foam, and uses thereof 有权
标题翻译：共聚物，橡胶组合物，交联橡胶，交联泡沫及其用途
公开(公告)号：US09193856B2
公开(公告)日：2015-11-24
申请号：US13130746
申请日：2009-11-26
申请人： Hiroki Ebata , Akinori Takehara , Mitsunao Arino , Masao Kunizane , Yoshiharu Kikuchi , Takayuki Kajihara
发明人： Hiroki Ebata , Akinori Takehara , Mitsunao Arino , Masao Kunizane , Yoshiharu Kikuchi , Takayuki Kajihara
IPC分类号： C08F210/18 , C08F4/6592 , C08L23/16 , C08F232/08
CPC分类号： C08L23/16 , C08F4/65908 , C08F4/6592 , C08F210/18 , C08F232/08 , C08F2420/02 , C08J9/04 , C08J2201/026 , C08J2323/16 , C08L2203/14 , C08L2312/00 , C08L2314/06 , C08L2666/08 , C08F210/06 , C08F236/20
摘要： The present invention provides a rubber composition having adequate foamability, uses thereof, a copolymer contained in the rubber composition, a rubber composition capable of providing a cross-linked foam, which has a low specific gravity and an excellent shape-retaining property even when the usage of a nonconjugated polyene is reduced, and a cross-linked rubber and a cross-linked foam, which are produced from the rubber composition. A copolymer (A) according to the present invention is a copolymer including structural units derived from ethylene [A], an α-olefin [B], a nonconjugated polyene [C-1], in which one carbon-carbon double bond (C═C) polymerizable with a metallocene catalyst is present in one molecule, and a nonconjugated polyene [C-2], in which two bonds of C═C polymerizable with the metallocene catalyst are present in one molecule, and being synthesized with the metallocene catalyst, wherein (1) the units derived from the component [B] constitute 10 to 50 percent by mole, (2) the total of the units derived from the component [C-1] and the units derived from the component [C-2] is 1.0 to 6.0 percent by mole, (3) the molar ratio of the units derived from the component [C-1] to the units derived from the component [C-2] is 75/25 to 99.5/0.5, (4) [ML (1+4) 100° C.] is 10 to 200, and (5) 50>activation energy of fluidization (kJ/mol)>35 is satisfied.
摘要翻译：本发明提供一种橡胶组合物，其具有足够的发泡性，其用途，包含在橡胶组合物中的共聚物，能够提供交联泡沫的橡胶组合物，即使在降低了非共轭多烯的使用，以及由橡胶组合物制备的交联橡胶和交联泡沫。根据本发明的共聚物（A）是包含衍生自乙烯[A]，α-烯烃[B]，非共轭多烯[C-1]的结构单元的共聚物，其中一个碳 - 碳双键可用金属茂催化剂聚合的≡C）存在于一个分子中，并且在一分子中存在可与金属茂催化剂聚合的C = C的两个键的非共轭多烯[C-2]，并与茂金属催化剂合成其中（1）衍生自组分[B]的单元构成10至50摩尔％，（2）衍生自组分[C-1]的单元和衍生自组分[C-2 ]为1.0〜6.0摩尔％，（3）[C-1]成分的单元与来自成分[C-2]的单元的摩尔比为75/25〜99.5 / 0.5，（4））[ML（1 + 4）100℃]为10〜200，（5）50>流化活化能（kJ / mol）> 35。

8. 发明授权

US5962543A Foam processable rubber compositions and vulcanized rubber foam molded products of the same 失效
标题翻译：泡沫加工橡胶组合物和硫化橡胶发泡成型制品相同
公开(公告)号：US5962543A
公开(公告)日：1999-10-05
申请号：US971107
申请日：1997-11-14
申请人： Masaaki Kawasaki , Shuichi Nonaka , Masao Kunizane , Taku Koda , Tetsuo Tojo
发明人： Masaaki Kawasaki , Shuichi Nonaka , Masao Kunizane , Taku Koda , Tetsuo Tojo
IPC分类号： C08L23/16 , C08J9/00
CPC分类号： C08L23/16 , C08L2203/14 , C08L2312/00
摘要： Disclosed is a foam processable rubber composition which comprises an ethylene/.alpha.-olefin of 3 to 20 carbon atoms/non-conjugated polyene copolymer rubber (A), a crystalline polyolefin resin (B) having a melting point of 100 to 150.degree. C. and a foaming agent (C), in specific proportions. The copolymer rubber (A) has an ethylene/.alpha.-olefin molar ratio of 60/40 to 80/20, an intrinsic viscosity (.eta.), as measured in decalin at 135.degree. C., of 0.7 to 2 dl/g, and an iodine value of 10 to 50. A vulcanized rubber foam-molded product can be obtained by vulcanizing and foaming the rubber composition. The rubber composition can provide vulcanized rubber foam-molded products having excellent vulcanization properties such as weathering resistance, heat resistance, ozone resistance and tear strength. Besides, the rubber composition exhibits excellent precision moldability and productivity of vulcanized rubber foam-molded products in transfer molding, injection molding and cast molding.
摘要翻译：公开了一种可发泡加工的橡胶组合物，其包含3至20个碳原子的乙烯/α-烯烃/非共轭多烯共聚物橡胶（A），熔点为100-150℃的结晶聚烯烃树脂（B）和发泡剂（C）。共聚物橡胶（A）的乙烯/α-烯烃摩尔比为60/40至80/20，在135℃萘烷中测定的特性粘度（η）为0.7-2dl / g，和碘值为10〜50。通过硫化和发泡橡胶组合物可以获得硫化橡胶发泡成型产品。橡胶组合物可以提供具有优异的硫化性能如耐候性，耐热性，耐臭氧性和撕裂强度的硫化橡胶发泡成型产品。此外，橡胶组合物在传递成型，注射成型和铸造成型中表现出优异的成型性和硫化橡胶发泡成型体的生产率。

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