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1. 发明授权

US6120653A Separation and purification method of t-butyl-methylphenol isomer 失效
标题翻译：叔丁基甲基苯酚异构体的分离纯化方法
公开(公告)号：US6120653A
公开(公告)日：2000-09-19
申请号：US76806
申请日：1998-05-13
申请人： Kiyoshi Ikimi , Susumu Tsukada , Masaaki Toma
发明人： Kiyoshi Ikimi , Susumu Tsukada , Masaaki Toma
IPC分类号： C07C37/74 , C07C39/06 , B01D3/00 , C07C27/28
CPC分类号： C07C37/74 , C07C37/685
摘要： A method is provided for industrially advantageously and effectively separating 4M2B and 3M6B from a t-butylcresol mixture containing 2-t-butyl-4-methylphenol (4M2B), 2-tbutyl-5-methylphenol (3M6B), compounds having a lower boiling point than that of 4M2B and compounds having a higher boiling point than that of 3M6B derived from a m,p-cresol mixture.
摘要翻译：提供了一种工业上有利和有效地从含有2-叔丁基-4-甲基苯酚（4M2B），2-叔丁基-5-甲基苯酚（3M6B），具有较低沸点的化合物的叔丁基甲酚混合物中分离4M2B和3M6B的方法比具有比来自对甲酚混合物的3M6B沸点高的沸点的4M2B和化合物。

2. 发明授权

US5334774A Process for purifying phenol 失效
标题翻译：苯酚纯化方法
公开(公告)号：US5334774A
公开(公告)日：1994-08-02
申请号：US64982
申请日：1993-05-24
申请人： Kayoko Kogure , Kazuo Kimura , Michihiro Kawasaki , Masaaki Toma , Eiji Imamura
发明人： Kayoko Kogure , Kazuo Kimura , Michihiro Kawasaki , Masaaki Toma , Eiji Imamura
IPC分类号： C07B61/00 , C07C7/06 , C07C15/02 , C07C37/68 , C07C37/80 , C07C37/88 , C07C39/04 , C07C37/74
CPC分类号： C07C37/685 , C07C37/80 , C07C37/88 , Y02P20/582
摘要： A process for purifying and recovering phenol present in a mixed solution containing phenol and one or more compounds capable of forming azeotropic mixtures with phenol wherein an additive which is at least one compound belonging to the following groups 1 to 5 is added to the mixed solution and the resulting mixture is distilled:group 1: dialkylene glycols having 2-10 carbon atoms, polyalkylene glycols having 2-10 carbon atoms, and the ethers thereof,group 2: alkanediols having 2-20 carbon atoms,group 3: ethanolamine-type compounds represented by the formula (1) shown below,group 4: lactam compounds represented by the formula (2) shown below,group 5: quinoline, sulfolane, and N,N-dimethylimidazolidinone, ##STR1## wherein R.sub.1 represents an alkyl group having 1-6 carbon atoms, a cycloalkyl group having 1-6 carbon atoms, a monohydroxyalkyl group having 1-6 carbon atoms or a hydrogen atom, m represents an integer of 1-4, and X represents a hydroxyl group, an amino group or a hydrogen atom provided that R.sub.1 and X may conjointly represent a group which can be formed by removing respectively one hydrogen atom from R.sub.1 and X, respectively, and connecting the rests of R.sub.1 and X to form a cyclic ring, ##STR2## wherein R.sub.2 represents an alkyl group having 1-6 carbon atoms, a cycloalkyl group having 1-6 carbon atoms, a monohydroxyalkyl group having 1-6 carbon atoms, or a hydrogen atom, and n represents an integer of 3-7.
摘要翻译：一种纯化和回收苯酚存在于苯酚和一种或多种与苯酚形成共沸混合物的混合溶液中的苯酚的方法，其中将至少一种属于下列基团1至5的化合物的添加剂加入到混合溶液中，蒸馏得到的混合物：组1：具有2-10个碳原子的二亚烷基二醇，具有2-10个碳原子的聚亚烷基二醇及其醚，第2组：具有2-20个碳原子的烷二醇，第3组：乙醇胺型化合物由下式（1）表示的组4：由下式（2）表示的内酰胺化合物，组5：喹啉，环丁砜和N，N-二甲基咪唑烷酮，其中R1表示烷基具有1-6个碳原子的基团，具有1-6个碳原子的环烷基，具有1-6个碳原子的一羟基烷基或氢原子，m表示1-4的整数，X表示羟基，氨基组或水平条件是R1和X可以共同表示可以通过分别从R1和X分别除去一个氢原子并连接其余的R 1和X以形成环状而形成的基团，其中（2）其中 R2表示具有1-6个碳原子的烷基，具有1-6个碳原子的环烷基，具有1-6个碳原子的一羟基烷基或氢原子，n表示3-7的整数。

3. 发明申请

US20060113239A1 Device and method of classifying emulsion and method of demulsifying emulsion 审中-公开
标题翻译：分级乳液的装置和方法以及乳化乳化方法
公开(公告)号：US20060113239A1
公开(公告)日：2006-06-01
申请号：US10543662
申请日：2004-01-26
申请人： Yoshihito Okubo , Taisuke Maki , Masaaki Toma , Kazuhiro Mae
发明人： Yoshihito Okubo , Taisuke Maki , Masaaki Toma , Kazuhiro Mae
IPC分类号： B01D29/00 , B01D24/00
CPC分类号： B01D17/045
摘要： A classifying apparatus (1) has a flow path (structure) through which an emulsion flows. The flow path is provided between at least two plates (upper plate (2), lower plate (4)) that are separated by a distance smaller than the largest diameter of a liquid droplet included in the emulsion. Emulsion is fed from a supply port (5) provided in the upper plate (2) and can be classified by passing it in the flow path.
摘要翻译：分级装置（1）具有乳液流过的流路（结构）。流路设置在至少两个分隔开比乳液中包含的液滴的最大直径的距离的板（上板（2），下板（4））之间。乳液从设置在上板（2）中的供给口（5）供给，并且可以通过在流路中进行分类。

4. 发明授权

US5589077A Liquid filtering and supply system controlling recirculation responsive to pressure difference across filter 失效
标题翻译：液体过滤和供应系统根据过滤器上的压力差控制再循环
公开(公告)号：US5589077A
公开(公告)日：1996-12-31
申请号：US341919
申请日：1994-11-16
申请人： Yoji Matsuda , Masao Morikawa , Masaaki Toma
发明人： Yoji Matsuda , Masao Morikawa , Masaaki Toma
IPC分类号： B01D29/60 , B01D37/04 , B01J4/00
CPC分类号： B01D29/606 , Y10S134/902
摘要： A liquid filtering and supply system according to the present invention comprises, a main line to connect a liquid introducing part to a liquid supplying part, a filter disposed in said main line to filter said liquid, a first pressure detector disposed in said main line at an upstream side of said filter to detect a pressure of said liquid before said liquid is introduced to said filter, a second pressure detector disposed in said main line at a downstream side of said filter to detect a pressure of said liquid after said liquid passed out of said filter, a first circulating line for returning a liquid in said main line to the liquid introducing part, a pressure difference computing element to determine a pressure difference between the first pressure detector and said second pressure detector, a control valve disposed in the first circulating line, and a controlling part to adjust an opening of said control valve, based on a signal of the pressure difference transmitted from the pressure difference computing element.
摘要翻译：根据本发明的液体过滤和供给系统包括：将液体引入部分连接到液体供应部分的主线，设置在所述主线中以过滤所述液体的过滤器，设置在所述主管线中的第一压力检测器所述过滤器的上游侧在所述液体被引入所述过滤器之前检测所述液体的压力;第二压力检测器，其设置在所述主管线的所述过滤器的下游侧，以在所述液体流出之后检测所述液体的压力的第一循环管线，用于将所述主管线中的液体返回到液体引入部分;压差计算元件，用于确定第一压力检测器和所述第二压力检测器之间的压力差;控制阀，其设置在第一循环管路，以及控制部分，用于根据从压力传递的压差的信号调节所述控制阀的开度肯定的差异计算元素。

5. 发明授权

US5304684A Process for producing phenol and methyl ethyl ketone 失效
标题翻译：苯酚和甲基乙基酮的制备方法
公开(公告)号：US5304684A
公开(公告)日：1994-04-19
申请号：US86896
申请日：1993-07-07
申请人： Hiroshi Nishida , Kazuo Kimura , Shouji Hamada , Masaaki Toma , Hirooki Nagaoka
发明人： Hiroshi Nishida , Kazuo Kimura , Shouji Hamada , Masaaki Toma , Hirooki Nagaoka
IPC分类号： C07C39/04 , C07C45/53 , C07C409/04
CPC分类号： C07C409/04 , C07C39/04 , C07C407/00 , C07C407/003 , C07C45/53
摘要： sec-Butylbenzene hydroperoxide obtained by oxidizing sec-butylbenzene is decomposed into phenol and methyl ethyl ketone, a resulting liquid comprising a methyl ethyl ketone as the main component is washed with an aqueous alkali solution to remove carboxylic acids, carboxylic acid esters, unsaturated ketones, and aldehydes, and the washed liquid is further subjected to neutralization, dehydration, and distillation.A methyl ethyl ketone can be obtained which has a high quality with regard to purity and potassium permanganate fading.
摘要翻译：将通过氧化仲丁基苯获得的仲丁基氢过氧化物分解成苯酚和甲基乙基酮，以含有甲基乙基酮为主要成分的所得液体用碱水溶液洗涤以除去羧酸，羧酸酯，不饱和酮，和醛，并且洗涤的液体进一步进行中和，脱水和蒸馏。可以获得在纯度和高锰酸钾褪色方面具有高质量的甲基乙基酮。

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