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1. 发明授权

US06172127B2 Preparation of polyimide foam 失效
标题翻译：聚酰亚胺泡沫的制备
公开(公告)号：US06172127B2
公开(公告)日：2001-01-09
申请号：US09151735
申请日：1998-09-11
申请人： Kil Yeong Choi , Jae Heung Lee , Sung Goo Lee , Mi Hie Yi , Seung Su Kim
发明人： Kil Yeong Choi , Jae Heung Lee , Sung Goo Lee , Mi Hie Yi , Seung Su Kim
IPC分类号： C08J902
CPC分类号： C08J9/02 , C08G73/1021 , C08G73/1028 , C08J9/28 , C08J2379/08
摘要： The invention herein relates to a process of preparing a novel polyimide foam having superior heat-resistance, flame retardancy, homogeneous size and distribution of cells, and low density, wherein a polyimide precursor in a granular form is prepared by means of using heterocyclic amine as catalyst and then foaming. According to the present invention, the preparing process of a polyimide foam comprises reacting aromatic carboxylic acid or the anhydrides thereof with an excess of aliphatic univalent alcohol to yield an aromatic ester solution. To the aromatic ester solution, divalent amines or the mixture thereof were added in the equivalent amount of said carboxylic acid or the anhydrides thereof in addition to a catalyst and surfactant to yield a polyimide. Then, the precursor in a granular form mixture was imidized while foaming by means of pre-heating and then heating in a microwave oven, after which was cured at a high temperature. Consequently, the present invention has the effect of providing a preparing process for a polyimide foam with superior heat-resistance and heat-insulating property, which can be widely used as substrate in aerospace, submarine, special ship, and high-speed train.
摘要翻译：本发明涉及一种制备具有优异的耐热性，阻燃性，均匀尺寸和细胞分布以及低密度的新型聚酰亚胺泡沫的方法，其中通过使用杂环胺作为颗粒形式制备颗粒形式的聚酰亚胺前体催化剂，然后发泡。根据本发明，聚酰亚胺泡沫的制备方法包括使芳族羧酸或其酸酐与过量的脂肪族单价醇反应，得到芳族酯溶液。除了催化剂和表面活性剂之外，向芳族酯溶液中加入等量的所述羧酸或其酸酐的二价胺或其混合物以产生聚酰亚胺。然后，将颗粒状混合物中的前体通过预热加热发泡，然后在微波炉中加热，然后在高温下固化。因此，本发明具有提供制备方法具有优异的耐热性和隔热性的聚酰亚胺泡沫，可广泛用作航空航天，潜艇，专用船和高速列车的基板。

2. 发明授权

US08316689B2 Quantitative evaluation of scratch-induced damages on polymeric and coating materials 有权
标题翻译：对聚合物和涂层材料的划痕损伤的定量评估
公开(公告)号：US08316689B2
公开(公告)日：2012-11-27
申请号：US12845388
申请日：2010-07-28
申请人： Jong Il Weon , Si Yong Song , Jong Bae Lee , Kil Yeong Choi , Sung Goo Lee , Jae Heung Lee
发明人： Jong Il Weon , Si Yong Song , Jong Bae Lee , Kil Yeong Choi , Sung Goo Lee , Jae Heung Lee
IPC分类号： G01N3/56
CPC分类号： G01N3/46
摘要： Provided is a method for quantitative evaluation of mar- and scratch-induced surface damage on polymeric and coating materials. The method for quantitative evaluation of scratch-induced damage on polymeric and coating materials includes: preparing a test specimen of polymeric and coating materials; inducing a scratch damage on the surface of the test specimen; representing the scratch damage formed on the test specimen as corresponding color coordinates; and calculating a quantitated scratch damage index from a combination of a load applied to the surface of the test specimen and the color coordinates corresponding to the scratch damage.
摘要翻译：提供了一种用于定量评估聚合物和涂层材料上的划痕和划痕表面损伤的方法。用于定量评估聚合物和涂层材料上的划痕损伤的方法包括：制备聚合物和涂层材料的试样; 在试样的表面引起划痕损伤; 代表在试样上形成的划痕损伤作为相应的颜色坐标; 以及从施加到测试样本表面的负载和对应于划痕损伤的颜色坐标的组合计算定量的划痕损伤指数。

3. 发明授权

US06232432B1 Process for the preparation of polycarbonates 有权
标题翻译：聚碳酸酯的制备方法
公开(公告)号：US06232432B1
公开(公告)日：2001-05-15
申请号：US09605394
申请日：2000-06-29
申请人： Kil-Yeong Choi , Jae Heung Lee , Sung-Goo Lee , Sang Hyun Park , Young Chan Ko , Il Seok Choi , Kwang Soo Yoon
发明人： Kil-Yeong Choi , Jae Heung Lee , Sung-Goo Lee , Sang Hyun Park , Young Chan Ko , Il Seok Choi , Kwang Soo Yoon
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： The present invention relates to a process for the preparation of polycarbonates, more specifically to a process for the preparation of polycarbonates by a solid polymerization of prepolymers obtained by the polymerization between aromatic dihydroxides and diarylcarbonates, which comprises: a) preparing said prepolymer having a viscosity average molecular weight of 4,000-18,000 g/mole; b) preparing a microporous foam by injecting high-pressure inert gas; and c) preparing polycarbonates by a solid polymerization, which facilitates the removal of phenol, a by-product, and enhances molecular weight of polycarbonates without using any catalyst due to the relatively high polymerization rate.
摘要翻译：本发明涉及一种制备聚碳酸酯的方法，更具体地涉及通过芳香族二氢氧化物和二芳基碳酸酯之间的聚合得到的预聚物的固体聚合制备聚碳酸酯的方法，该方法包括：a）制备所述预聚物的粘度平均分子量为4,000-18,000g / mol; b）通过注入高压惰性气体制备微孔泡沫; 和c）通过固体聚合制备聚碳酸酯，其有助于除去苯酚，副产物，并且由于相对高的聚合速率而不使用任何催化剂，从而提高聚碳酸酯的分子量。

4. 发明授权

US06433184B1 Polyamide-imide having head-to-tail backbone 失效
标题翻译：具有头对头骨架的聚酰胺酰亚胺
公开(公告)号：US06433184B1
公开(公告)日：2002-08-13
申请号：US09605026
申请日：2000-06-28
申请人： Kil-Yeong Choi , Jae Heung Lee , Young-Taik Hong , Moon Young Jin , Kyoung-Su Choi , Ho-Jin Park
发明人： Kil-Yeong Choi , Jae Heung Lee , Young-Taik Hong , Moon Young Jin , Kyoung-Su Choi , Ho-Jin Park
IPC分类号： C07D20948
CPC分类号： C08G73/14
摘要： The present invention relates to polyamide-imides having head-to-tail backbone and more particularly, to polyamide-imimdes having head-to-tail ragularity to provide excellent heat and chemical resistance, physical and mechanical properties, processability, and gas permeability and selectivity. The polyamide-imides represented in the following formula (1) are obtained by direct polymerization, in the presence of dehydrating catalyst, of alone or as a mixture of 2 or above of monomers prepared by condensation of an amine compound having a nitro group with a carboxylic acid anhydride,
摘要翻译：本发明涉及具有头 - 尾主链的聚酰胺 - 酰亚胺，更具体地说，涉及具有头对尾的粗糙度以提供优异的耐热和耐化学性，物理和机械性能，可加工性和气体渗透性和选择性的聚酰胺酰亚胺。在下式（1）中表示的聚酰胺 - 酰亚胺通过在脱水催化剂的存在下，单独或作为2种以上的单体的混合物直接聚合而获得，所述单体通过具有硝基的胺化合物与羧酸酐，

5. 发明授权

US06423812B1 Process of preparing polycarbonates 有权
标题翻译：制备聚碳酸酯的方法
公开(公告)号：US06423812B1
公开(公告)日：2002-07-23
申请号：US09901727
申请日：2001-07-11
申请人： Young Chan Ko , Il Seok Choi , Cheol-Hyun Kim , Kwang Soo Yoon , Seung-Joo Kim , Kil-Yeong Choi , Jae Heung Lee , Kyong Soon Lee
发明人： Young Chan Ko , Il Seok Choi , Cheol-Hyun Kim , Kwang Soo Yoon , Seung-Joo Kim , Kil-Yeong Choi , Jae Heung Lee , Kyong Soon Lee
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： The present invention relates to a process of preparing polycarbonates and more particularly, to the process of preparing polycarbonates through a melt polymerization reaction of dihydroxyaryl compounds with diarylcarbonate, wherein said melt polymerization is performed in the presence of a mixed catalyst composed of an oxygen (O) or sulfur (S) containing compound having lone-pair electrons and an alkali metal or alkaline earth metal salt in an appropriate ratio at a reduced temperature by accelerating a reaction rate to obtain high quality polycarbonates with higher than 15,000 g/mole of a viscosity average molecular weight and improved color.
摘要翻译：本发明涉及一种制备聚碳酸酯的方法，更具体地说，涉及通过二羟基芳基化合物与碳酸二芳基酯的熔融聚合反应制备聚碳酸酯的方法，其中所述熔融聚合在由氧（O ）或含硫（S）的化合物，具有单对电子的碱金属或碱土金属盐，碱金属或碱土金属盐在降低的温度下通过加速反应速率以适当的比例获得高质量的聚碳酸酯，其粘度高于15,000g / 平均分子量和颜色改善。

6. 发明授权

US06525109B2 Process of preparing polycarbonates using microwave 有权
标题翻译：使用微波制备聚碳酸酯的工艺
公开(公告)号：US06525109B2
公开(公告)日：2003-02-25
申请号：US09903602
申请日：2001-07-13
申请人： Kil-Yeong Choi , Jae Heung Lee , Young Chan Ko , Il Seok Choi , Cheol-Hyun Kim , Kwang Soo Yoon , Kyong Soon Lee
发明人： Kil-Yeong Choi , Jae Heung Lee , Young Chan Ko , Il Seok Choi , Cheol-Hyun Kim , Kwang Soo Yoon , Kyong Soon Lee
IPC分类号： C08F246
CPC分类号： C08J3/28 , C08G64/307 , C08J2369/00
摘要： The present invention relates to a process of preparing polycarbonate, more specifically to a process of preparing polycarbonates by solid state polymerization using microwave radiation, which comprises steps of preparing polycarbonate prepolymer having a certain range of viscosity average molecular weight; converting said polycarbonate prepolymer into crystalline particles having a certain degree of crystallinity; and producing polycarbonates by solid state polymerization of said crystalline particles by applying microwave radiation, thus resulting in production of high quality polycarbonates with high molecular weight within short time.
摘要翻译：本发明涉及一种制备聚碳酸酯的方法，更具体地涉及使用微波辐射固相聚合制备聚碳酸酯的方法，其包括制备具有一定粘度平均分子量范围的聚碳酸酯预聚物的步骤; 将所述聚碳酸酯预聚物转化为具有一定结晶度的结晶颗粒; 并通过微波辐射使所述结晶颗粒的固态聚合制备聚碳酸酯，从而在短时间内生产高分子量的高质量聚碳酸酯。

7. 发明申请

US20130053530A1 METHOD FOR PREPARING A POLY(ETHER SULFONIMIDE OR -AMIDE) COPOLYMER USING CYCLIC OLIGOMERS 有权
标题翻译：使用环状低聚物制备聚（醚磺酰胺或酰胺）共聚物的方法
公开(公告)号：US20130053530A1
公开(公告)日：2013-02-28
申请号：US13641585
申请日：2010-10-07
申请人： Yong Seok Kim , Hyun Min Jung , Jong Chan Won , Jae Heung Lee
发明人： Yong Seok Kim , Hyun Min Jung , Jong Chan Won , Jae Heung Lee
IPC分类号： C08G75/30 , C08G69/00 , C07D273/00 , C08G69/40 , C08G69/42 , C07D327/00 , C08G75/23 , C08G73/10
CPC分类号： C07D273/00 , C07D323/00 , C07D327/00 , C08G75/30
摘要： Disclosed is a method for preparing a poly(ethersulfonimide or ethersulfonamide) copolymer using cyclic oligomers, and more particularly, to a method for preparing a poly(ethersulfonimide or ethersulfonamide) copolymer by preparing a cyclic ether sulfone oligomer and a cyclic imide or amide oligomer and subjecting the cyclic ether sulfone oligomer and the cyclic imide or amide oligomer to ring-opening copolymerization in the presence of an alkali metal fluoride catalyst.
摘要翻译：公开了使用环状低聚物制备聚（醚砜酰亚胺或醚磺酰胺）共聚物的方法，更具体地说，涉及通过制备环醚砜聚合物和环状酰亚胺或酰胺低聚物制备聚（醚磺酰亚胺或醚磺酰胺）共聚物的方法，在碱金属氟化物催化剂的存在下使环醚砜低聚物和环状酰亚胺或酰胺低聚物进行开环共聚。

8. 发明授权

US5962287A Process for producing erythritol using mutant Trichosporonoides 失效
标题翻译：使用突变型Trichosporonoides生产赤藓糖醇的方法
公开(公告)号：US5962287A
公开(公告)日：1999-10-05
申请号：US863573
申请日：1997-05-27
申请人： Seung Hyun Suh , Dae Chul Kim , Young Je Cho , Yeang Joong Jeon , Jae Heung Lee
发明人： Seung Hyun Suh , Dae Chul Kim , Young Je Cho , Yeang Joong Jeon , Jae Heung Lee
IPC分类号： C12N1/16 , C12P7/18 , C12R1/645
CPC分类号： C12R1/01 , C12P7/18
摘要： A novel Trichosporonoides madida CJ-NT1 microorganism which is capable of converting fermentable sugars to a high titre of erythritol under low aeration conditions and a method of producing erythritol by fermentation of sugar, which comprises culturing the cells of the Trichosporonoides madida CJ-NT1 strain are provided.
摘要翻译：在低通气条件下能够将发酵糖转化为高滴度赤藓糖醇的新型Trichosporonoides madida CJ-NT1微生物和通过发酵糖生产赤藓糖醇的方法，其包括培养Trichosporonoides madida CJ-NT1菌株的细胞是提供。

9. 发明授权

US08419918B2 Method of surface modification of polyimide film using ethyleneimines coupling agent, manufacturing method of flexible copper clad laminate and its product thereby 有权
标题翻译：使用乙烯亚胺偶联剂对聚酰亚胺膜进行表面改性的方法，由此形成柔性覆铜层压板及其制品的制造方法
公开(公告)号：US08419918B2
公开(公告)日：2013-04-16
申请号：US11920492
申请日：2006-05-18
申请人： Young-Taik Hong , Hyung Dae Kang , Seog Je Kim , Jae Heung Lee
发明人： Young-Taik Hong , Hyung Dae Kang , Seog Je Kim , Jae Heung Lee
IPC分类号： C25D5/56 , C25D5/34 , C23C28/02
CPC分类号： H05K3/389 , C08J7/12 , C08J7/18 , C08J2379/08 , C08L79/08 , H05K1/0346 , H05K3/381 , H05K3/388 , H05K2201/0154 , H05K2203/095 , Y10T428/12569
摘要： A method of surface modifying a polyimide film, a method of manufacturing a flexible copper clad laminate using the same, and a flexible copper clad laminate (FCCL) having a two-layer structure manufactured thereby. The method of surface modifying a polyimide film is conducted by modifying the surface of a polyimide film through a first plasma treatment, dipping the polyimide film into a solution containing an ethyleneimine-based silane coupling agent prepared by mixing the compound of Formula 1 and the compound of Formula 2 at a molar ratio of with 0.25˜1, and then modifying the surface of the polyimide film through a second plasma treatment. The method of surface modifying a polyimide film is advantageous because it may be substituted for a conventional surface treatment processes using ion beams. Also, the FCCL having a two-layer structure, formed by conducting copper sputtering and electroplating on the surface modified polyimide film, has good adhesive strength between the polyimide film and the copper foil and can maintain such adhesive strength even at high temperatures for a long period of time. Further, it may be usefully applied to electronic parts, such as flexible printed circuit boards, TCP (Tape Carrier Package), COF (Chip On Film), etc.
摘要翻译：对聚酰亚胺膜进行表面改性的方法，使用该方法的柔性覆铜层压板的制造方法以及由此制造的具有两层结构的柔性覆铜层压板（FCCL）。聚酰亚胺薄膜的表面改性方法是通过第一等离子体处理改性聚酰亚胺薄膜的表面，将聚酰亚胺薄膜浸入含有通过将式1化合物与化合物混合而制备的乙烯亚胺基硅烷偶联剂的溶液的摩尔比为0.25〜1，然后通过第二等离子体处理改性聚酰亚胺膜的表面。对聚酰亚胺膜进行表面改性的方法是有利的，因为它可以代替使用离子束的常规表面处理方法。此外，具有通过在表面改性聚酰亚胺膜上进行铜溅射和电镀形成的双层结构的FCCL具有在聚酰亚胺膜和铜箔之间的良好的粘合强度，并且即使在高温下也能够保持这种粘合强度长时间一段的时间。此外，它可以有用地应用于诸如柔性印刷电路板，TCP（胶带载体封装），COF（片上胶片）等电子部件。

10. 发明授权

US08808587B2 Preparation of microcapsule with double layered structure 有权
标题翻译：具有双层结构的微胶囊的制备
公开(公告)号：US08808587B2
公开(公告)日：2014-08-19
申请号：US12675700
申请日：2008-08-19
申请人： Hyun Min Jung , Yong Seok Kim , Jae Heung Lee , Jong Chan Won , Soon-Ryoung Hur
发明人： Hyun Min Jung , Yong Seok Kim , Jae Heung Lee , Jong Chan Won , Soon-Ryoung Hur
IPC分类号： B01J13/02 , B32B5/16
CPC分类号： B01J13/16 , B01J13/22 , Y10T428/254 , Y10T428/259 , Y10T428/2984 , Y10T428/2985
摘要： The present invention relates to a method of preparing a microcapsule with a double-layered structure which comprises the steps of performing an interfacial polymerization of an amine-aldehyde prepolymer on droplets containing an inorganic metal precursor selected from carboxylate and alkoxide compounds, and hydrolyzing the including inorganic precursors for formation of inorganic inner layer. The method of the present invention can prepare a microcapsule with a double-layered structure of an inorganic inner layer and a polymer outer layer, which is effective for eluting and substituting a core material inside the capsule.
摘要翻译：本发明涉及一种制备具有双层结构的微胶囊的方法，其包括以下步骤：在含有选自羧酸盐和烷氧基化合物的无机金属前体的液滴上进行胺 - 醛预聚物的界面聚合，并水解包含用于形成无机内层的无机前体。本发明的方法可以制备具有无机内层和聚合物外层的双层结构的微胶囊，其对于在胶囊内部的芯材进行洗脱和取代是有效的。

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