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    • 1. 发明申请
    • Process and apparatus for preparing metal or nonmetal phthalocyanine
    • 制备金属或非金属酞菁的方法和设备
    • US20070181416A1
    • 2007-08-09
    • US10556785
    • 2004-05-14
    • Ki JungJong KwonSeong ParkWoo Son
    • Ki JungJong KwonSeong ParkWoo Son
    • B01J19/12
    • C07D487/22B01J19/10B01J19/126B01J2219/00063B01J2219/089B01J2219/0892B01J2219/123B01J2219/1275
    • Disclosed herein is a process for preparing a metal or nonmetal phthalocyanine by using both microwave and ultrasonic wave energy in the presence of a solvent, or by using microwave energy in the absence of a solvent. Specifically, according to the process, anhydrous phthalic acid, phthalimide, 1,3-diiminoisoindoline, 1,2-dicyanobenzene, an halogen derivative thereof, an alkyl_derivative thereof or an alkoxy derivative thereof is mixed with a metal chloride or an alkoxy metal at 130250° C. for 0.2515 hours by using microwave at a frequency of 0.1-1000 Hz and a power of 100-3,000 W and ultrasonic wave at a frequency of 1-1,000 GHz and a power of 100-5,000 W in the presence of a solvent, or by using microwave at a frequency of 0.1-100 GHz and a power of 100-4,000 W in the absence of a solvent. Further disclosed is an apparatus for preparing a metal or nonmetal phthalocyanine in the absence or presence of solvent.
    • 本文公开了通过在溶剂存在下使用微波和超声波能量或在不存在溶剂的情况下使用微波能量来制备金属或非金属酞菁的方法。 具体地说,根据该方法,在130250下将无水邻苯二甲酸,邻苯二甲酰亚胺,1,3-二亚氨基异吲哚啉,1,2-二氰基苯,其卤素衍生物,其烷基衍生物或其烷氧基衍生物与金属氯化物或烷氧基金属混合 在溶剂存在下,使用频率为0.1〜1000Hz,功率为100〜300W的微波,频率为1-1000GHz,功率为100〜500W的超声波, ,或在不存在溶剂的情况下使用频率为0.1-100GHz的微波和功率为100-4,000W的微波。 还公开了在不存在或存在溶剂的情况下制备金属或非金属酞菁的装置。
    • 3. 发明申请
    • Method for preparing oxytitanium phthalocyanine chartge generating material and apparatus for preparing the same
    • 氧钛酞菁生成材料的制备方法及其制备方法
    • US20070122725A1
    • 2007-05-31
    • US10574797
    • 2004-10-07
    • Jong Ho KwonKi JungWoo SonSeong ParkJin KoHyun Jung
    • Jong Ho KwonKi JungWoo SonSeong ParkJin KoHyun Jung
    • C07D487/22H05B6/64
    • C09B67/0026C07D487/22G03G5/051G03G5/0525G03G5/0696H05B6/74
    • Disclosed herein are a method and an apparatus for preparing oxytitanium phthalocyanine as a charge generating material. The method comprises the steps of homogeneously mixing an oxytitanium phthalocyanine crude with an organic solvent while microwave energy having a frequency of 0.1˜100 GHz and a power of 10˜3,000 W and ultrasonic wave energy having a frequency of 1˜1,000 kHz and a power of 10˜5,000 W are applied thereto, and reacting the mixture at 30˜100° C. for 0.5˜5 hours. The apparatus comprises: a magnetron 1 capable of generating a frequency of 0.1˜100 GHz and a power of 100˜3,000 W; a mode stirrer 3 for making the wavelength of microwaves uniform in a microwave container 2; a PID type temperature controller 9 for accurately measurement and controlling the temperature of reactants; a K-type thermocouple shielded from microwaves 4; a condenser 5; an agitator 6, the thermocouple 4, the condenser 5 and the agitator 6 being inserted into three openings formed at a top of the microwave container 2; an ultrasonic tip 7 inserted into an opening formed at a bottom of the microwave container 2; a Pyrex container 9 into which the reactants are introduced; and a solvent tank 10. According to the method and the apparatus, an oxytitanium phthalocyanine charge generating material having superior thermal stability and crystal stability can be prepared in an efficient manner.
    • 本文公开了一种制备氧钛酞菁作为电荷产生材料的方法和装置。 该方法包括以下步骤:将氧钛酞菁粗品与有机溶剂均匀混合,同时具有频率为0.1〜100GHz,功率为10〜3000W的微波能量,频率为1〜1000kHz的超声波能量和功率 施加10〜5000W,使混合物在30〜100℃下反应0.5〜5小时。 该装置包括:能够产生0.1〜100GHz的频率和100〜3000W的功率的磁控管1; 用于使微波波长在微波容器2中均匀的模式搅拌器3; 用于精确测量和控制反应物温度的PID型温度控制器9; 与微波屏蔽的K型热电偶4; 冷凝器5; 搅拌器6,热电偶4,冷凝器5和搅拌器6插入形成在微波容器2的顶部的三个开口中; 插入到形成在微波容器2的底部的开口中的超声波尖端7; 其中引入反应物的Pyrex容器9; 和溶剂罐10。 根据该方法和装置,可以有效地制备具有优异热稳定性和晶体稳定性的氧钛酞菁电荷产生材料。
    • 7. 发明申请
    • Anisotropic conductive film forming composition
    • 各向异性导电膜形成组合物
    • US20060148956A1
    • 2006-07-06
    • US11273160
    • 2005-11-14
    • Ki JungJeong KangJung ChoiJong LeeHyoun KimTu Chang
    • Ki JungJeong KangJung ChoiJong LeeHyoun KimTu Chang
    • C08K3/08
    • C08K3/08H05K3/323
    • Disclosed herein is an anisotropic conductive film forming composition, including at least one polymer comprising a polymer containing a silane group; at least one polymerizable compound; and a plurality of conductive particles. The at least one polymer may include an elastomeric polymer and a filler polymer, at least one of which contains a silane group. The at least one polymerizable compound may include a cross-linking agent and/or a polymerization reaction enhancer. The cross-linking agent may also have a silane group. In addition, the film forming composition may include a solvent. The film forming composition is advantageous in that the resulting anisotropic conductive film exhibits enhanced peel and adhesive strength and low electrical contact resistance.
    • 本文公开了各向异性导电膜形成组合物,其包括至少一种包含含有硅烷基团的聚合物的聚合物; 至少一种可聚合化合物; 和多个导电粒子。 至少一种聚合物可以包括弹性体聚合物和填料聚合物,其中至少一种含有硅烷基团。 所述至少一种可聚合化合物可包括交联剂和/或聚合反应增强剂。 交联剂也可以具有硅烷基。 此外,成膜组合物可以包括溶剂。 成膜组合物的优点在于所得到的各向异性导电膜具有增强的剥离和粘合强度以及低的接触电阻。
    • 8. 发明申请
    • Fluid pump control system for excavators
    • 挖掘机流体泵控制系统
    • US20060147315A1
    • 2006-07-06
    • US11323508
    • 2005-12-29
    • Dal JangKi Jung
    • Dal JangKi Jung
    • F04B49/00
    • E02F9/2285E02F9/2232E02F9/2292E02F9/2296
    • A fluid pump control system for excavators enables fluid pumps to produce hydraulic flows of a quantity great enough to actuate hydraulic actuators for smooth composite operations. The system includes variable displacement fluid pumps, fluid quantity control mechanisms for controlling the discharge quantity of the respective fluid pumps, fluid quantity control signal lines respectively connected to the fluid quantity control mechanisms, signal pressure control lines for bringing the fluid quantity control signal lines into connection with a fluid tank to drop the fluid quantity control signal pressures within the fluid quantity control signal lines, and a plurality of cutoff valves attached to the signal pressure control lines in tandem and shiftable in concert with the shifting movement of spools of a control valve for increasing the fluid quantity control signal pressures within the signal pressure control lines in proportion to the shifting amounts of the cutoff valves.
    • 用于挖掘机的流体泵控制系统使得流体泵能够产生足够大的液压流量来致动液压致动器以实现平滑的复合操作。 该系统包括可变排量流体泵,用于控制各个流体泵的排出量的流体量控制机构,分别连接到流体量控制机构的流体量控制信号线,用于使流体量控制信号线进入的信号压力控制线 与流体箱连接以降低流体量控制信号线内的流体量控制信号压力,以及串联连接到信号压力控制线的多个截止阀,并且与控制阀的阀芯的移动运动相一致地移动 用于与所述截止阀的换档量成比例地增加所述信号压力控制线内的流体量控制信号压力。