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1. 发明申请

US20120040195A1 MODIFIED CARBOXYLATED POLYOLEFINS AND THEIR USE AS ADHESION PROMOTERS FOR POLYOLEFIN SURFACES 审中-公开
标题翻译：改性聚氧乙烯和它们作为粘合剂表面的粘合促进剂
公开(公告)号：US20120040195A1
公开(公告)日：2012-02-16
申请号：US13277504
申请日：2011-10-20
申请人： Kevin Alan Williams , Robert Lee Eagan , Lisa Kay Templeton , Richard Leon McConnell
发明人： Kevin Alan Williams , Robert Lee Eagan , Lisa Kay Templeton , Richard Leon McConnell
IPC分类号： B32B15/085 , C09D5/16 , B32B27/32 , C09D167/02
CPC分类号： C08J7/047 , C08F8/14 , C08F255/00 , C08F255/02 , C08F290/042 , C08F2800/10 , C08F2810/20 , C08J2423/00 , C09D7/65 , C09D151/06 , C09J151/06 , Y10T428/31692 , Y10T428/31938 , C08F222/06 , C08F255/04
摘要： The present invention provides solvent- and water-based primer compositions that include at least one carboxylated polyolefin that has been modified with one or more polyfunctional alcohols. The carboxylated polyolefins are obtained by the reaction of polyolefins with at least one of unsaturated carboxylic esters, unsaturated carboxylic acids, unsaturated carboxylic anhydrides, acrylic monomers, and mixtures thereof. The carboxylated polyolefins are then further modified by reaction with one or more polyfunctional alcohols. These polyfunctional alcohol-modified polyolefins may also contain pendant carboxyl groups, which have the propensity to form hydrophilic salts with amines or inorganic bases, thereby rendering the polyfunctional alcohol-modified polyolefins water-dispersible. These primer compositions are useful for significantly improving the adhesion of paints, adhesives, and inks to various plastic and metal substrates.
摘要翻译：本发明提供了溶剂和水基底漆组合物，其包括至少一种已被一种或多种多官能醇改性的羧化聚烯烃。羧基化的聚烯烃是通过聚烯烃与不饱和羧酸酯，不饱和羧酸，不饱和羧酸酐，丙烯酸类单体及其混合物中的至少一种的反应得到的。然后通过与一种或多种多官能醇反应来进一步修饰羧化聚烯烃。这些多官能醇改性聚烯烃也可以含有侧链羧基，其倾向于与胺或无机碱形成亲水盐，从而使多官能醇改性的聚烯烃水分散。这些底漆组合物可用于显着改善涂料，粘合剂和油墨对各种塑料和金属基材的粘合性。

2. 发明授权

US08058354B2 Modified carboxylated polyolefins and their use as adhesion promoters 有权
标题翻译：改性羧化聚烯烃及其作为粘合促进剂的用途
公开(公告)号：US08058354B2
公开(公告)日：2011-11-15
申请号：US10610238
申请日：2003-06-30
申请人： Kevin Alan Williams , Robert Lee Eagan , Lisa Kay Templeton , Richard Leon McConnell
发明人： Kevin Alan Williams , Robert Lee Eagan , Lisa Kay Templeton , Richard Leon McConnell
IPC分类号： C08F8/14 , C08F8/32 , C08F8/46 , C08C19/22 , C08C19/28 , C08C19/36
CPC分类号： C08J7/047 , C08F8/14 , C08F255/00 , C08F255/02 , C08F290/042 , C08F2800/10 , C08F2810/20 , C08J2423/00 , C09D7/65 , C09D151/06 , C09J151/06 , Y10T428/31692 , Y10T428/31938 , C08F222/06 , C08F255/04
摘要： The present invention provides solvent- and water-based primer compositions that include at least one carboxylated polyolefin that has been modified with one or more polyfunctional alcohols. The carboxylated polyolefins are obtained by the reaction of polyolefins with at least one of unsaturated carboxylic esters, unsaturated carboxylic acids, unsaturated carboxylic anhydrides, acrylic monomers, and mixtures thereof. The carboxylated polyolefins are then further modified by reaction with one or more polyfunctional alcohols. These polyfunctional alcohol-modified polyolefins may also contain pendant carboxyl groups, which have the propensity to form hydrophilic salts with amines or inorganic bases, thereby rendering the polyfunctional alcohol-modified polyolefins water-dispersible. These primer compositions are useful for significantly improving the adhesion of paints, adhesives, and inks to various plastic and metal substrates.
摘要翻译：本发明提供了溶剂和水基底漆组合物，其包括至少一种已被一种或多种多官能醇改性的羧化聚烯烃。羧基化的聚烯烃是通过聚烯烃与不饱和羧酸酯，不饱和羧酸，不饱和羧酸酐，丙烯酸类单体及其混合物中的至少一种的反应得到的。然后通过与一种或多种多官能醇反应来进一步修饰羧化聚烯烃。这些多官能醇改性聚烯烃也可以含有侧链羧基，其倾向于与胺或无机碱形成亲水盐，从而使多官能醇改性的聚烯烃水分散。这些底漆组合物可用于显着改善涂料，粘合剂和油墨对各种塑料和金属基材的粘合性。

3. 发明授权

US06262182B1 Solution modification of polyolefins 有权
标题翻译：聚烯烃的溶液改性
公开(公告)号：US06262182B1
公开(公告)日：2001-07-17
申请号：US09453892
申请日：2000-03-14
申请人： Robert Lee Eagan , Lisa Kay Templeton
发明人： Robert Lee Eagan , Lisa Kay Templeton
IPC分类号： C08F25500
CPC分类号： C08F255/02 , C08F255/04 , C08F222/06
摘要： The invention enables solution modification of a polyolefin with an unsaturated anhydride, unsaturated acid, or unsaturated ester, with high efficiency without the formation of undesirable impurities resulting from the competing reaction of the solvent with the unsaturated anhydride, unsaturated acid, or unsaturated ester. The process entails combining a polyolefin; a solvent; an unsaturated anhydride, unsaturated acid or unsaturated ester and a free-radical initiator to form a reaction mixture. The solvent is selected from the group consisting of substituted aromatic solvents which do not contain benzylic hydrogens and mixtures thereof. This reaction mixture is reacted under suitable conditions to produce a modified polyolefin.
摘要翻译：本发明可以高效率地使用不饱和酸酐，不饱和酸或不饱和酯进行聚烯烃的溶液改性，而不会由于溶剂与不饱和酸酐，不饱和酸或不饱和酯的竞争反应而产生不希望的杂质。该方法需要组合聚烯烃; 溶剂; 不饱和酸酐，不饱和酸或不饱和酯和自由基引发剂以形成反应混合物。溶剂选自不含苄基氢的取代芳族溶剂及其混合物。该反应混合物在合适的条件下反应生成改性聚烯烃。

4. 发明授权

US08058355B2 Modified chlorinated carboxylated polyolefins and their use as adhesion promoters 有权
标题翻译：改性氯化羧基聚烯烃及其用作粘合促进剂
公开(公告)号：US08058355B2
公开(公告)日：2011-11-15
申请号：US11218071
申请日：2005-08-31
申请人： Robert Lee Eagan , Kevin Alan Williams , Allen Morgan Cheek
发明人： Robert Lee Eagan , Kevin Alan Williams , Allen Morgan Cheek
IPC分类号： C08F8/20 , C08F8/14 , C09D151/06 , C09D123/28
CPC分类号： C09D175/04 , C08F8/44 , C08F2810/20 , C08K5/42 , C08L23/283 , C09D7/63 , C09D11/03 , C09D167/00 , C09D167/07 , C09D167/08 , Y10T428/31855 , C08L2666/06 , C08F8/22 , C08F285/00 , C08F8/14
摘要： The present invention provides solvent- and water-based primer compositions that include at least one chlorinated carboxylated polyolefin that has been modified with one or more polyfunctional alcohols. The chlorinated carboxylated polyolefins are obtained by the reaction of polyolefins with at least one of unsaturated carboxylic esters, unsaturated carboxylic acids, unsaturated carboxylic anhydrides, acrylic monomers, and mixtures thereof then chlorinated. The chlorinated carboxylated polyolefins are then further modified by reaction with one or more polyfunctional alcohols. These polyfunctional alcohol-modified chlorinated carboxylated polyolefins may also contain pendant carboxyl groups, which have the propensity to form hydrophilic salts with amines or inorganic bases, thereby rendering the polyfunctional alcohol-modified chlorinated carboxylated polyolefins water-dispersible. These primer compositions are useful for significantly improving the adhesion of paints, adhesives, and inks to various plastic and metal substrates.
摘要翻译：本发明提供溶剂和水基底漆组合物，其包括至少一种已经用一种或多种多官能醇改性的氯化羧化聚烯烃。通过聚烯烃与不饱和羧酸酯，不饱和羧酸，不饱和羧酸酐，丙烯酸类单体及其混合物中的至少一种的反应得到氯化羧基化的聚烯烃，然后氯化。然后通过与一种或多种多官能醇反应来进一步修饰氯化羧化聚烯烃。这些多官能醇改性的氯化羧基化聚烯烃也可以含有侧链羧基，其倾向于与胺或无机碱形成亲水盐，从而使多官能醇改性的氯化羧化聚烯烃水分散。这些底漆组合物可用于显着改善涂料，粘合剂和油墨对各种塑料和金属基材的粘合性。

5. 发明授权

US08809446B2 Substituted 3-oxopentanoates and their uses in coating compositions 有权
标题翻译：取代的3-氧代戊酸酯及其在涂料组合物中的用途
公开(公告)号：US08809446B2
公开(公告)日：2014-08-19
申请号：US12968780
申请日：2010-12-15
申请人： John Thorton Maddox , Robert Lee Eagan
发明人： John Thorton Maddox , Robert Lee Eagan
IPC分类号： C07C69/716 , C09D5/02 , C08F220/14 , C08F220/28
CPC分类号： C07C69/716 , C08F220/14 , C08F2220/282 , C08F2220/283 , C09D5/024 , C08F2220/1825 , C08F220/06
摘要： Substituted 3-oxopentanoates are disclosed that correspond to the following formula 1: in which R is hydrogen, or a methyl group; X is a straight-chain, branched, or cyclic alkyl or alkyl ether group having from 1 to 15 carbon atoms or aromatic group having from 6 to 15 carbon atoms; and Y1 and Y2 are independently hydrogen or an alkyl having 1 to 2 carbon atoms. Also disclosed are emulsion polymers, suspension polymers, and solution polymers that comprise residues from the substituted 3-oxopentanoate monomers, and that may also include one or more additional ethylenically unsaturated monomers. Also disclosed are coating compositions that include a latex emulsion polymer and the substituted 3-oxopentanoate monomer of formula 1 provided as a coalescent.
摘要翻译：公开了取代的3-氧代戊酸酯，其对应于下式1：其中R是氢或甲基; X是具有1至15个碳原子的直链，支链或环状烷基或烷基醚基或具有6至15个碳原子的芳族基团; 并且Y 1和Y 2独立地为氢或具有1至2个碳原子的烷基。还公开了包含来自取代的3-氧代戊酸酯单体的残基的乳液聚合物，悬浮聚合物和溶液聚合物，并且还可以包括一种或多种另外的烯属不饱和单体。还公开了包含胶乳乳液聚合物和作为聚结剂提供的式1的取代的3-氧代戊酸酯单体的涂料组合物。

6. 发明申请

US20120157609A1 SUBSTITUTED 3-OXOPENTANOATES AND THEIR USES IN COATING COMPOSITIONS 有权
标题翻译：取代的3-氧化戊酸酯及其在涂料组合物中的用途
公开(公告)号：US20120157609A1
公开(公告)日：2012-06-21
申请号：US12968780
申请日：2010-12-15
申请人： John Thorton Maddox , Robert Lee Eagan
发明人： John Thorton Maddox , Robert Lee Eagan
IPC分类号： C09D129/12 , C08F116/36 , C07C69/73
CPC分类号： C07C69/716 , C08F220/14 , C08F2220/282 , C08F2220/283 , C09D5/024 , C08F2220/1825 , C08F220/06
摘要： Substituted 3-oxopentanoates are disclosed that correspond to the following formula 1: in which R is hydrogen, or a methyl group; X is a straight-chain, branched, or cyclic alkyl or alkyl ether group having from 1 to 15 carbon atoms or aromatic group having from 6 to 15 carbon atoms; and Y1 and Y2 are independently hydrogen or an alkyl having 1 to 2 carbon atoms. Also disclosed are emulsion polymers, suspension polymers, and solution polymers that comprise residues from the substituted 3-oxopentanoate monomers, and that may also include one or more additional ethylenically unsaturated monomers. Also disclosed are coating compositions that include a latex emulsion polymer and the substituted 3-oxopentanoate monomer of formula 1 provided as a coalescent.
摘要翻译：公开了取代的3-氧代戊酸酯，其对应于下式1：其中R是氢或甲基; X是具有1至15个碳原子的直链，支链或环状烷基或烷基醚基或具有6至15个碳原子的芳族基团; 并且Y 1和Y 2独立地为氢或具有1至2个碳原子的烷基。还公开了包含来自取代的3-氧代戊酸酯单体的残基的乳液聚合物，悬浮聚合物和溶液聚合物，并且还可以包括一种或多种另外的烯属不饱和单体。还公开了包含胶乳乳液聚合物和作为聚结剂提供的式1的取代的3-氧代戊酸酯单体的涂料组合物。

7. 发明授权

US09029451B2 Waterborne coating compositions that include 2,2,4-trimethyl-3-oxopentanoate esters as reactive coalescents 有权
标题翻译：包括2,2,4-三甲基-3-氧代戊酸酯作为活性聚结剂的水性涂料组合物
公开(公告)号：US09029451B2
公开(公告)日：2015-05-12
申请号：US12968816
申请日：2010-12-15
申请人： John Thorton Maddox , Mark Dwight Clark , Robert Lee Eagan
发明人： John Thorton Maddox , Mark Dwight Clark , Robert Lee Eagan
IPC分类号： C08K5/10 , C09D7/06 , C09D5/02
CPC分类号： C09D7/06 , C09D5/024 , C09D7/47
摘要： Waterborne coating compositions are disclosed that include a latex emulsion polymer, and, as a reactive coalescent, a 2,2,4-trimethyl-3-oxopentanoate ester. The coating compositions of the invention have a reduced VOC content, and provide improved coalescing activity.
摘要翻译：公开了包含胶乳乳液聚合物和作为反应性聚结剂的2,2,4-三甲基-3-氧代戊酸酯的水性涂料组合物。本发明的涂料组合物具有降低的VOC含量，并提供改善的聚结活性。

8. 发明申请

US20120157614A1 WATERBORNE COATING COMPOSITIONS THAT INCLUDE 2,2,4-TRIMETHYL-3-OXOPENTANOATE ESTERS AS REACTIVE COALESCENTS 有权
标题翻译：包含2,2,4-三甲基-3-氧化戊酸酯的水性涂料组合物作为反应性煤
公开(公告)号：US20120157614A1
公开(公告)日：2012-06-21
申请号：US12968816
申请日：2010-12-15
申请人： John Thorton Maddox , Mark Dwight Clark , Robert Lee Eagan
发明人： John Thorton Maddox , Mark Dwight Clark , Robert Lee Eagan
IPC分类号： C08L25/14 , C08L25/16 , C08L33/12
CPC分类号： C09D7/06 , C09D5/024 , C09D7/47
摘要： Waterborne coating compositions are disclosed that include a latex emulsion polymer, and, as a reactive coalescent, a 2,2,4-trimethyl-3-oxopentanoate ester. The coating compositions of the invention have a reduced VOC content, and provide improved coalescing activity.
摘要翻译：公开了包含胶乳乳液聚合物和作为反应性聚结剂的2,2,4-三甲基-3-氧代戊酸酯的水性涂料组合物。本发明的涂料组合物具有降低的VOC含量，并提供改善的聚结活性。

9. 发明授权

US06527690B2 Purification of phenyl ester salts 失效
公开(公告)号：US06527690B2
公开(公告)日：2003-03-04
申请号：US09871695
申请日：2001-06-04
申请人： Bhaskar Krishna Arumugam , Michael Eugene Burns , Dimmick Lee Bymaster , Jeffrey Scott DuPont , Robert Richard Dykstra , Robert Lee Eagan , Eddie Joseph Eckart , Jarvey Eugene Felty, Jr. , Kevin John Fontenot , Jeffrey William Green , Shane Kipley Kirk , Gary Paul Lutz , Tony Lee Sander , Thomas Hugh Williams , George Chester Zima
发明人： Bhaskar Krishna Arumugam , Michael Eugene Burns , Dimmick Lee Bymaster , Jeffrey Scott DuPont , Robert Richard Dykstra , Robert Lee Eagan , Eddie Joseph Eckart , Jarvey Eugene Felty, Jr. , Kevin John Fontenot , Jeffrey William Green , Shane Kipley Kirk , Gary Paul Lutz , Tony Lee Sander , Thomas Hugh Williams , George Chester Zima
IPC分类号： C07C23100
CPC分类号： C07C303/44 , C07C309/42
摘要： The invention relates to a process for purifying and decolorizing a phenyl ester salt. The process combines a phenyl ester salt with a solvent to form a mixture and then stirs the mixture to form a slurry. The phenyl ester salt is substantially insoluble in this solvent. The process then collects the phenyl ester salt from the slurry. The collected phenyl ester salt may then be optionally dried or recrystallized. The collected phenyl ester salt is dissolved in a solvent to form a solution. The solution is decolorized and then spray dried to form a powder of the phenyl ester salt. As a result of the process the phenyl ester salt powder has a higher purity and an improved color as compared to the starting phenyl ester salt.

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