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1. 发明授权

US06747114B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US06747114B2
公开(公告)日：2004-06-08
申请号：US09745394
申请日：2000-12-21
申请人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Sudhin Datta , Charles Cozewith
发明人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Sudhin Datta , Charles Cozewith
IPC分类号： C08F21006
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 &agr;-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250° dg/min. at 230° C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250℃/分钟的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃下。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

2. 发明授权

US08383731B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US08383731B2
公开(公告)日：2013-02-26
申请号：US12391286
申请日：2009-02-24
申请人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
发明人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
IPC分类号： C08L23/16 , C08L23/30 , C08L23/14 , C09J123/14 , C09J123/16
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238 (B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRS) equal to and above 250 dg/min. at 230°C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了一种粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，该共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFRS）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

3. 发明授权

US07521507B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US07521507B2
公开(公告)日：2009-04-21
申请号：US10720512
申请日：2003-11-24
申请人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
发明人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
IPC分类号： C08F4/6192 , C08F4/6592 , C08F210/06 , C08L23/14
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250 dg/min. at 230° C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃下。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

4. 发明申请

US20090156729A1 Polypropylene-Based Adhesive Compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US20090156729A1
公开(公告)日：2009-06-18
申请号：US12391286
申请日：2009-02-24
申请人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J.F. Georjon
发明人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J.F. Georjon
IPC分类号： C09J123/00 , C09J123/10 , C08F255/02 , C08F10/14
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250 dg/min. at 230 NC. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230 NC。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

5. 发明授权

US06627723B2 Adhesive alpha-olefin inter-polymers 有权
标题翻译：粘合剂α-烯烃聚合物
公开(公告)号：US06627723B2
公开(公告)日：2003-09-30
申请号：US09746332
申请日：2000-12-21
申请人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
发明人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
IPC分类号： C08F21016
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： The invention relates to novel adhesive alpha-olefin inter-polymers which are largely amorphous and have a rheological behavior that makes them suitable for adhesive use, both without and with minimized amounts of tackifying resins. Specifically, the invention poly-alpha olefin inter-polymer may be composed of A) from 60 to 94 mol % of units derived from one alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); the diad distribution of component A in the polymer as determined by 13C NMR as described herein showing a ratio of experimentally determined diad distribution over the calculated Bernoullian diad distribution of less than 1.07; and the storage modulus G′ of said polymer, determined upon cooling as described herein, intersecting a value of 3.105 Pa at a temperature of less than 85° C. The invention also describes polymerization processes suitable for the manufacture of these adhesive alpha-olefin inter-polymers.
摘要翻译：本发明涉及新型粘合剂α-烯烃聚合物，它们大部分是无定形的并且具有使其适合于粘合剂使用的流变行为，两者都没有和最少量的增粘树脂。具体而言，本发明的聚α烯烃聚合物可以由A）60〜94摩尔％的来自1个具有3〜6个碳原子的α-单烯烃的单元组成，B）6〜40摩尔％的单元衍生自一种或多种其它具有4至10个碳原子和至少一个碳原子的单烯烃，比A）多; 和C）任选地0至10mol％衍生自不同于A）和B）的另一种可共聚不饱和烃的单元; 如本文所述，通过13 C NMR确定的聚合物中组分A的二元分布显示出计算的伯努利二元分布的实验测定的二单元分布的比例小于1.07; 并且在本文所述的冷却下测定的所述聚合物的储能模量G'在小于85℃的温度下与3.10 5 Pa的值相交。本发明还描述了适用于制造这些粘合剂α 烯烃聚合物。

6. 发明授权

US07067603B1 Adhesive alpha-olefin inter-polymers 有权
标题翻译：粘合剂α-烯烃聚合物
公开(公告)号：US07067603B1
公开(公告)日：2006-06-27
申请号：US10431547
申请日：2003-05-07
申请人： Anthony G. Karandinos , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington
发明人： Anthony G. Karandinos , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington
IPC分类号： C08F210/16 , C08F4/64
CPC分类号： C09J123/10 , C08F4/65912 , C08F10/00 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F4/65927 , C08F210/14 , C08F2500/03 , C08F2500/12 , C08F2500/17 , C08F210/16 , C08F210/08
摘要： The invention relates to novel adhesive alpha-olefin inter-polymers which are largely amorphous and have a rheological behavior that makes them suitable for adhesive use, both without and with minimzed amounts of tackifying resins. Specifically, the invention poly-alpha olefin inter-polymer may be composed of A) from 60 to 94% of units derived from one alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); the diad distribution of component A in the polymer as determined by 13C NMR as described herein showing a ratio of experimentally determined diad distribution over the calculated Bernoullian diad distribution of less than 1.07; and the storage modulus G′ of said polymer, determined upon cooling as described herein, intersecting a value of 3.105 Pa at a temperature of less than 85° C. The invention also describes polymerization processes suitable for the manufacture of these adhesive alpha-olefin inter-polymers.
摘要翻译：本发明涉及新型粘合剂α-烯烃聚合物，其主要是无定形的并且具有使其适合于粘合剂使用的流变行为，不含和最少量的增粘树脂。具体地说，本发明的聚α-烯烃聚合物可以由A）60-94％的衍生自一个具有3至6个碳原子的α-单烯烃的单元组成，B）6-40摩尔％衍生的单元来自一种或多种其它具有4至10个碳原子和至少一个碳原子的单烯烃，比A）多; 和C）任选地0至10mol％衍生自不同于A）和B）的另一种可共聚不饱和烃的单元; 通过本文所述的13 C NMR确定的聚合物中组分A的二元分布显示出计算的伯努利二元分布的实验测定的二单元分布的比率小于1.07; 并且在本文所述的冷却下测定的所述聚合物的储能模量G'在小于85℃的温度下与3.10Pa的值相交。本发明还描述了适合于制造这些粘合的α-烯烃聚合物。

7. 发明授权

US5750623A Hot-melt adhesives for disposable items and articles made therefrom 失效
标题翻译：用于一次性物品的热熔粘合剂和由其制成的制品
公开(公告)号：US5750623A
公开(公告)日：1998-05-12
申请号：US650734
申请日：1996-05-20
申请人： Charles F. Diehl , Jean M. Tancrede
发明人： Charles F. Diehl , Jean M. Tancrede
IPC分类号： C09J7/02 , A61L15/58 , C08F297/04 , C09J153/02 , C08L9/06 , C08L53/02
CPC分类号： C09J153/02 , A61L15/585 , C08F297/04
摘要： Hot-melt adhesive compositions containing high molecular weight linear styrene-isoprene-styrene block copolymers or high molecular weight linear styrene-butadiene-styrene copolymers, having little or no residual diblock, and articles made therefrom. The resulting adhesive composition may include solid tackifying and liquid tackifying resins.
摘要翻译：含有很少或没有残留二嵌段的高分子量线性苯乙烯 - 异戊二烯 - 苯乙烯嵌段共聚物或高分子量线性苯乙烯 - 丁二烯 - 苯乙烯共聚物的热熔粘合剂组合物及由其制成的制品。所得粘合剂组合物可以包括固体增粘和液体增粘树脂。

8. 发明授权

US5358783A Blends containing polystyrene-polyisoprene-polystyrene block copolymers and articles thereof 失效
标题翻译：含有聚苯乙烯 - 聚异戊二烯 - 聚苯乙烯嵌段共聚物的共混物及其制品
公开(公告)号：US5358783A
公开(公告)日：1994-10-25
申请号：US169165
申请日：1993-12-17
申请人： Charles F. Diehl , Jean M. Tancrede
发明人： Charles F. Diehl , Jean M. Tancrede
IPC分类号： A61L15/58 , B32B7/12 , C08F297/04 , C09J153/02 , C08L9/06 , C08L47/00 , C08L53/02
CPC分类号： A61L15/58 , B32B7/12 , C08F297/046 , C09J153/02 , Y10T428/2804 , Y10T428/2852 , Y10T428/31895 , Y10T428/31909
摘要： Blends of low styrene content polystyrene-polyisoprene-polystyrene block copolymer and high styrene content polystyrene-polyisoprene-polystyrene block copolymer can be used with tackifier resins, plasticizer oil and antioxidants to formulate pressure sensitive adhesives of improved cohesive strength vis-a-vis adhesives formed from the low styrene content polystyrene-polyisoprene-polystyrene block copolymer while maintaining good balance between tack, bonding characteristics and heat resistance.
摘要翻译：低苯乙烯含量的聚苯乙烯 - 聚异戊二烯 - 聚苯乙烯嵌段共聚物和高苯乙烯含量的聚苯乙烯 - 聚异戊二烯 - 聚苯乙烯嵌段共聚物的共混物可与增粘树脂，增塑剂油和抗氧化剂一起使用，以配制粘合强度更高的粘合强度的粘合剂来自低苯乙烯含量的聚苯乙烯 - 聚异戊二烯 - 聚苯乙烯嵌段共聚物，同时保持粘性，粘合特性和耐热性之间的良好平衡。

9. 发明授权

US08431642B2 Polyolefin adhesive compositions and articles made therefrom 有权
标题翻译：聚烯烃粘合剂组合物和由其制成的制品
公开(公告)号：US08431642B2
公开(公告)日：2013-04-30
申请号：US12472022
申请日：2009-05-26
申请人： Jean M. Tancrede , Christopher L. Curry , David R. Johnsrud , George Rodriguez , Fran A. Shipley
发明人： Jean M. Tancrede , Christopher L. Curry , David R. Johnsrud , George Rodriguez , Fran A. Shipley
IPC分类号： D21H19/18
CPC分类号： C09J123/10 , C08L23/06 , C08L2666/06
摘要： Provided are adhesive compositions composed of a polyolefin composition comprising at least about 50 wt. % polypropylene and at least one wax. The polymer compositions have a Dot T-Peel of about 1 Newton or more, a branching index (g′) of 0.95 or less measured at the Mz of the polymer, a molecular weight of 100,000 or less, and the adhesive compositions has a fast set time. The packaging industry desires adhesive compositions having a fast set time, such as those setting in less than five seconds from a molten state at conventional packaging operating temperatures to a solid or quasi solid having favorable Dot T-Peel, set time, and or fiber tear adhesion properties. Polymer based adhesives performing within this window are a favorable alternative to conventional formulated adhesives. The provided adhesive compositions exhibit a favorable balance of properties such as high adhesive strength, wide temperature operating window, and fast set time.
摘要翻译：提供了由聚烯烃组合物组成的粘合剂组合物，其包含至少约50wt。％聚丙烯和至少一种蜡。聚合物组合物具有约1牛顿或更多的点T皮，在聚合物的Mz下测量的支化指数（g'）为0.95或更小，分子量为100,000或更小，并且粘合剂组合物具有快速设置时间。包装工业希望具有快速固化时间的粘合剂组合物，例如在常规包装操作温度下从熔融状态设定在不到5秒钟的固态或准固体，具有有利的点T-Peel，凝固时间和/或纤维撕裂粘附性能。在该窗口内执行的基于聚合物的粘合剂是常规配制粘合剂的有利替代。所提供的粘合剂组合物表现出良好的性能平衡，例如高粘合强度，宽温度操作窗口和快速凝固时间。

10. 发明申请

US20090306281A1 Polyolefin Adhesive Compositions and Articles Made Therefrom 有权
标题翻译：聚烯烃粘合剂组合物及其制品
公开(公告)号：US20090306281A1
公开(公告)日：2009-12-10
申请号：US12472022
申请日：2009-05-26
申请人： Jean M. Tancrede , Christopher L. Curry , David R. Johnsrud , George Rodriguez , Fran A. Shipley
发明人： Jean M. Tancrede , Christopher L. Curry , David R. Johnsrud , George Rodriguez , Fran A. Shipley
IPC分类号： C08L23/12 , C08L23/06
CPC分类号： C09J123/10 , C08L23/06 , C08L2666/06
摘要： Provided are adhesive compositions composed of a polyolefin composition comprising at least about 50 wt. % polypropylene and at least one wax. The polymer compositions have a Dot T-Peel of about 1 Newton or more, a branching index (g′) of 0.95 or less measured at the Mz of the polymer, a molecular weight of 100,000 or less, and the adhesive compositions has a fast set time. The packaging industry desires adhesive compositions having a fast set time, such as those setting in less than five seconds from a molten state at conventional packaging operating temperatures to a solid or quasi solid having favorable Dot T-Peel, set time, and or fiber tear adhesion properties. Polymer based adhesives performing within this window are a favorable alternative to conventional formulated adhesives. The provided adhesive compositions exhibit a favorable balance of properties such as high adhesive strength, wide temperature operating window, and fast set time.
摘要翻译：提供了由聚烯烃组合物组成的粘合剂组合物，其包含至少约50wt。％聚丙烯和至少一种蜡。聚合物组合物具有约1牛顿或更多的点T皮，在聚合物的Mz下测量的支化指数（g'）为0.95或更小，分子量为100,000或更小，并且粘合剂组合物具有快速设置时间。包装工业希望具有快速固化时间的粘合剂组合物，例如在常规包装操作温度下从熔融状态设定在不到5秒钟的固态或准固体，具有有利的点T-Peel，凝固时间和/或纤维撕裂粘附性能。在该窗口内执行的基于聚合物的粘合剂是常规配制粘合剂的有利替代。所提供的粘合剂组合物表现出良好的性能平衡，例如高粘合强度，宽温度操作窗口和快速凝固时间。

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