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1. 发明授权

US06747114B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US06747114B2
公开(公告)日：2004-06-08
申请号：US09745394
申请日：2000-12-21
申请人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Sudhin Datta , Charles Cozewith
发明人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Sudhin Datta , Charles Cozewith
IPC分类号： C08F21006
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 &agr;-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250° dg/min. at 230° C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250℃/分钟的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃下。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

2. 发明授权

US08383731B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US08383731B2
公开(公告)日：2013-02-26
申请号：US12391286
申请日：2009-02-24
申请人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
发明人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
IPC分类号： C08L23/16 , C08L23/30 , C08L23/14 , C09J123/14 , C09J123/16
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238 (B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRS) equal to and above 250 dg/min. at 230°C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了一种粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，该共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFRS）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

3. 发明授权

US07521507B2 Polypropylene-based adhesive compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US07521507B2
公开(公告)日：2009-04-21
申请号：US10720512
申请日：2003-11-24
申请人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
发明人： Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J. F. Georjon , Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede
IPC分类号： C08F4/6192 , C08F4/6592 , C08F210/06 , C08L23/14
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250 dg/min. at 230° C. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230℃下。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

4. 发明申请

US20090156729A1 Polypropylene-Based Adhesive Compositions 有权
标题翻译：聚丙烯基粘合剂组合物
公开(公告)号：US20090156729A1
公开(公告)日：2009-06-18
申请号：US12391286
申请日：2009-02-24
申请人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J.F. Georjon
发明人： Anthony G. Karandinos , Keith A. Nelson , Jean M. Tancrede , Kenneth Lewtas , Sudhin Datta , Charles Cozewith , Bruce A. Harrington , David J. Lohse , Olivier J.F. Georjon
IPC分类号： C09J123/00 , C09J123/10 , C08F255/02 , C08F10/14
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： An adhesive blend is described that can include a semi-crystalline copolymer of propylene and at least one comonomer selected from the group consisting of ethylene and at least one C4 to C20 α-olefin, the copolymer having a weight average molecular weight (Mw) from about 15,000 to about 200,000; an melt index (MI) from about 7 dg/min to about 3000 dg/min as measured by ASTM D 1238(B), and a (Mw/Mn) of approximately 2. Various production processes are also described. Also described are adhesive compositions and methods for making adhesive compositions having polymers or polymer blends with melt flow rates (MFRs) equal to and above 250 dg/min. at 230 NC. Certain specific embodiments of the invention involve the use of a free radical initiator, e.g., a peroxide.
摘要翻译：描述了粘合剂共混物，其可以包括丙烯和至少一种选自乙烯和至少一种C 4 -C 20α-烯烃的共聚单体的半结晶共聚物，所述共聚物的重均分子量（Mw）约15,000至约20万; 通过ASTM D 1238（B）测量的约7dg / min至约3000dg / min的熔体指数（MI）和约2的（Mw / Mn）。还描述了各种制备方法。还描述了粘合剂组合物和制备具有熔体流动速率（MFR）等于或高于250dg / min的聚合物或聚合物共混物的粘合剂组合物的方法。在230 NC。本发明的某些具体实施方案涉及使用自由基引发剂，例如过氧化物。

5. 发明授权

US06627723B2 Adhesive alpha-olefin inter-polymers 有权
标题翻译：粘合剂α-烯烃聚合物
公开(公告)号：US06627723B2
公开(公告)日：2003-09-30
申请号：US09746332
申请日：2000-12-21
申请人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
发明人： Anthony G. Karandinos , David J. Lohse , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington , Olivier J. F. Georjon , Kenneth Lewtas
IPC分类号： C08F21016
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/14 , C08F2500/17 , C08F210/16 , C08F2500/12 , C08F2500/03
摘要： The invention relates to novel adhesive alpha-olefin inter-polymers which are largely amorphous and have a rheological behavior that makes them suitable for adhesive use, both without and with minimized amounts of tackifying resins. Specifically, the invention poly-alpha olefin inter-polymer may be composed of A) from 60 to 94 mol % of units derived from one alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); the diad distribution of component A in the polymer as determined by 13C NMR as described herein showing a ratio of experimentally determined diad distribution over the calculated Bernoullian diad distribution of less than 1.07; and the storage modulus G′ of said polymer, determined upon cooling as described herein, intersecting a value of 3.105 Pa at a temperature of less than 85° C. The invention also describes polymerization processes suitable for the manufacture of these adhesive alpha-olefin inter-polymers.
摘要翻译：本发明涉及新型粘合剂α-烯烃聚合物，它们大部分是无定形的并且具有使其适合于粘合剂使用的流变行为，两者都没有和最少量的增粘树脂。具体而言，本发明的聚α烯烃聚合物可以由A）60〜94摩尔％的来自1个具有3〜6个碳原子的α-单烯烃的单元组成，B）6〜40摩尔％的单元衍生自一种或多种其它具有4至10个碳原子和至少一个碳原子的单烯烃，比A）多; 和C）任选地0至10mol％衍生自不同于A）和B）的另一种可共聚不饱和烃的单元; 如本文所述，通过13 C NMR确定的聚合物中组分A的二元分布显示出计算的伯努利二元分布的实验测定的二单元分布的比例小于1.07; 并且在本文所述的冷却下测定的所述聚合物的储能模量G'在小于85℃的温度下与3.10 5 Pa的值相交。本发明还描述了适用于制造这些粘合剂α 烯烃聚合物。

6. 发明授权

US07067603B1 Adhesive alpha-olefin inter-polymers 有权
标题翻译：粘合剂α-烯烃聚合物
公开(公告)号：US07067603B1
公开(公告)日：2006-06-27
申请号：US10431547
申请日：2003-05-07
申请人： Anthony G. Karandinos , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington
发明人： Anthony G. Karandinos , David J. Lohse , Olivier J. F. Georjon , Kenneth Lewtas , Keith A. Nelson , Jean M. Tancrede , Bruce Allan Harrington
IPC分类号： C08F210/16 , C08F4/64
CPC分类号： C09J123/10 , C08F4/65912 , C08F10/00 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F4/65927 , C08F210/14 , C08F2500/03 , C08F2500/12 , C08F2500/17 , C08F210/16 , C08F210/08
摘要： The invention relates to novel adhesive alpha-olefin inter-polymers which are largely amorphous and have a rheological behavior that makes them suitable for adhesive use, both without and with minimzed amounts of tackifying resins. Specifically, the invention poly-alpha olefin inter-polymer may be composed of A) from 60 to 94% of units derived from one alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); the diad distribution of component A in the polymer as determined by 13C NMR as described herein showing a ratio of experimentally determined diad distribution over the calculated Bernoullian diad distribution of less than 1.07; and the storage modulus G′ of said polymer, determined upon cooling as described herein, intersecting a value of 3.105 Pa at a temperature of less than 85° C. The invention also describes polymerization processes suitable for the manufacture of these adhesive alpha-olefin inter-polymers.
摘要翻译：本发明涉及新型粘合剂α-烯烃聚合物，其主要是无定形的并且具有使其适合于粘合剂使用的流变行为，不含和最少量的增粘树脂。具体地说，本发明的聚α-烯烃聚合物可以由A）60-94％的衍生自一个具有3至6个碳原子的α-单烯烃的单元组成，B）6-40摩尔％衍生的单元来自一种或多种其它具有4至10个碳原子和至少一个碳原子的单烯烃，比A）多; 和C）任选地0至10mol％衍生自不同于A）和B）的另一种可共聚不饱和烃的单元; 通过本文所述的13 C NMR确定的聚合物中组分A的二元分布显示出计算的伯努利二元分布的实验测定的二单元分布的比率小于1.07; 并且在本文所述的冷却下测定的所述聚合物的储能模量G'在小于85℃的温度下与3.10Pa的值相交。本发明还描述了适合于制造这些粘合的α-烯烃聚合物。

7. 发明授权

US06582762B2 Sprayable hot melt adhesives 有权
标题翻译：可喷涂热熔胶
公开(公告)号：US06582762B2
公开(公告)日：2003-06-24
申请号：US09839316
申请日：2001-04-20
申请人： Michel L. Faissat , Charles L. Sims , Olivier J. Georjon , Anthony G. Karandinos
发明人： Michel L. Faissat , Charles L. Sims , Olivier J. Georjon , Anthony G. Karandinos
IPC分类号： B05D510
CPC分类号： C09J123/10 , C08F210/06 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09J123/14 , C08F210/16 , C08F2500/12 , C08F2500/03 , C08F2500/17 , C08F210/14
摘要： This invention relates to a process for atomizing, spiral spraying, oscillation spraying or melt blowing propylene copolymers onto a substrate comprising selecting a poly-alpha olefin inter-polymer comprising: A) from 60 to 94% of units derived from an alpha mono-olefin having from 3 to 6 carbon atoms and B) from 6 to 40 mol % of units derived from ethylene or one or more other mono-olefins having from 4 to 10 carbon atoms and at least one carbon atom more than A); and C) optionally from 0 to 10 mol % of units derived from another copolymerizable unsaturated hydrocarbon, different from A) and B); wherein the inter-polymer has: i) an Mw/Mn of 6 or less; ii) a storage modulus G′, determined upon cooling, intersecting a value of 0.3 M Pa at a temperature of less than 85° C.; iii) a G″/G′ ratio of 18 or more when G′ is 10 Pa when measured at a frequency of 1 hz; and iv) a viscosity of 5000 mPa·sec or less at 190° C., and atomizing, spiral spraying, oscillation spraying or melt blowing the inter-polymer into a substrate. Blends of the above copolymers can also be used herein.
摘要翻译：本发明涉及一种在基材上雾化，螺旋喷涂，振荡喷涂或熔融丙烯共聚物的方法，包括选择聚α-烯烃聚合物，其包含：A）60至94％的衍生自α-单烯烃的单元具有3至6个碳原子和B）6至40摩尔％的衍生自乙烯或一种或多种其它具有4至10个碳原子和至少1个碳原子的其它单烯烃的单元; 和C）任选地0至10摩尔％来自不同于A）和B）的另一种可共聚不饱和烃的单元;其中所述共聚物具有：i）Mw / Mn为6以下; ii）储能模量G '，在低于85℃的温度下与0.3Mpa的值相交; iii）当G'为10Pa时，G“/ G'比为18或更大，当以 1 hz; andiv）在190℃下的粘度为5000mPa.sec或更低，并进行溶解，螺旋喷涂，振荡喷雾或将共聚物熔融吹制到基底中。上述共聚物的延伸部分也可用于本文。

8. 发明授权

US08435622B2 Packaging film 有权
标题翻译：包装膜
公开(公告)号：US08435622B2
公开(公告)日：2013-05-07
申请号：US12083999
申请日：2006-01-13
申请人： Georgios Papadopoulos , Anthony G. Karandinos , Damianos Markakis , Emmanouil Grevetzakis , Sofia Parouti
发明人： Georgios Papadopoulos , Anthony G. Karandinos , Damianos Markakis , Emmanouil Grevetzakis , Sofia Parouti
IPC分类号： B32B3/04 , B32B3/10
CPC分类号： B65D65/38 , B65D75/006 , Y10T428/2419 , Y10T428/24273 , Y10T428/24298 , Y10T428/24322 , Y10T428/24479 , Y10T428/24777 , Y10T428/31855
摘要： A packaging film with a main film made of a stretchable polymer film material and having a multiplicity of holes. A first condition of the main film including that a ratio of aeration percentage over final weight is greater than or equal to 14 meters per gram. A second condition of the main film is that the width of the packaging film is reducible by less than 15% between a condition before any stretching of the packaging film and a condition when the packaging film is stretched at an elongation equal to the elongation at the NDR point. A third condition of the main film is that a ratio of an absolute value of the difference of a holding force of the packaging film minus a predetermined target holding force divided by the target holding force is less than or equal to 5%.
摘要翻译：一种具有由可拉伸聚合物膜材料制成的并具有多个孔的主膜的包装膜。主膜的第一条件包括通气百分比与最终重量的比值大于或等于14克/克。主膜的第二个条件是，在包装膜的任何拉伸之前的条件和包装膜在伸长率等于拉伸时的条件下，包装膜的宽度可以减小小于15％ NDR点。主膜的第三条件是包装膜的保持力的差异的绝对值与预定的目标夹持力除以目标保持力之间的比率小于或等于5％。

9. 发明授权

US08053055B2 Stretch film 失效
标题翻译：拉伸膜
公开(公告)号：US08053055B2
公开(公告)日：2011-11-08
申请号：US11630226
申请日：2004-07-16
申请人： Georgios Papadopoulos , Damianos Markakis , Anthony G. Karandinos
发明人： Georgios Papadopoulos , Damianos Markakis , Anthony G. Karandinos
IPC分类号： B32B3/24
CPC分类号： B65D75/006 , B65D71/0088 , Y10T428/24273 , Y10T428/24322 , Y10T428/24331
摘要： A stretch film comprising a base film made of a stretchable plastic film material, a multiplicity of holes in the base film arranged in several columns along a main direction, at least one reinforcement strip made of a stretchable plastic film material. The reinforcement strip is arranged and fixed on the base film in an area between two adjacent columns of holes. The thickness of the base film is greater than or equal to the thickness of the reinforcement strip and the width (w) of the reinforcement strip is as great as possible, but is such that the reinforcement strip does not contact or overlap the holes in the adjacent columns of holes. The reinforcement strip may be fixed to the base film so as to be inseparable and indistinguishable from the base film.
摘要翻译：一种拉伸膜，包括由可拉伸塑料膜材料制成的基膜，沿着主方向布置成多列的基膜中的多个孔，至少一个由伸缩塑料膜材料制成的加强条。加强条在两个相邻的孔之间的区域中布置并固定在基膜上。基膜的厚度大于或等于加强条的厚度，并且加强条的宽度（w）尽可能大，但是这样使得加强条不接触或重叠在相邻列的孔。加强条可以固定到基膜，以便与基膜不可分离和不可区分。

10. 发明申请

US20120270003A1 Polyolefin Pre-Stretched Packaging Film 有权
标题翻译：聚烯烃预拉伸包装膜
公开(公告)号：US20120270003A1
公开(公告)日：2012-10-25
申请号：US13393885
申请日：2010-09-03
申请人： Michalis Apostolakis , Konstantinos G. Gatos , Anthony G. Karandinos
发明人： Michalis Apostolakis , Konstantinos G. Gatos , Anthony G. Karandinos
IPC分类号： B32B3/24 , B26D7/14 , B32B27/32
CPC分类号： B32B27/32 , B32B3/266 , B32B27/08 , B32B2250/24 , B32B2270/00 , B32B2307/50 , B32B2307/514 , B32B2307/5825 , B32B2307/718 , B32B2307/72 , B32B2553/00 , Y10T83/0424 , Y10T428/15
摘要： The invention provides a polyolefin pre-stretched packaging film comprising perforations arranged in a series of columns along a longitudinal direction of the film, wherein each adjacent column of said perforations is separated by a column without perforations along the longitudinal direction, and the perforations are staggered in a transverse direction across the film, wherein said film comprises an inherent cling surface on at least one of its surfaces; wherein the perforations cover at least 25% of the total surface area of the film, and the film has an inside/inside cling property of 5 to 22 gr, and a weight of no more than 13 g/m2.
摘要翻译：本发明提供了一种聚烯烃预拉伸包装薄膜，其包括沿着薄膜的纵向方向排列成一列列的穿孔，其中每个相邻的所述穿孔的柱分隔开一列，而不是沿着纵向的穿孔，并且穿孔是交错的在所述膜的横向方向上，其中所述膜包括在其至少一个表面上的固有粘附表面; 其中所述穿孔覆盖所述膜的总表面积的至少25％，并且所述膜具有5至22gr的内部/内部粘附性，并且重量不超过13g / m 2。

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