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1. 发明授权

US4201639A Processes for preparing cyclohexadiene derivatives 失效
标题翻译：制备环己二烯衍生物的方法
公开(公告)号：US4201639A
公开(公告)日：1980-05-06
申请号：US8886
申请日：1979-02-02
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C11B9/00 , B01J1/10 , C07C45/00
CPC分类号： C07C13/23 , A24B15/34 , C11B9/0034 , C07C2101/16 , Y10S204/912
摘要： Described is a process for preparing cyclohexadiene derivatives having the generic formula: ##STR1## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen comprising the step of reacting a 1-alkyl-3,5,5-trimethylcyclohexa-1,3-diene or a 1-alkyl-3,4,4-trimethylcyclohexa-1,3-diene with oxygen in the presence of light, an ultraviolet sensitizer, and a basic catalyst; and fractionally distilling the resulting product.
摘要翻译：描述了制备具有以下通式的环己二烯衍生物的方法：其中R是C 1 -C 5烷基之一，当R 2为氢时R 1为甲基，包括使1-烷基-3,5,5-三甲基环己烷 1,3-二烯或1-烷基-3,4,4-三甲基环己-1,3-二烯与氧在光存在下，紫外线敏化剂和碱性催化剂; 并分馏蒸馏生成的产物。

2. 发明授权

US4186149A Processes for preparing cyclohexadiene derivatives 失效
标题翻译：制备环己二烯衍生物的方法
公开(公告)号：US4186149A
公开(公告)日：1980-01-29
申请号：US8779
申请日：1979-02-02
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C07D317/72 , C11B9/00 , C07C45/00
CPC分类号： C07D317/72 , A24B15/34 , C07C13/23 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C11B9/0034 , C07C2101/16
摘要： Described is a process for preparing cyclohexadiene derivatives having the generic formula: ##STR1## by means of reacting a compound having the structure: ##STR2## with mineral acid selected from the group consisting of dilute hydrochloric acid, dilute phosphoric acid and dilute sulfuric acid; wherein R is C.sub.1 -C.sub.5 alkyl. The products produced by this process are useful for their organoleptic properties in perfumes, foodstuffs and tobaccos.
摘要翻译：描述了通过使具有以下结构的化合物与选自稀盐酸，稀磷酸和稀硫酸的无机酸反应制备具有以下通式的环己二烯衍生物的方法：＆lt; IMAGE＆gt; 其中R是C 1 -C 5烷基。通过该方法生产的产品对于其在香料，食品和烟草中的感官特性是有用的。

3. 发明授权

US4154763A 4-Butyl-3,4,5-trimethylcyclohexa-25-dienone 失效
标题翻译： 4-丁基-3,4,5-三甲基环己基-25-二烯酮
公开(公告)号：US4154763A
公开(公告)日：1979-05-15
申请号：US860121
申请日：1977-12-13
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C07D317/72 , C11B9/00 , C11D3/50 , C11D9/44 , C07C49/48
CPC分类号： C07D317/72 , A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C11B9/0034 , C11D3/50 , C11D9/442 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma; tobacco flavor and aroma; perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, tobacco, perfume and perfumed article aroma imparting materials of one or more cyclohexadiene derivatives having the generic formula: ##STR1## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen, and R.sub.1 is hydrogen when R.sub.2 is methyl, produced by one of the following processes:(i) Reacting a 1-alkyl-3,5,5-trimethylcyclohexa-1,3-diene with oxygen in the presence of light, an ultraviolet sensitizer, and a basic catalyst; and fractionally distilling the resulting product; or(ii) Reacting a 4-alkyl-4-hydroxy-3,5,5-trimethyl-2-cyclohexen-1-one with dilute aqueous mineral acid and distilling the resulting reaction product.Addition of one or more of the cyclohexadiene derivatives having the formula: ##STR2## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen, and R.sub.1 is hydrogen when R.sub.2 is methyl, to consumable materials is indicated to produce:(a) In foodstuffs, foodstuff flavoring compositions, chewing gums, toothpastes and medicinal products, sweet, hay-like, heliotropine-like, black pepper-like, woody, tobacco-like and "Oriental" aroma characteristics with sweet, hay-like, heliotropine-like, black pepper-like, woody, tobacco, "Oriental" flavor characteristics;(b) In perfumes, colognes and perfumed articles, warm sweet, slightly minty, woody, natural green, herbaceous, Jasmine-like, fruity aromas; and(c) In tobaccos and tobacco flavors, "dry black tobacco-like" notes, spicey notes, celery-like notes, black pepper-like notes, sweet notes and Virginia tobacco-like notes prior to and on smoking, in both the main stream and the side stream.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品香味和香气的方法和组合物; 烟草香气和香气; 香水和香水制品香气增强，增强和赋予组合物; 作为一种或多种具有以下通式的环己二烯衍生物的食品，口香糖，牙膏，药用产品，烟草，香料和香料制品香气赋予材料：其中R是C 1 -C 5烷基之一，当R 2为R 1时，R 1为甲基是氢，当R 2为甲基时，R 1为氢，由以下方法之一制备：

4. 发明授权

US4135520A Tobacco flavoring with cyclohexadiene derivatives 失效
标题翻译：烟草香料与环己二烯衍生物
公开(公告)号：US4135520A
公开(公告)日：1979-01-23
申请号：US860122
申请日：1977-12-13
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C07D317/72 , C11B9/00 , C11D3/50 , C11D9/44 , A24B3/12
CPC分类号： C07D317/72 , A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C11B9/0034 , C11D3/50 , C11D9/442 , C07C2101/16
摘要： Cyclohexadiene derivatives as tobacco flavoring compositions.
摘要翻译：环己二烯衍生物作为烟草香料组合物。

5. 发明授权

US4154696A Detergent containing cyclohexadiene derivatives 失效
标题翻译：含有环己二烯衍生物的洗涤剂
公开(公告)号：US4154696A
公开(公告)日：1979-05-15
申请号：US917772
申请日：1978-06-21
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C07D317/72 , C11B9/00 , C11D3/50 , C11D9/44 , C11D3/60
CPC分类号： C07D317/72 , A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C11B9/0034 , C11D3/50 , C11D9/442 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma; tobacco flavor and aroma; perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, tobacco, perfume and perfumed article aroma imparting materials of one or more cyclohexadiene derivatives having the generic formula: ##STR1## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen, and R.sub.1 is hydrogen when R.sub.2 is methyl, produced by one of the following processes:(i) Reacting a 1-alkyl-3,5,5-trimethylcyclohexa-1,3-diene with oxygen in the presence of light, an ultraviolet sensitizer, and a basic catalyst; and fractionally distilling the resulting product; or(ii) Reacting a 4-alkyl-4-hydroxy-3,5,5-trimethyl-2-cyclohexen-1-one with dilute aqueous mineral acid and distilling the resulting reaction product.Addition of one or more of the cyclohexadiene derivatives having the formula: ##STR2## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen, and R.sub.1 is hydrogen when R.sub.2 is methyl, to consumable materials is indicated to produce:(a) In foodstuffs, foodstuff flavoring compositions, chewing gums, toothpastes and medicinal products, sweet, hay-like, heliotropine-like, black pepper-like, woody, tobacco-like and "Oriental" aroma characteristics with sweet, hay-like, heliotropine-like, black pepper-like, woody, tobacco, "Oriental" flavor characteristics;(b) In perfumes, colognes and perfumed articles, warm sweet, slightly minty, woody, natural green, herbaceous, Jasmine-like, fruity aromas; and(c) In tobaccos and tobacco flavors, "dry black tobacco-like" notes, spicey notes, celery-like notes, black pepper-like notes, sweet notes and Virginia tobacco-like notes prior to and on smoking, in both the main stream and the side stream.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品香味和香气的方法和组合物; 烟草香气和香气; 香水和香水制品香气增强，增强和赋予组合物; 作为一种或多种具有以下通式的环己二烯衍生物的食品，口香糖，牙膏，药用产品，烟草，香料和香料制品香气赋予材料：其中R是C 1 -C 5烷基之一，当R 2为R 1时，R 1为甲基是氢，当R 2为甲基时，R 1为氢，由以下方法之一制备：

6. 发明授权

US4139650A Flavoring with a tricyclic alcohol 失效
标题翻译：用三环酒精调味
公开(公告)号：US4139650A
公开(公告)日：1979-02-13
申请号：US683310
申请日：1976-05-05
申请人： Kenneth K. Light , Edward J. Shuster , Joaquin F. Vinals , Manfred H. Vock
发明人： Kenneth K. Light , Edward J. Shuster , Joaquin F. Vinals , Manfred H. Vock
IPC分类号： C07C49/587 , A24B15/34 , C07C27/00 , C07C29/00 , C07C29/136 , C07C35/37 , C07C45/00 , C07C45/62 , C07C67/00 , C11B9/00 , A23L1/226
CPC分类号： C07C45/63 , A24B15/345 , C07C45/62 , C07C45/69 , C11B9/0042
摘要： Compositions for altering the flavor and/or aroma of consumable products including foods, tobacco and perfumes utilizing as the essential ingredient at least one organic tricyclic alcohol having the formula: ##STR1## wherein each of R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 and R.sub.6 is selected from the group consisting of hydrogen and methyl; wherein the dashed line is a carbon-carbon single bond or a carbon-carbon double bond; and wherein when the dashed line is a carbon-carbon single bond, one of R.sub.2 or R.sub.3 is hydrogen.
摘要翻译：用于改变消费品的味道和/或香气的组合物，包括食品，烟草和香料，其利用至少一种具有下式的有机三环醇作为必需组分：其中R1，R2，R3，R4，R5和R6 选自氢和甲基; 其中虚线是碳 - 碳单键或碳 - 碳双键; 并且其中当虚线为碳 - 碳单键时，R 2或R 3中的一个为氢。

7. 发明授权

US4130508A Perfume compositions containing cyclohexadiene derivatives 失效
标题翻译：含有环己二烯衍生物的香料组合物
公开(公告)号：US4130508A
公开(公告)日：1978-12-19
申请号：US860123
申请日：1977-12-13
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C07D317/72 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C07D317/72 , A24B15/34 , C07C13/23 , C07C29/09 , C07C29/40 , C07C29/68 , C07C45/34 , C07C45/59 , C07C45/66 , C07C49/603 , C07C49/713 , C11B9/0034 , C11D3/50 , C11D9/442 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma; tobacco flavor and aroma; perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, tobacco, perfume and perfumed article aroma imparting materials of one or more cyclohexadiene derivatives having the generic formula: ##STR1## wherein R is one of C.sub.1 -C.sub.5 alkyl, R.sub.1 is methyl when R.sub.2 is hydrogen, and R.sub.1 is hydrogen when R.sub.2 is methyl.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品香味和香气的方法和组合物; 烟草香气和香气; 香水和香水制品香气增强，增强和赋予组合物; 作为一种或多种具有以下通式的环己二烯衍生物的食品，口香糖，牙膏，药用产品，烟草，香料和香料制品香气赋予材料：其中R是C 1 -C 5烷基之一，当R 2为R 1时，R 1为甲基是氢，当R 2是甲基时，R 1是氢。

8. 发明授权

US4126140A Smoking tobacco and smoking tobacco flavoring compositions containing hydroxy cyclohexenone derivatives 失效
标题翻译：吸烟烟草和含有羟基环己烯酮衍生物的烟草调味组合物
公开(公告)号：US4126140A
公开(公告)日：1978-11-21
申请号：US851684
申请日：1977-11-15
申请人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
发明人： Kenneth K. Light , Bette M. Spencer , Joaquin F. Vinals , Jacob Kiwala , Manfred H. Vock , Edward J. Shuster
IPC分类号： A23G4/00 , A23G4/06 , A23L27/20 , A24B15/34 , C07C13/23 , C07C29/40 , C07C29/50 , C07C45/59 , C07D317/72 , C11B9/00 , A24B3/12 , A24B15/04
CPC分类号： A23G4/06 , A23L27/203 , A24B15/34 , C07C13/23 , C07C29/40 , C07C45/34 , C07C45/59 , C07D317/72 , C11B9/0034 , C07C2101/16
摘要： Processes and compositions are described for the use in smoking tobacco flavor and aroma augmenting, enhancing and imparting compositions and as smoking tobacco aroma and taste imparting materials of hydroxy cyclohexenone derivatives having the generic formula: ##STR1## wherein one of X and Y is a keto moiety having the structure: ##STR2## and the other of X and Y is a carbinol moiety having the structure: ##STR3##
摘要翻译：描述了用于吸烟烟草风味和香气增强，增强和赋予组合物以及吸烟具有以下通式的羟基环己烯酮衍生物的烟草香气和味道赋予材料的方法和组合物：其中X和Y之一是酮具有以下结构的部分：＆lt; IMAGE＆gt; X和Y中的另一个是具有以下结构的甲醇部分：

9. 发明授权

US4327749A Alkyl esters of 1-alkanoyl cycloalkanols, process for preparing same and organoleptic uses thereof 失效
标题翻译： 1-烷酰基环烷醇的烷基酯，其制备方法及其感官用途
公开(公告)号：US4327749A
公开(公告)日：1982-05-04
申请号：US133828
申请日：1980-03-25
申请人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
发明人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , A24B15/30
CPC分类号： A24B15/34
摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.
摘要翻译：描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草，吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

10. 发明授权

US4374055A Alkyl esters of 1-alkanoyl cycloalkanols and organoleptic uses thereof 失效
标题翻译： 1-烷酰基环烷醇的烷基酯及其感官用途
公开(公告)号：US4374055A
公开(公告)日：1983-02-15
申请号：US314002
申请日：1981-10-22
申请人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
发明人： Ronald P. Schreck , Kenneth K. Light , John B. Hall , Frederick L. Schmitt , Manfred H. Vock , William L. Schreiber , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： A24B15/34 , C11B9/0026 , C11D3/50
摘要： Described is a process for preparing several substituted or unsubstituted cycloalkyl acyl alkanoates defined according to the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 taken together complete a cycloalkyl moiety or methyl, dimethyl or trimethyl substituted cycloalkyl moiety containing five or six carbon atoms in the ring and wherein R.sub.3 is C.sub.1 -C.sub.3 lower alkyl and R.sub.4 is methyl or hydrogen by reacting a compound having the generic structure: ##STR2## in an aqueous silver-ion containing solution having a weakly acidic pH at elevated temperatures. The compounds so produced are useful for their organoleptic properties in consumable materials, such as foodstuffs, foodstuff flavorants, chewing gums, chewing gum flavorants, toothpastes, toothpaste flavorants, medicinal products, medicinal product flavorants, chewing tobaccos, chewing tobacco flavorants, smoking tobaccos, smoking tobacco flavorants, perfume compositions, perfumed articles, such as cationic, anionic, nonionic and zwitterionic detergents, fabric softener compositions, drier-added fabric softener articles, textile sizing agents and optical brighteners for textiles as well as colognes.
摘要翻译：描述了根据通用结构定义的若干取代或未取代的环烷基酰基链烷酸酯的方法：其中R 1和R 2一起完成环烷基部分或含有5或6个碳原子的甲基，二甲基或三甲基取代的环烷基部分环，其中R 3是C 1 -C 3低级烷基，R 4是甲基或氢，通过使具有通式结构的化合物：在高温下具有弱酸性pH的含水银离子溶液中。如此生产的化合物可用于消费材料如食品，食品香料，口香糖，口香糖调味剂，牙膏，牙膏调味剂，药用产品，药用香料，咀嚼烟草，咀嚼烟草香料，烟草烟草，吸烟烟草调味剂，香料组合物，香料制品，例如阳离子，阴离子，非离子和两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，纺织品上浆剂和用于纺织品的荧光增白剂以及古龙水。

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