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1. 发明授权

US06448436B1 Integrated process for the production of 2, 6-naphthalene dicarboxylic acid 失效
标题翻译：用于生产2,6-萘二羧酸的综合工艺
公开(公告)号：US06448436B1
公开(公告)日：2002-09-10
申请号：US09644003
申请日：2000-08-22
申请人： Keith Michael Kreitman , Steve Edward Brewer , John Bernard Rodden , Robert Lawrence Blackbourn , Thomas Fairchild Brownscombe , James Laurel Buechele , Ye-Mon Chen , Zaida Diaz , Donn Anthony DuBois , Raymond Lawrence June , Brendan Dermot Murray , Michael Wayne Potter
发明人： Keith Michael Kreitman , Steve Edward Brewer , John Bernard Rodden , Robert Lawrence Blackbourn , Thomas Fairchild Brownscombe , James Laurel Buechele , Ye-Mon Chen , Zaida Diaz , Donn Anthony DuBois , Raymond Lawrence June , Brendan Dermot Murray , Michael Wayne Potter
IPC分类号： C07C51265
CPC分类号： C08G63/189 , B01J27/232 , C07C51/02 , C07C51/15 , C07C51/265 , C07C51/412 , C07C51/416 , C07C51/42 , C07C51/43 , C07C51/47 , C07C51/487 , Y02P20/125 , C07C63/16 , C07C63/36 , C07C63/24 , C07C63/38 , C07C63/26 , C07C63/15 , C07C63/307
摘要： Disclosed is an integrated process for producing 2,6-naphthalene dicarboxylicacid comprising oxidizing a methylnaphthalene feedstock, hydrodebrominating the crude naphthoic acid product under conditions different from any work known in the art, forming a potassium salt of the acid; disproportionating the potassium salt to produce 2,6 potassium salts of NDA; selectively precipitating K2NDA; selectively precipitating the monopotassium salt of 2,6 NDA(KHNDA); disproportionating the KHNDA into 2,6 NDA and K2NDA; further reacting the 2,6 NDA in a pipe reactor; and drying the product 2,6 NDA by conventional means or directly slurrying directly into a PEN process. The process can tolerate impurities in the economical methylnaphthalene feed and the resulting 2,6 NDA is of high quality with
摘要翻译：公开了一种用于生产2,6-萘二羧酸的综合方法，包括氧化甲基萘原料，在与本领域已知的任何工作不同的条件下氢化溴化粗萘甲酸产物，形成酸的钾盐; 歧化钾盐生成2,6-二硝基苯胺钾盐; 选择性沉淀K2NDA; 选择性沉淀2,6 NDA（KHNDA）的单钾盐; 将KHNDA分解为2,6 NDA和K2NDA; 进一步使2,6 NDA在管式反应器中反应; 并通过常规方法干燥产品2,6NDA或直接浆化成PEN方法。该方法可以耐受经济的甲基萘进料中的杂质，并且所得的2,6 NDA是高质量的，具有<50ppm的钾。

2. 发明授权

US06448437B1 Disproportionation catalyst 失效
标题翻译：歧化催化剂
公开(公告)号：US06448437B1
公开(公告)日：2002-09-10
申请号：US09643398
申请日：2000-08-22
申请人： Donn Anthony DuBois , Brendan Dermot Murray
发明人： Donn Anthony DuBois , Brendan Dermot Murray
IPC分类号： C02C51347
CPC分类号： C08G63/189 , B01J23/002 , B01J23/80 , B01J23/83 , B01J27/232 , B01J37/088 , B01J2523/00 , C07C51/02 , C07C51/15 , C07C51/265 , C07C51/412 , C07C51/416 , C07C51/42 , C07C51/43 , C07C51/47 , C07C51/487 , C07C63/38 , C07C63/15 , C07C63/16 , C07C63/36 , C07C63/24 , C07C63/26 , C07C63/307 , B01J2523/17 , B01J2523/27 , B01J2523/48
摘要： Disclosed are halide-free catalyst compositions for the disproportionation/isomerization of aromatic carboxylic acid salts. In one embodiment the catalyst comprises a mixed catalyst of compounds of copper, zinc, and zirconium; and, in a second embodiment, the catalyst comprises a copper compound treated with a base, optionally used with a promoter. Both halide-free catalysts provide advantages with respect to metallurgic problems, as well as good stability, activity and selectivity, and the later is faster kinetically at lower temperatures.
摘要翻译：公开了用于芳族羧酸盐的歧化/异构化的无卤化物催化剂组合物。在一个实施方案中，催化剂包含铜，锌和锆化合物的混合催化剂; 并且在第二实施方案中，催化剂包含用碱处理的铜化合物，任选与启动子一起使用。无卤化物催化剂在冶金问题方面提供优点，以及良好的稳定性，活性和选择性，并且在较低温度下动力学更快。

3. 发明申请

US20110113958A1 METHOD OF MAKING A HIGH-PERFORMANCE SUPPORTED GAS SEPARATION MOLECULAR SIEVE MEMBRANE USING A SHORTENED CRYSTALLIZATION TIME 失效
标题翻译：使用短时间结晶时间制备高性能支持气体分离分子筛膜的方法
公开(公告)号：US20110113958A1
公开(公告)日：2011-05-19
申请号：US12936795
申请日：2009-05-15
申请人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
发明人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
IPC分类号： B01D53/22 , B05D5/00
CPC分类号： B01D71/028 , B01D53/22 , B01D53/228 , B01D63/06 , B01D67/0051 , B01D67/0083 , B01D69/105 , B01D2256/22 , B01D2256/24 , B01D2257/504 , B01D2257/7022 , B01D2323/12 , Y02C10/10
摘要： A method of making a supported gas separation molecular sieve membrane. In this method a porous support, which is preferably pretreated, is contacted with a molecular sieve synthesis mixture under hydrothermal synthesis conditions. The contacting step is conducted for a shortened crystallization time period. The resulting coated porous support is calcined to yield the supported gas separation molecular sieve membrane having particularly good gas separation characteristics.
摘要翻译：制备负载型气体分离分子筛膜的方法。在该方法中，优选预处理的多孔载体在水热合成条件下与分子筛合成混合物接触。接触步骤进行缩短的结晶时间段。将得到的涂覆的多孔载体煅烧，得到具有特别好的气体分离特性的负载气体分离分子筛膜。

4. 发明授权

US06492568B1 Removal of phosphorus-containing compounds from an olefin feedstock 失效
标题翻译：从烯烃原料中除去含磷化合物
公开(公告)号：US06492568B1
公开(公告)日：2002-12-10
申请号：US09566463
申请日：2000-05-08
申请人： Brendan Dermot Murray , Zaida Diaz , Glenn Charles Komplin
发明人： Brendan Dermot Murray , Zaida Diaz , Glenn Charles Komplin
IPC分类号： C07C2720
CPC分类号： C07C7/14841 , C07C29/16 , C07C11/02 , C07C31/125
摘要： The invention pertains to a process of removing phosphorus-containing impurities from an olefin stream using a sorbent comprising a metal. The olefin stream preferably comprises primarily olefins having at least 6 carbon atoms.
摘要翻译：本发明涉及使用包含金属的吸附剂从烯烃流中除去含磷杂质的方法。烯烃流优选主要包含具有至少6个碳原子的烯烃。

5. 发明申请

US20100116130A1 METHOD OF MAKING A HIGH-PERFORMANCE SUPPORTED GAS SEPARATION MOLECULAR SIEVE MEMBRANE USING A SHORTENED CRYSTALLIZATION TIME 审中-公开
标题翻译：使用短时间结晶时间制备高性能支持气体分离分子筛膜的方法
公开(公告)号：US20100116130A1
公开(公告)日：2010-05-13
申请号：US12466569
申请日：2009-05-15
申请人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
发明人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
IPC分类号： B01D53/22 , B05D1/36 , B05D3/02
CPC分类号： B01D71/028 , B01D53/22 , B01D53/228 , B01D63/06 , B01D67/0051 , B01D67/0083 , B01D69/105 , B01D2256/22 , B01D2256/24 , B01D2257/504 , B01D2257/7022 , B01D2323/12 , Y02C10/10
摘要： A method of making a supported gas separation molecular sieve membrane. In this method a porous support, which is preferably pretreated, is contacted with a molecular sieve synthesis mixture under hydrothermal synthesis conditions. The contacting step is conducted for a shortened crystallization time period. The resulting coated porous support is calcined to yield the supported gas separation molecular sieve membrane having particularly good gas separation characteristics.
摘要翻译：制备负载型气体分离分子筛膜的方法。在该方法中，优选预处理的多孔载体在水热合成条件下与分子筛合成混合物接触。接触步骤进行缩短的结晶时间段。将得到的涂覆的多孔载体煅烧，得到具有特别好的气体分离特性的负载气体分离分子筛膜。

6. 发明授权

US08685143B2 Method of making a high-performance supported gas separation molecular sieve membrane using a shortened crystallization time 失效
标题翻译：使用缩短结晶时间制备高性能负载型气体分离分子筛膜的方法
公开(公告)号：US08685143B2
公开(公告)日：2014-04-01
申请号：US12936795
申请日：2009-05-15
申请人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
发明人： Moises Abraham Carreon , Zaida Diaz , John Lucien Falconer , Hans Heinrich Funke , Shiguang Li , Brendan Dermot Murray , Richard Daniel Noble , Paul Jason Williams
IPC分类号： B01D53/22 , B01D67/00
CPC分类号： B01D71/028 , B01D53/22 , B01D53/228 , B01D63/06 , B01D67/0051 , B01D67/0083 , B01D69/105 , B01D2256/22 , B01D2256/24 , B01D2257/504 , B01D2257/7022 , B01D2323/12 , Y02C10/10
摘要： A method of making a supported gas separation molecular sieve membrane. In this method a porous support, which is preferably pretreated, is contacted with a molecular sieve synthesis mixture under hydrothermal synthesis conditions. The contacting step is conducted for a shortened crystallization time period. The resulting coated porous support is calcined to yield the supported gas separation molecular sieve membrane having particularly good gas separation characteristics.
摘要翻译：制备负载型气体分离分子筛膜的方法。在该方法中，优选预处理的多孔载体在水热合成条件下与分子筛合成混合物接触。接触步骤进行缩短的结晶时间段。将得到的涂覆的多孔载体煅烧，得到具有特别好的气体分离特性的负载气体分离分子筛膜。

7. 发明授权

US06653514B1 Removal of phosphorus-containing impurities from an olefin feedstock 失效
标题翻译：从烯烃原料中除去含磷杂质
公开(公告)号：US06653514B1
公开(公告)日：2003-11-25
申请号：US09566461
申请日：2000-05-08
申请人： Brendan Dermot Murray , David Michael Singleton , Zaida Diaz
发明人： Brendan Dermot Murray , David Michael Singleton , Zaida Diaz
IPC分类号： C07C2720
CPC分类号： C07C7/13 , C07C7/12 , C07C29/16 , C07C11/02 , C07C31/125
摘要： The invention pertains to a process of removing phosphorous-containing impurities and preferably also dienes, from an olefin stream using a sorbent selected from the group consisting of an acidic ion exchange resin, an acidic zeolite, an acidic alumina, a neutral alumina, and an activated carbon. The olefin stream preferably comprises primarily olefins having at least 6 carbon atoms.
摘要翻译：本发明涉及一种使用选自酸性离子交换树脂，酸性沸石，酸性氧化铝，中性氧化铝和酸性氧化铝的吸附剂从烯烃流中除去含磷杂质，优选二烯的方法。活性炭。烯烃流优选主要包含具有至少6个碳原子的烯烃。

8. 发明授权

US07462752B2 Process to convert linear alkanes into alpha olefins 失效
标题翻译：将线性烷烃转化为α-烯烃的方法
公开(公告)号：US07462752B2
公开(公告)日：2008-12-09
申请号：US11109551
申请日：2005-04-19
申请人： Howard Lam-Ho Fong , Lizbeth Olivia Cisneros Trevino , Brendan Dermot Murray , Manuel Luis Cano
发明人： Howard Lam-Ho Fong , Lizbeth Olivia Cisneros Trevino , Brendan Dermot Murray , Manuel Luis Cano
IPC分类号： C07C1/26
CPC分类号： C07C29/124 , C07C1/30 , C07C11/02 , C07C17/10 , C07C17/358 , C07C17/37 , C07C2521/10 , C07C2521/14 , C07C2523/14 , C07C2523/44 , C07C2523/745 , C07C2523/78 , C07C19/075 , C07C19/01 , C07C31/125
摘要： This invention provides for a process to convert branched or linear alkanes to branched or linear alpha olefins (AO) of the same carbon number. The process comprises the steps of: a) halogenating linear alkanes, branched alkanes, or a mixture of linear and branched alkane to produce a mixture containing primary mono-haloalkanes and hydrogen halide; b) separating the hydrogen halide from the mixture and optionally neutralizing it with a metal oxide to produce a partially halogenated metal oxide and/or metal halide which may be regenerated; c) separating the primary mono-haloalkanes from the mixture; d) reacting the separated primary mono-haloalkanes with a metal oxide to produce a mixture of products that contains alpha olefins, unconverted primary mono-haloalkanes, possibly other reaction products, and a partially halogenated metal oxide and/or metal halide which may be regenerated; e) regenerating the partially halogenated metal oxide and/or metal halide to halogen and/or acid and a metal oxide (such as Cl2) for recycle by reaction with air or oxygen ; and f) removing the unreacted primary mono-haloalkane from the reaction mixture and then purifying the alpha olefin.
摘要翻译：本发明提供将支链或直链烷烃转化为相同碳数的支链或直链α-烯烃（AO）的方法。该方法包括以下步骤：a）将直链烷烃，支链烷烃或直链和支链烷烃的混合物卤化以产生含有主要单卤代烷烃和卤化氢的混合物; b）从混合物中分离卤化氢并任选地用金属氧化物中和它以产生可再生的部分卤化的金属氧化物和/或金属卤化物; c）从混合物中分离初级单卤代烷烃; d）使分离的初级单卤代烷烃与金属氧化物反应以产生含有α-烯烃，未转化的初级单卤代烷烃，可能的其它反应产物和可再生的部分卤化的金属氧化物和/或金属卤化物的产物的混合物 ; e）将部分卤化的金属氧化物和/或金属卤化物再生成卤素和/或酸和金属氧化物（例如Cl 2），以通过与空气或氧气反应再循环; 和f）从反应混合物中除去未反应的主要单卤代烷烃，然后纯化α-烯烃。

9. 发明授权

US07348462B2 Process for preparing branched olefins from a paraffinic wax 有权
标题翻译：从链烷烃蜡制备支链烯烃的方法
公开(公告)号：US07348462B2
公开(公告)日：2008-03-25
申请号：US10789115
申请日：2004-02-27
申请人： Laurent Alain Michel Fenouil , Brendan Dermot Murray , Paul Marie Ayoub
发明人： Laurent Alain Michel Fenouil , Brendan Dermot Murray , Paul Marie Ayoub
IPC分类号： C10L5/00 , C10L1/16 , C10M101/02 , C10M107/00 , C10M143/00 , C10M165/00 , C10M167/00 , C10M169/00 , C10M171/00
CPC分类号： C10G45/00 , C10G65/043 , C10G69/123 , C10G2300/1085 , C10G2300/1096 , C10G2400/22 , C10G2400/30
摘要： A process for preparing branched alkyl aromatic hydrocarbons, which process comprises contacting branched olefins with an aromatic hydrocarbon under alkylating conditions, which branched olefins have been obtained by a process which comprises dehydrogenating an isoparaffinic composition over a suitable catalyst which isoparaffinic composition has been obtained by hydrocracking and hydroisomerization of a paraffinic wax and which isoparaffinic composition comprises paraffins having a carbon number in the range of from 7 to 35, of which paraffins at least a portion of the molecules is branched, the average number of branches per paraffin molecule being at least 0.5 and the branching comprising methyl and optionally ethyl branches; a process for preparing (branched-alkyl)arylsulfonates, comprising sulfonating branched alkyl aromatic hydrocarbons which branched alkyl aromatic hydrocarbons have been prepared by the said process for preparing branched alkyl aromatic hydrocarbons; and branched alkyl aromatic hydrocarbon compositions and (branched-alkyl)arylsulfonate compositions which are obtainable by the processes so defined.
摘要翻译：一种制备支链烷基芳烃的方法，该方法包括在烷基化条件下使支链烯烃与芳族烃接触，该支链烯烃已经通过包括使异链烷烃组合物在合适的催化剂上脱氢的方法获得，该催化剂已经通过加氢裂化获得了异链烷烃组合物和链烷烃蜡的加氢异构化，并且所述异链烷烃组合物包含碳数为7至35的链烷烃，其中至少部分分子的链烷烃是支链的，每个链烷烃分子的平均支链数为至少0.5 并且支链包含甲基和任选的乙基支链; 一种制备（支链 - 烷基）芳基磺酸盐的方法，包括磺化支化烷基芳烃，其中支链烷基芳烃是通过所述制备支链烷基芳烃的方法制备的; 和支链烷基芳烃组合物和（支链 - 烷基）芳基磺酸盐组合物，其可通过如此定义的方法获得。

10. 发明授权

US06747165B2 Process for preparing (branched-alkyl) arylsulfonates and a (branched-alkyl) arylsulfonate composition 失效
公开(公告)号：US06747165B2
公开(公告)日：2004-06-08
申请号：US10075318
申请日：2002-02-14
申请人： Laurent Alain Michel Fenouil , Brendan Dermot Murray , Paul Marie Ayoub
发明人： Laurent Alain Michel Fenouil , Brendan Dermot Murray , Paul Marie Ayoub
IPC分类号： C07C30300
CPC分类号： C10G45/00 , C10G65/043 , C10G69/123 , C10G2300/1085 , C10G2300/1096 , C10G2400/22 , C10G2400/30
摘要： A process for preparing branched alkyl aromatic hydrocarbons, which process comprises contacting branched olefins with an aromatic hydrocarbon under alkylating conditions, which branched olefins have been obtained by a process which comprises dehydrogenating an isoparaffinic composition over a suitable catalyst which isoparaffinic composition has been obtained by hydrocracking and hydroisomerization of a paraffinic wax and which isoparaffinic composition comprises paraffins having a carbon number in the range of from 7 to 35, of which paraffins at least a portion of the molecules is branched, the average number of branches per paraffin molecule being at least 0.5 and the branching comprising methyl and optionally ethyl branches; a process for preparing (branched-alkyl)arylsulfonates, comprising sulfonating branched alkyl aromatic hydrocarbons which branched alkyl aromatic hydrocarbons have been prepared by the said process for preparing branched alkyl aromatic hydrocarbons; and branched alkyl aromatic hydrocarbon compositions and (branched-alkyl)arylsulfonate compositions which are obtainable by the processes so defined.

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