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    • 7. 发明授权
    • Article with organic-inorganic composite film
    • 文章用有机 - 无机复合膜
    • US08039111B2
    • 2011-10-18
    • US12083038
    • 2006-10-05
    • Teruyuki SasakiKazutaka KamitaniKazuyuki Inoguchi
    • Teruyuki SasakiKazutaka KamitaniKazuyuki Inoguchi
    • B32B9/04B32B17/06B32B9/00B32B13/04
    • C03C17/009Y10T428/26Y10T428/265Y10T428/31504
    • An article with a silica-based film that contains an organic material and has excellent mechanical strength. This article includes a substrate and an organic-inorganic composite film that is formed on the surface of the substrate. The organic-inorganic composite film contains silica as its main component. A value of (0.19A+0.03) or lower (A denotes the film thickness [μm]) is obtained through X-ray diffraction analysis on the organic-inorganic composite film, with the X-ray incident angle being fixed at 1° with respect to the surface of the organic-inorganic composite film, when the intensity of a peak at a diffraction angle of 3° to 10° is standardized using the intensity of a halo pattern peak at a diffraction angle of 20° to 30°. A value of 0.25 or lower is obtained through Fourier transform infrared spectroscopy analysis on the organic-inorganic composite film, when the intensity of a peak at around 950 cm−1 based on a Si—OH group is standardized using the intensity of a peak at around 1100 cm−1 based on a Si—O—Si bond.
    • 具有含有有机材料并具有优异机械强度的二氧化硅基膜的制品。 该制品包括基材和形成在基材表面上的有机 - 无机复合膜。 有机 - 无机复合膜含有二氧化硅作为其主要成分。 通过对有机 - 无机复合膜的X射线衍射分析获得(0.19A + 0.03)以下的值(A表示膜厚度[μm]),将X射线入射角度固定为1°, 相对于有机 - 无机复合膜的表面,使用衍射角为20°〜30°的光晕图案峰的强度,将衍射角为3°〜10°的峰的强度标准化。 通过对有机 - 无机复合膜的傅里叶变换红外光谱分析,当使用基于Si-OH基的950cm -1附近的峰强度用标准化的峰强度进行标准化时,可获得0.25以下的值 基于Si-O-Si键约1100cm -1。
    • 9. 发明申请
    • Article With Organic-Inorganic Composite Film
    • 有机无机复合薄膜
    • US20090246512A1
    • 2009-10-01
    • US12083038
    • 2006-10-05
    • Teruyuki SasakiKazutaka KamitaniKazuyuki Inoguchi
    • Teruyuki SasakiKazutaka KamitaniKazuyuki Inoguchi
    • B32B17/06B32B9/00
    • C03C17/009Y10T428/26Y10T428/265Y10T428/31504
    • An article with a silica-based film that contains an organic material and has excellent mechanical strength. This article includes a substrate and an organic-inorganic composite film that is formed on the surface of the substrate. The organic-inorganic composite film contains silica as its main component. A value of (0.19A+0.03) or lower (A denotes the film thickness [μm]) is obtained through X-ray diffraction analysis on the organic-inorganic composite film, with the X-ray incident angle being fixed at 1° with respect to the surface of the organic-inorganic composite film, when the intensity of a peak at a diffraction angle of 3° to 10° is standardized using the intensity of a halo pattern peak at a diffraction angle of 20° to 30°. A value of 0.25 or lower is obtained through Fourier transform infrared spectroscopy analysis on the organic-inorganic composite film, when the intensity of a peak at around 950 cm−1 based on a Si—OH group is standardized using the intensity of a peak at around 1100 cm−1 based on a Si—O—Si bond.
    • 具有含有有机材料并具有优异机械强度的二氧化硅基膜的制品。 该制品包括基材和形成在基材表面上的有机 - 无机复合膜。 有机 - 无机复合膜含有二氧化硅作为其主要成分。 通过对有机 - 无机复合膜的X射线衍射分析得到(0.19A + 0.03)以下的值(A表示膜厚度[μm]),将X射线入射角固定为1°, 相对于有机 - 无机复合膜的表面,使用衍射角为20°〜30°的光晕图案峰的强度,将衍射角为3°〜10°的峰的强度标准化。 通过对有机 - 无机复合膜的傅立叶变换红外光谱分析,当使用基于Si-OH基团的约950cm -1处的峰强度通过使用Si-OH基的峰强度来标准化时,获得0.25以下的值 基于Si-O-Si键约1100cm -1。