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1. 发明申请

US20090234036A1 METHOD FOR PRODUCING RIGID POLYURETHANE FOAM, AND RIGID POLYURETHANE FOAM 失效
标题翻译：生产刚性聚氨酯泡沫的方法和刚性聚氨酯泡沫
公开(公告)号：US20090234036A1
公开(公告)日：2009-09-17
申请号：US12469178
申请日：2009-05-20
申请人： Katsuhiko SHIMIZU , Teruhiko Yasuda , Hiroshi Wada
发明人： Katsuhiko SHIMIZU , Teruhiko Yasuda , Hiroshi Wada
IPC分类号： C08J9/10
CPC分类号： C08G18/61 , C08G18/4072 , C08G18/409 , C08G18/482 , C08G18/4837 , C08G18/4883 , C08G18/5021 , C08G18/506 , C08G18/632 , C08G18/638 , C08G2101/0025 , C08G2101/005 , C08G2101/0083 , C08J2205/10
摘要： To provide a method for producing a rigid polyurethane foam, whereby it is possible to reduce the density without causing deterioration in dimensional stability, and a rigid polyurethane foam.A method for producing a rigid polyurethane foam, which comprises a step of reacting a polyol having a hydroxyl value of from 200 to 800 mgKOH/g with a polyisocyanate compound in the presence of an amino-modified silicone, a catalyst, a blowing agent and a surfactant.
摘要翻译：为了提供硬质聚氨酯泡沫塑料的制造方法，可以降低密度而不会使尺寸稳定性下降，并且硬质聚氨酯泡沫体也可。一种硬质聚氨酯泡沫塑料的制造方法，其特征在于，在羟基值为200〜800mgKOH / g的多元醇与多异氰酸酯化合物在氨基改性硅酮，催化剂，发泡剂和表面活性剂。

2. 发明授权

US08258196B2 Method for producing rigid polyurethane foam, and rigid polyurethane foam 失效
标题翻译：硬质聚氨酯泡沫塑料的制造方法，硬质聚氨酯泡沫塑料
公开(公告)号：US08258196B2
公开(公告)日：2012-09-04
申请号：US12469178
申请日：2009-05-20
申请人： Katsuhiko Shimizu , Teruhiko Yasuda , Hiroshi Wada
发明人： Katsuhiko Shimizu , Teruhiko Yasuda , Hiroshi Wada
IPC分类号： C08G77/46
CPC分类号： C08G18/61 , C08G18/4072 , C08G18/409 , C08G18/482 , C08G18/4837 , C08G18/4883 , C08G18/5021 , C08G18/506 , C08G18/632 , C08G18/638 , C08G2101/0025 , C08G2101/005 , C08G2101/0083 , C08J2205/10
摘要： To provide a method for producing a rigid polyurethane foam, whereby it is possible to reduce the density without causing deterioration in dimensional stability, and a rigid polyurethane foam.A method for producing a rigid polyurethane foam, which comprises a step of reacting a polyol having a hydroxyl value of from 200 to 800 mgKOH/g with a polyisocyanate compound in the presence of an amino-modified silicone, a catalyst, a blowing agent and a surfactant.
摘要翻译：为了提供硬质聚氨酯泡沫塑料的制造方法，可以降低密度而不会使尺寸稳定性下降，并且硬质聚氨酯泡沫塑料。一种硬质聚氨酯泡沫塑料的制造方法，其特征在于，在羟基值为200〜800mgKOH / g的多元醇与多异氰酸酯化合物在氨基改性硅酮，催化剂，发泡剂和表面活性剂。

3. 发明申请

US20090234038A1 METHOD FOR PRODUCING RIGID POLYURETHANE FOAM 审中-公开
标题翻译：生产刚性聚氨酯泡沫的方法
公开(公告)号：US20090234038A1
公开(公告)日：2009-09-17
申请号：US12468963
申请日：2009-05-20
申请人： Hiroshi Wada , Hisashi Sato , Teruhiko Yasuda , Yasuhito Adachi , Katsuhiko Shimizu
发明人： Hiroshi Wada , Hisashi Sato , Teruhiko Yasuda , Yasuhito Adachi , Katsuhiko Shimizu
IPC分类号： C08J9/14
CPC分类号： C08G18/5021 , C08G18/4072 , C08G18/482 , C08G18/632 , C08G18/636 , C08G18/638 , C08G18/672 , C08G2101/0025 , C08G2101/005 , C08G2101/0083 , C08G18/48
摘要： To provide a method for producing a rigid polyurethane foam, whereby it is possible to obtain a rigid polyurethane foam which has a low density and good dimensional stability, and when a mixture of a polymer-dispersed polyol and a polyol for a rigid polyurethane foam to be used, is stored, the mixture is excellent in storage stability, so that a rigid polyurethane foam can be produced constantly.A method for producing a rigid polyurethane foam, which comprises reacting a polyol component (Z) with a polyisocyanate component in the presence of a blowing agent, a surfactant and a catalyst, wherein the polyol component (Z) has an average hydroxyl value of from 200 is to 800 mgKOH/g and contains a polymer-dispersed polyol (A) having polymer particles dispersed in a polyol by polymerizing a monomer having a polymerizable unsaturated group in a polyol (X), wherein the polyol (X) contains a polyether polyol, and the monomer having a polymerizable unsaturated group contains a fluorinated acrylate or a fluorinated methacrylate, and styrene.
摘要翻译：为了提供硬质聚氨酯泡沫塑料的制造方法，可以得到密度低，尺寸稳定性好的硬质聚氨酯泡沫塑料，将聚合物分散多元醇与硬质聚氨酯泡沫体用多元醇的混合物被使用，储存，混合物的储存稳定性优异，从而可以不断地生产硬质聚氨酯泡沫。一种硬质聚氨酯泡沫塑料的制造方法，其特征在于，在发泡剂，表面活性剂和催化剂的存在下，使多元醇成分（Z）与多异氰酸酯成分反应，其中多元醇成分（Z）的平均羟值为 200为800mgKOH / g，含有通过在多元醇（X）中聚合具有聚合性不饱和基团的单体而分散在多元醇中的聚合物粒子的聚合物分散多元醇（A），其中多元醇（X）含有聚醚多元醇，具有聚合性不饱和基团的单体含有氟化丙烯酸酯或氟化甲基丙烯酸酯和苯乙烯。

4. 发明授权

US08084562B2 Method for producing polymer-dispersed polyol 失效
标题翻译：制备聚合物分散多元醇的方法
公开(公告)号：US08084562B2
公开(公告)日：2011-12-27
申请号：US12469296
申请日：2009-05-20
申请人： Teruhiko Yasuda , Hisashi Sato , Hiroshi Wada , Yasuhito Adachi , Tomohiro Hayashi , Chitoshi Suzuki
发明人： Teruhiko Yasuda , Hisashi Sato , Hiroshi Wada , Yasuhito Adachi , Tomohiro Hayashi , Chitoshi Suzuki
IPC分类号： C08F2/44 , C08F20/44 , C08F283/06 , C08G18/63 , C08L75/04
CPC分类号： C08G18/632 , C08G18/4072 , C08G18/482 , C08G18/5021 , C08G18/506 , C08G18/636 , C08G18/638 , C08G18/672 , C08G2101/0025 , C08G2101/005 , C08G2101/0083 , C08L27/18 , C08L75/04 , C08G18/48 , C08L2666/04
摘要： To provide a method for producing a polymer-dispersed polyol which has high compatibility with a polyol for rigid polyurethane foams and is excellent in storage stability and which provides good heat-insulating performance when it is formed into a rigid polyurethane foam. Also a method for producing a polymer-dispersed polyol for rigid polyurethane foams, having polymer particles dispersed in a polyol, which comprises polymerizing a monomer having a polymerizable unsaturated group in a polyol (X), wherein the polyol (X) contains a polyether polyol (Y) having an oxyethylene group content of at least 10 mass %, and the monomer having a polymerizable unsaturated group contains a fluorinated acrylate or a fluorinated methacrylate.
摘要翻译：提供一种与硬质聚氨酯泡沫的多元醇高相容性的聚合物分散多元醇的制造方法，其储存稳定性优异，在形成硬质聚氨酯泡沫体时，具有良好的隔热性能。另外，制备聚合物分散在多元醇中的聚合物颗粒的聚合物分散多元醇的方法，其中聚合物颗粒分散在多元醇中，其包括在多元醇（X）中聚合具有可聚合不饱和基团的单体，其中多元醇（X）含有聚醚多元醇（Y），具有至少10质量％的氧化乙烯含量，具有聚合性不饱和基团的单体含有氟化丙烯酸酯或氟化甲基丙烯酸酯。

5. 发明申请

US20090227696A1 METHOD FOR PRODUCING POLYMER-DISPERSED POLYOL 失效
标题翻译：生产聚合物分散多元醇的方法
公开(公告)号：US20090227696A1
公开(公告)日：2009-09-10
申请号：US12469296
申请日：2009-05-20
申请人： Teruhiko YASUDA , Hisashi Sato , Hiroshi Wada , Yasuhito Adachi , Tomohiro Hayashi , Chitoshi Suzuki
发明人： Teruhiko YASUDA , Hisashi Sato , Hiroshi Wada , Yasuhito Adachi , Tomohiro Hayashi , Chitoshi Suzuki
IPC分类号： C08L75/04
CPC分类号： C08G18/632 , C08G18/4072 , C08G18/482 , C08G18/5021 , C08G18/506 , C08G18/636 , C08G18/638 , C08G18/672 , C08G2101/0025 , C08G2101/005 , C08G2101/0083 , C08L27/18 , C08L75/04 , C08G18/48 , C08L2666/04
摘要： To provide a method for producing a polymer-dispersed polyol which has high compatibility with a polyol for rigid polyurethane foams and is excellent in storage stability and which provides good heat-insulating performance when it is formed into a rigid polyurethane foam.A method for producing a polymer-dispersed polyol for rigid polyurethane foams, having polymer particles dispersed in a polyol, which comprises polymerizing a monomer having a polymerizable unsaturated group in a polyol (X), wherein the polyol (X) contains a polyether polyol (Y) having an oxyethylene group content of at least 10 mass %, and the monomer having a polymerizable unsaturated group contains a fluorinated acrylate or a fluorinated methacrylate.
摘要翻译：提供一种与硬质聚氨酯泡沫的多元醇高相容性的聚合物分散多元醇的制造方法，其储存稳定性优异，在形成硬质聚氨酯泡沫体时，具有良好的隔热性能。一种聚合物分散多元醇用于硬质聚氨酯泡沫体的制造方法，其具有分散在多元醇中的聚合物粒子，其包括在多元醇（X）中聚合具有聚合性不饱和基团的单体，其中所述多元醇（X）含有聚醚多元醇 Y），具有至少10质量％的氧乙烯基含量，并且具有聚合性不饱和基团的单体含有氟化丙烯酸酯或氟化甲基丙烯酸酯。

6. 发明授权

US08507036B2 Process for producing rigid open-cell foam 失效
标题翻译：生产刚性开孔泡沫的方法
公开(公告)号：US08507036B2
公开(公告)日：2013-08-13
申请号：US13526162
申请日：2012-06-18
申请人： Katsuhiko Shimizu , Hiroshi Wada , Yoshinori Toyota
发明人： Katsuhiko Shimizu , Hiroshi Wada , Yoshinori Toyota
IPC分类号： B05D1/02
CPC分类号： C08G18/482 , C08G18/1825 , C08G18/1833 , C08G18/3206 , C08G18/4816 , C08G18/4829 , C08G18/4833 , C08G18/4837 , C08G18/4841 , C08G18/5021 , C08G18/6674 , C08G18/7664 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： To provide a process capable of producing a light-weight rigid open-cell foam by a spraying method using mainly or solely water as a blowing agent, wherein a polyol system liquid is excellent in storage stability even when the blowing agent is used in a large amount, and the foam is excellent in dimensional stability without sagging and capable of forming a uniform thermal insulation layer having an excellent appearance for the purpose of constructing a whole constructions.
摘要翻译：为了提供一种能够通过主要或单独的水作为发泡剂的喷雾法生产轻质刚性开孔泡沫的方法，其中多元醇系液体即使在发泡剂使用时也具有优异的储存稳定性量，并且泡沫体在尺寸稳定性方面优异而没有下垂，并且能够形成具有优异外观的均匀保温层，以构成整个结构。

7. 发明申请

US20120251727A1 PROCESS FOR PRODUCING RIGID OPEN-CELL FOAM 失效
标题翻译：生产刚性开口泡沫的方法
公开(公告)号：US20120251727A1
公开(公告)日：2012-10-04
申请号：US13526162
申请日：2012-06-18
申请人： Katsuhiko Shimizu , Hiroshi Wada , Yoshinori Toyota
发明人： Katsuhiko Shimizu , Hiroshi Wada , Yoshinori Toyota
IPC分类号： B05D5/00
CPC分类号： C08G18/482 , C08G18/1825 , C08G18/1833 , C08G18/3206 , C08G18/4816 , C08G18/4829 , C08G18/4833 , C08G18/4837 , C08G18/4841 , C08G18/5021 , C08G18/6674 , C08G18/7664 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： To provide a process capable of producing a light-weight rigid open-cell foam by a spraying method using mainly or solely water as a blowing agent, wherein a polyol system liquid is excellent in storage stability even when the blowing agent is used in a large amount, and the foam is excellent in dimensional stability without sagging and capable of forming a uniform thermal insulation layer having an excellent appearance for the purpose of constructing a whole constructions.
摘要翻译：为了提供一种能够通过主要或单独的水作为发泡剂的喷雾法生产轻质刚性开孔泡沫的方法，其中多元醇系液体即使在发泡剂使用时也具有优异的储存稳定性量，并且泡沫体在尺寸稳定性方面优异而没有下垂，并且能够形成具有优异外观的均匀保温层，以构成整个结构。

8. 发明申请

US20120088851A1 PROCESS FOR PRODUCING POLYETHER POLYOL AND PROCESS FOR PRODUCING RIGID FOAMED SYNTHETIC RESIN USING SAME 失效
标题翻译：制造聚醚多元醇的方法和使用其制造刚性泡沫合成树脂的方法
公开(公告)号：US20120088851A1
公开(公告)日：2012-04-12
申请号：US13326998
申请日：2011-12-15
申请人： Katsuhiko Shimizu , Tomohiro Hayashi , Hiroshi Wada , Yoshinori Toyota
发明人： Katsuhiko Shimizu , Tomohiro Hayashi , Hiroshi Wada , Yoshinori Toyota
IPC分类号： C08J9/35 , C08L75/08 , C07C215/10 , C08J9/04
CPC分类号： C08G65/2612 , C08G18/4072 , C08G18/5033 , C08G18/632 , C08G18/636 , C08G18/637 , C08G18/8175 , C08G2101/0025
摘要： Provided is a process for producing a polyether polyol which can form low viscosity rigid foamed synthetic resins excellent in strength, dimensional stability and flame retardancy, can give a low viscosity polyol system solution containing water instead of HFCs as a blowing agent with good miscibility with isocyanate compounds and can form good rigid foamed synthetic resins by spraying.A polyether polyol (A) is produced by reacting a phenol component (molar ratio 1) selected from phenol and phenol derivatives having a hydrogen atom at one or more ortho-positions to the phenolic hydroxyl group, an aldehyde component (molar ratio 0.3 to 0.9) selected from formaldehyde and acetoaldehyde and an alkanolamine component (molar ratio 1.5 to 3.5) selected from monoethanolamine, diethanolamine and 1-amino-2-propanol and then adding an alkylene oxide to the resulting reaction product.
摘要翻译：提供一种能够形成强度，尺寸稳定性和阻燃性优异的低粘度刚性发泡合成树脂的聚醚多元醇的方法，可以得到含有水的低粘度多元醇体系溶液，而不是HFC，作为与异氰酸酯具有良好混溶性的发泡剂化合物，并可通过喷涂形成良好的刚性发泡合成树脂。聚醚多元醇（A）通过使选自苯酚的酚成分（摩尔比1）和在一个或多个邻位具有氢原子的酚衍生物与酚羟基反应，醛成分（摩尔比为0.3〜0.9 ）和选自单乙醇胺，二乙醇胺和1-氨基-2-丙醇的链烷醇胺组分（摩尔比为1.5-3.5），然后向所得反应产物中加入烯化氧。

9. 发明授权

US08623933B2 Process for producing polyether polyol and process for producing rigid foamed synthetic resin using same 失效
标题翻译：制备聚醚多元醇的方法和使用该聚醚多元醇制备刚性发泡合成树脂的方法
公开(公告)号：US08623933B2
公开(公告)日：2014-01-07
申请号：US13326998
申请日：2011-12-15
申请人： Katsuhiko Shimizu , Tomohiro Hayashi , Hiroshi Wada , Yoshinori Toyota
发明人： Katsuhiko Shimizu , Tomohiro Hayashi , Hiroshi Wada , Yoshinori Toyota
IPC分类号： C08G18/50 , C08J9/04 , C08J9/08 , C07C213/00 , C07C213/06
CPC分类号： C08G65/2612 , C08G18/4072 , C08G18/5033 , C08G18/632 , C08G18/636 , C08G18/637 , C08G18/8175 , C08G2101/0025
摘要： A process for producing a polyether polyol which can form low viscosity rigid foamed synthetic resins excellent in strength, dimensional stability and flame retardancy, can give a low viscosity polyol system solution containing water instead of HFCs as a blowing agent with good miscibility with isocyanate compounds and can form good rigid foamed synthetic resins by spraying, which polyether polyol is produced by reacting a phenol component (molar ratio 1) selected from phenol and phenol derivatives having a hydrogen atom at one or more ortho-positions to the phenolic hydroxyl group, an aldehyde component (molar ratio 0.3 to 0.9) selected from formaldehyde and acetoaldehyde and an alkanolamine component (molar ratio 1.5 to 3.5) selected from monoethanolamine, diethanolamine and 1-amino-2-propanol and then adding an alkylene oxide to the resulting reaction product.
摘要翻译：可以形成能够形成强度，尺寸稳定性和阻燃性优异的低粘度刚性发泡合成树脂的聚醚多元醇的方法，可以得到含有水的低粘度多元醇体系溶液代替与异氰酸酯化合物具有良好混溶性的发泡剂的HFC，可以通过喷雾形成良好的刚性发泡合成树脂，该聚醚多元醇通过使选自苯酚组分（摩尔比1）和酚羟基在一个或多个邻位的氢原子的酚衍生物与酚羟基反应来制备，醛选自甲醛和乙醛的组分（摩尔比为0.3至0.9）和选自单乙醇胺，二乙醇胺和1-氨基-2-丙醇的链烷醇胺组分（摩尔比为1.5至3.5），然后向所得反应产物中加入烯化氧。

10. 发明申请

US20110060063A1 METHOD FOR PRODUCING RIGID POLYURETHANE FOAM 审中-公开
标题翻译：生产刚性聚氨酯泡沫的方法
公开(公告)号：US20110060063A1
公开(公告)日：2011-03-10
申请号：US12944809
申请日：2010-11-12
申请人： Tatsuya YABUNO , Katsuhiko Shimizu , Hiroshi Wada , Tomohiro Hayashi
发明人： Tatsuya YABUNO , Katsuhiko Shimizu , Hiroshi Wada , Tomohiro Hayashi
IPC分类号： C08G18/42
CPC分类号： C08G18/632 , C08G18/4072 , C08G18/636 , C08G18/638 , C08G2101/0025 , C08G2101/0083
摘要： To provide a method for producing a rigid polyurethane foam using a polymer-dispersed polyol, which has high compatibility with a polyol to be used and is excellent in the storage stability, and with which good heat insulating properties can be obtained when it is formed into a foam.A method for producing a rigid polyurethane foam, which comprises reacting a polyol (Z) with a polyisocyanate in the presence of a blowing agent, a surfactant and a catalyst, wherein the (Z) is obtained by mixing a polyol (Z1) with a polymer-dispersed polyol (A) and has an average hydroxy value of from 200 to 800 mgKOH/g. The (A) is one having a monomer polymerized in a polyol (X), the (X) contains a polyether polyol (Y), the (Y) has an oxyethylene group content of at least 15 mass % and contains a polyol Y1 having a hydroxy value of from 200 to 800 mgKOH/g and a polyol Y2 having a hydroxy value of from 5 to 84 mgKOH/g, and the monomer contains a fluorinated acrylate or a fluorinated methacrylate.
摘要翻译：提供一种使用与所使用的多元醇高相容性的聚合物分散多元醇制造硬质聚氨酯泡沫体的方法，并且储存稳定性优异，并且当其形成时可获得良好的隔热性能泡沫。一种硬质聚氨酯泡沫塑料的制造方法，其特征在于，在发泡剂，表面活性剂和催化剂的存在下，使多元醇（Z）与多异氰酸酯反应，其中（Z）是通过将多元醇（Z1）与聚合物分散多元醇（A），平均羟值为200〜800mgKOH / g。（A）是在多元醇（X）中聚合的单体，（X）含有聚醚多元醇（Y），（Y）的氧化乙烯基含量为15质量％以上，含有多元醇Y1，羟值为200〜800mgKOH / g，羟基值为5〜84mgKOH / g的多元醇Y2，单体含氟化丙烯酸酯或氟化甲基丙烯酸酯。

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