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1. 发明授权

US07868126B2 Process for producing polyester, polyester produced using said process, and polyester molded product 有权
标题翻译：使用该方法制造聚酯，聚酯的方法和聚酯模制品
公开(公告)号：US07868126B2
公开(公告)日：2011-01-11
申请号：US11795556
申请日：2005-06-24
申请人： Katsuhiko Kageyama , Tooru Kitagawa , Kenichi Funaki , Masaki Fuchikami , Kazuo Katayose , Takahiro Nakajima , Toshiyuki Tsuchiya , Satoru Nakagawa , Fumikazu Yoshida , Haruhiko Kohyama , Naoki Watanabe
发明人： Katsuhiko Kageyama , Tooru Kitagawa , Kenichi Funaki , Masaki Fuchikami , Kazuo Katayose , Takahiro Nakajima , Toshiyuki Tsuchiya , Satoru Nakagawa , Fumikazu Yoshida , Haruhiko Kohyama , Naoki Watanabe
IPC分类号： C08G63/00
CPC分类号： C08G63/84 , C08J5/18 , C08J2367/02 , D01F6/62 , Y10T428/13 , Y10T428/1352 , Y10T428/162 , Y10T428/249921
摘要： This invention provides a polyester and a polyester molded product, which, while maintaining color tone, transparency, and thermal stability, can realize a high polycondensation rate, are less likely to cause the production of polycondensation catalyst-derived undesired materials, and can simultaneously meet both quality and cost effectiveness requirements, which can exhibit the characteristic features, for example, in the fields of ultrafine fibers, high transparent films for optical use, or ultrahigh transparent molded products. These advantages can be realized by using, in the production of a polyester in the presence of an aluminum compound-containing polyester polycondensation catalyst, an aluminum compound having an absorbance of not more than 0.0132 as measured in the form of an aqueous aluminum compound solution, prepared by dissolving the aluminum compound in pure water to give a concentration of 2.7 g/liter in terms of the amount of aluminum element, under conditions of cell length 1 cm and wavelength 680 nm.
摘要翻译：本发明提供一种聚酯和聚酯成型体，其在保持色调，透明性和热稳定性的同时，可以实现高缩聚率，不太可能导致产生缩聚催化剂衍生的不需要的材料，并且可以同时满足质量和成本效益要求，其可以表现出特征，例如在超细纤维，用于光学用途的高透明膜或超高透明模制品的领域。这些优点可以通过在含铝化合物的聚酯缩聚催化剂的存在下制造聚酯，通过以铝化合物水溶液的形式测定的吸光度不大于0.0132的铝化合物来实现，通过将铝化合物溶解在纯水中，在细胞长度为1cm和波长680nm的条件下，以铝元素的量计，浓度为2.7g /升。

2. 发明申请

US20080249280A1 Process for Producing Polyester, Polyester Produced Using Said Process, and Polyester Molded Product 有权
标题翻译：使用所述方法生产聚酯，聚酯的方法和聚酯模塑产品的方法
公开(公告)号：US20080249280A1
公开(公告)日：2008-10-09
申请号：US11795556
申请日：2005-06-24
申请人： Katsuhiko Kageyama , Tooru Kitagawa , Kenichi Funaki , Masaki Fuchikami , Kazuo Katayose , Takahiro Nakajima , Toshiyuki Tsuchiya , Satoru Nakagawa , Fumikazu Yoshida , Haruhiko Kohyama , Naoki Watanabe
发明人： Katsuhiko Kageyama , Tooru Kitagawa , Kenichi Funaki , Masaki Fuchikami , Kazuo Katayose , Takahiro Nakajima , Toshiyuki Tsuchiya , Satoru Nakagawa , Fumikazu Yoshida , Haruhiko Kohyama , Naoki Watanabe
IPC分类号： C08G63/00
CPC分类号： C08G63/84 , C08J5/18 , C08J2367/02 , D01F6/62 , Y10T428/13 , Y10T428/1352 , Y10T428/162 , Y10T428/249921
摘要： This invention provides a polyester and a polyester molded product, which, while maintaining color tone, transparency, and thermal stability, can realize a high polycondensation rate, are less likely to cause the production of polycondensation catalyst-derived undesired materials, and can simultaneously meet both quality and cost effectiveness requirements, which can exhibit the characteristic features, for example, in the fields of ultrafine fibers, high transparent films for optical use, or ultrahigh transparent molded products. These advantages can be realized by using, in the production of a polyester in the presence of an aluminum compound-containing polyester polycondensation catalyst, an aluminum compound having an absorbance of not more than 0.0132 as measured in the form of an aqueous aluminum compound solution, prepared by dissolving the aluminum compound in pure water to give a concentration of 2.7 g/liter in terms of the amount of aluminum element, under conditions of cell length 1 cm and wavelength 680 nm.
摘要翻译：本发明提供一种聚酯和聚酯成型体，其在保持色调，透明性和热稳定性的同时，可以实现高缩聚率，不太可能导致产生缩聚催化剂衍生的不需要的材料，并且可以同时满足质量和成本效益要求，其可以表现出特征，例如在超细纤维，用于光学用途的高透明膜或超高透明模制品的领域。这些优点可以通过在含铝化合物的聚酯缩聚催化剂的存在下制造聚酯，通过以铝化合物水溶液的形式测定的吸光度不大于0.0132的铝化合物来实现，通过将铝化合物溶解在纯水中，在细胞长度为1cm和波长680nm的条件下，以铝元素的量计，浓度为2.7g /升。

3. 发明申请

US20070106055A1 Polyester polymerization catalyst, polyester produced therewith and process for producing the polyester 审中-公开
标题翻译：聚酯聚合催化剂，由其制造的聚酯和聚酯的制造方法
公开(公告)号：US20070106055A1
公开(公告)日：2007-05-10
申请号：US10588652
申请日：2005-02-08
申请人： Katsuhiko Kageyama , Kenichi Funaki , Masaki Fuchikami , Satoru Nakagawa , Kazuo Katayose , Takahiro Nakajima , Naoki Watanabe , Fumikazu Yoshida , Tetsumori Atsuchi , Shoichi Gyobu , Haruo Matsumoto , Ryuichi Murashige , Gaku Maruyama , Yoshiko Akitomo , Hideki Shimizu
发明人： Katsuhiko Kageyama , Kenichi Funaki , Masaki Fuchikami , Satoru Nakagawa , Kazuo Katayose , Takahiro Nakajima , Naoki Watanabe , Fumikazu Yoshida , Tetsumori Atsuchi , Shoichi Gyobu , Haruo Matsumoto , Ryuichi Murashige , Gaku Maruyama , Yoshiko Akitomo , Hideki Shimizu
IPC分类号： C08G63/00
CPC分类号： C08G63/84 , C08G63/87
摘要： The invention provides a polyester produced in the presence of a polycondensation catalyst comprising at least one compound selected from a group consisting of aluminum compounds and at least one compound selected from a group consisting of phosphorus compounds and being excellent in color tone, thermal stability, and transparency and improved in terms of insoluble particles. Particularly, the invention provides a polyester in which the content of an aluminum containing insoluble particles in the polyester is 3500 ppm or lower and a polyester which has a haze value of 2% or lower when being formed into a monoaxially oriented film. The aluminum catalyst for attaining these characteristics and properties may be polyester polymerization catalyst obtained by mixing an aluminum compound and a phosphorus compound in a solvent and has specified spectral characteristics in the side measurement of 31P-NMR spectrum and 27Al-NMR spectrum.
摘要翻译：本发明提供一种在缩聚催化剂存在下制备的聚酯，其包含至少一种选自铝化合物和至少一种选自磷化合物的化合物并且色调优异，热稳定性和透明度和不溶性颗粒方面的改进。特别地，本发明提供一种聚酯，其中在形成单轴取向膜时，聚酯中含有不溶性的铝的含量为3500ppm以下，聚酯的雾度值为2％以下。用于获得这些特性和性质的铝催化剂可以是通过在溶剂中混合铝化合物和磷化合物而获得的聚酯聚合催化剂，并且在侧谱测定中具有特定的光谱特性， Al-NMR光谱。

4. 发明授权

US07132383B2 Polymerization catalyst for polyester, polyester produced with the same, and process for producing polyester 有权
标题翻译：用于聚酯的聚合催化剂，与此相同的聚酯，以及聚酯的制造方法
公开(公告)号：US07132383B2
公开(公告)日：2006-11-07
申请号：US10363648
申请日：2001-09-10
申请人： Takahiro Nakajima , Kenichi Tsukamoto , Shoichi Gyobu , Fumikazu Yoshida , Maki Sato , Naoki Watanabe , Katsuhiko Kageyama , Mitsuyoshi Kuwata , Nobuo Moriyama , Haruo Matsumoto , Yoshitomo Ikehata , Yoshinao Matsui , Masaou Matsuda , Munekazu Okuhara , Hiroki Fukuda
发明人： Takahiro Nakajima , Kenichi Tsukamoto , Shoichi Gyobu , Fumikazu Yoshida , Maki Sato , Naoki Watanabe , Katsuhiko Kageyama , Mitsuyoshi Kuwata , Nobuo Moriyama , Haruo Matsumoto , Yoshitomo Ikehata , Yoshinao Matsui , Masaou Matsuda , Munekazu Okuhara , Hiroki Fukuda
IPC分类号： B01J31/00
CPC分类号： D01F6/62 , C08G63/82 , C08G63/83 , C08G63/84 , C08G63/87
摘要： A polymerization catalyst for polyester production which contains neither a germanium compound nor an antimony compound as a major component. It contains aluminum as the main metallic ingredient, has excellent catalytic activity, and gives a polyester which is effectively inhibited from suffering thermal degradation, during melt molding, without deactivating or removing the catalyst, and is excellent in thermal stability, stability to thermal oxidation, and hydrolytic resistance. The polymerization catalyst contains as a first metallic ingredient at least one member selected among aluminum and compounds thereof and further contains a phosphorus compound represented by a specific chemical formula. The polyester produced with this catalyst is usable as fibers, films, sheets, various moldings including hollow moldings, etc.
摘要翻译：用于聚酯生产的聚合催化剂，既不含锗化合物也不含锑化合物作为主要成分。它含有铝作为主要的金属成分，具有优异的催化活性，并且在熔融成型期间得到有效抑制热降解的聚酯，而不会使催化剂失活或除去，并且热稳定性，热氧化稳定性优异，和耐水解性。聚合催化剂含有选自铝及其化合物中的至少一种元素作为第一金属成分，并且还含有由特定化学式表示的磷化合物。使用该催化剂制造的聚酯可用作纤维，薄膜，片材，各种模制品，包括中空模制品等。

5. 发明授权

US5173366A Electrically conductive fibers, apparatus and method for the production thereof 失效
标题翻译：导电纤维，其制造方法及其制造方法
公开(公告)号：US5173366A
公开(公告)日：1992-12-22
申请号：US789539
申请日：1991-11-08
申请人： Hideyuki Mitamura , Fumikazu Yoshida , Tatsuo Shimura
发明人： Hideyuki Mitamura , Fumikazu Yoshida , Tatsuo Shimura
IPC分类号： D01D5/34 , D01F1/09 , D01F8/04
CPC分类号： D01F1/09 , D01D5/34 , D01F8/04 , Y10T428/2929 , Y10T428/2931
摘要： Electrically conductive conjugate fibers having a diameter less than 50.mu.m. The fibers include a thermoplastic sheath and a low-melting metal core, with the core occupying 0.2 to 50% of the sectional area of the fiber. The sectional area of the core varies by less than 25% in the longitudinal direction, and the total length of the discontinuous portions of the core is 5 cm or less per meter. The fibers can be produced with a conjugate spinning nozzle. The low-melting metal is provided to the nozzle from the closed fusion tank located at a position below the spinning nozzle. The metal is supplied to the spinning nozzle by means of pressure from inert gas, which is supplied to an upper space of the fusion tank. The level of metal in the fusion tank is maintained substantially constant, and the pressure of the gas is controlled so as to maintain a pressure variation of 0.1 kg/cm.sup.2 or less.
摘要翻译：直径小于50微米的导电复合纤维。纤维包括热塑性护套和低熔点金属芯，其中芯占纤维截面面积的0.2-50％。芯的截面积沿纵向变化小于25％，芯的不连续部分的总长度为每米5厘米或更小。纤维可以用复合纺丝喷嘴生产。低熔点金属从位于纺丝喷嘴下方位置的封闭式熔化罐提供给喷嘴。通过来自惰性气体的压力将金属供给到纺丝喷嘴，惰性气体被供应到熔化罐的上部空间。熔池中的金属含量保持基本恒定，并且控制气体的压力以保持0.1kg / cm 2以下的压力变化。

6. 发明授权

US4600743A Antistatic fiber containing polyoxyalkylene glycol 失效
标题翻译：含聚氧亚烷基二醇的抗静电纤维
公开(公告)号：US4600743A
公开(公告)日：1986-07-15
申请号：US600054
申请日：1984-04-13
申请人： Tatsuhiko Shizuki , Kaoru Ban , Fumikazu Yoshida , Masakatsu Ohguchi
发明人： Tatsuhiko Shizuki , Kaoru Ban , Fumikazu Yoshida , Masakatsu Ohguchi
IPC分类号： D01F6/92 , D01F1/09 , C08L67/02 , C08L77/06
CPC分类号： D01F1/09
摘要： An antistatic fiber obtained by melt spinning of a fiber-forming thermoplastic polymer containing at least one of polyoxyalkylene glycol and its derivatives in an amount of not less than 0.5% by weight, characterized in that said fiber has a half life time of electric charge leakage of not more than 150 seconds before and after treatment with a weight decreasing agent and, when treated with a weight decreasing agent, provides a number of streaks arranged in parallel in the lengthwise direction at the surface.
摘要翻译：通过将含有至少一种聚氧亚烷基二醇及其衍生物的成纤热塑性聚合物熔体纺丝得到的抗静电纤维的量不小于0.5重量％，其特征在于所述纤维具有电荷泄漏的半衰期在用减轻剂处理之前和之后不超过150秒，并且当用减轻剂处理时，提供在表面上沿长度方向平行布置的多条条纹。

7. 发明授权

US5248468A Method of making electrically conductive fibers 失效
标题翻译：制造导电纤维的方法
公开(公告)号：US5248468A
公开(公告)日：1993-09-28
申请号：US786170
申请日：1991-10-31
申请人： Hideyuki Mitamura , Fumikazu Yoshida , Tatsuo Shimura
发明人： Hideyuki Mitamura , Fumikazu Yoshida , Tatsuo Shimura
IPC分类号： D01D5/34 , D01F1/09 , D01F8/04
CPC分类号： D01D5/34 , D01F1/09 , D01F8/04
摘要： Electrically conductive conjugate fibers having a diameter less than 50 fm. The fibers include a thermoplastic sheath and a low-melting metal core, with the core occupying 0.2 to 50% of the sectional area of the fiber. The sectional area of the core varies by less than 25% in the longitudinal direction, and the total length of the discontinuous portions of the core is 5 cm or less per meter. The fibers can be produced with a conjugate spinning nozzle. The low-melting metal is provided to the nozzle from a closed fusion tank located at a position below the spinning nozzle. The metal is supplied to the spinning nozzle by means of pressure from inert gas, which is supplied to an upper space of the fusion tank. The level of metal in the fusion tank is maintained substantially constant, and the pressure of the gas is controlled so as to maintain a pressure variation of 0.1 kg/cm.sup.2 or less.
摘要翻译：直径小于50微米的导电复合纤维。纤维包括热塑性护套和低熔点金属芯，其中芯占纤维截面面积的0.2-50％。芯的截面积沿纵向变化小于25％，芯的不连续部分的总长度为每米5厘米或更小。纤维可以用复合纺丝喷嘴生产。将低熔点金属从位于纺丝喷嘴下方位置的封闭的熔化罐提供给喷嘴。通过来自惰性气体的压力将金属供给到纺丝喷嘴，惰性气体被供应到熔化罐的上部空间。熔池中的金属含量保持基本恒定，并且控制气体的压力以保持0.1kg / cm 2以下的压力变化。

8. 发明授权

US4940560A Process for preparing antistatic fiber 失效
标题翻译：抗静电纤维制备方法
公开(公告)号：US4940560A
公开(公告)日：1990-07-10
申请号：US186664
申请日：1988-04-25
申请人： Tatsuhiko Shizuki , Kaoru Ban , Fumikazu Yoshida , Masakatsu Ohguchi
发明人： Tatsuhiko Shizuki , Kaoru Ban , Fumikazu Yoshida , Masakatsu Ohguchi
IPC分类号： D01F6/92 , D01F1/09
CPC分类号： D01F1/09
摘要： An antistatic fiber obtained by melt spinning of a fiber-forming thermoplastic polymer containing at least one of polyoxyalkylene glycol and its derivatives in an amount of not less than 0.5% by weight, characterized in that said fiber has a half life time of electric charge leakage of not more than 150 seconds before and after treatment with a weight decreasing agent and, when treated with a weight decreasing agent, provides a number of streaks arranged in parallel in the lengthwise direction at the surface.

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