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    • 3. 发明申请
    • METHOD AND SYSTEM FOR CONCENTRATING WASTE SULPHURIC ACIDS FROM NITRATION PROCESSES
    • 从硝化过程中浓缩废硫酸的方法和系统
    • US20100233069A1
    • 2010-09-16
    • US12305902
    • 2007-06-20
    • Ulrich WalterGottfried Dichtl
    • Ulrich WalterGottfried Dichtl
    • C01B17/82B01D3/40
    • C01B17/94B01D3/148B01D3/40
    • Disclosed is a method for recovering diluted waste sulfuric acid containing impurities from nitration processes, a highly concentrated nitric acid required in the nitration process being produced in association with the nitration process by means of extractive rectification with concentrated sulfuric acid which is re-concentrated in order to be reutilized. According to the inventive method, the waste sulfuric acid from the nitration process is fed to the top of a first, indirectly heated stripping column, optionally together with another waste sulfuric acid in the form of a DNT washing acid, and is divided into an overhead product containing nitric acid and nitro-organic compounds as well as a prepurified sulfuric acid in the bottom product. The prepurified sulfuric acid withdrawn from the bottom of the first stripping column is fed to the top of a second, serially connected additional indirectly heated stripping column, into the bottom zone of which another waste sulfuric acid is fed in the form of a diluted sulfuric acid recovered from the nitric acid concentration system such that the prepurified sulfuric acid from the first stripping column is further purified in the second stripping column and is preconcentrated along with the diluted sulfuric acid recovered from the extractive rectification of nitric acid.
    • 公开了一种从硝化过程中回收稀释的含有杂质的废硫酸的方法,硝化过程中所需的高浓度硝酸是通过与浓硫酸进行萃取精馏相结合的硝化过程制备的,该浓硫酸按顺序重新浓缩 被重新利用。 根据本发明的方法,将来自硝化过程的废硫酸进料到第一间接加热的汽提塔的顶部,任选地与另一种DNT洗涤酸形式的废硫酸一起分配成塔顶 含有硝酸和硝基有机化合物的产品以及底部产物中的预硫化硫酸。 将从第一汽提塔底部排出的预纯化硫酸进料到第二个连续连续的另外间接加热的汽提塔的顶部,进入其中另一个废硫酸以稀硫酸的形式进料的底部区域 从硝酸浓缩系统回收,使得来自第一汽提塔的预纯化硫酸在第二汽提塔中进一步纯化,并与从硝酸萃取精馏中回收的稀硫酸一起预浓缩。
    • 10. 发明授权
    • Nozzle for spraying liquids
    • 用于喷涂液体的喷嘴
    • US4773597A
    • 1988-09-27
    • US129948
    • 1987-12-03
    • Wolfgang DittrichIngomar FischerRainer LingnerOlaf PagelHeinrich PetzoldUwe RohlandUlrich Walter
    • Wolfgang DittrichIngomar FischerRainer LingnerOlaf PagelHeinrich PetzoldUwe RohlandUlrich Walter
    • B05B7/04B05B7/10
    • B05B7/0466
    • A nozzle for spraying liquids is provided, especially high viscosity liquid media used in the food and chemical industries. The nozzle finds particular use in fluidized bed spray granulators. A fine spray of high viscosity liquid media is attained. A nozzle head is arranged inside a nozzle housing. The nozzle head has a cylindrical portion terminating in a truncated, cone-shaped portion. A plurality of first flow ducts are arranged like the threads on a screw along the surface of the cylindrical portion for guiding a pressure medium such as air. A plurality of second ducts are arranged between the cylindrical portion and truncated, cone-shaped portion of the nozzle head and supply high viscosity liquid medium to the pressure medium exiting the downstream ends of the plurality of first ducts. The mixing high viscosity liquid and pressure media are supplied to a nozzle outlet via the truncated, cone-shaped portion of the nozzle head, which is mated by the inner surface of a nozzle cap, both of which are hardened and polished to a mirror-finish.
    • 提供用于喷射液体的喷嘴,特别是用于食品和化学工业中的高粘度液体介质。 喷嘴在流化床喷雾造粒机中特别有用。 获得高粘度液体介质的细喷雾。 喷嘴头布置在喷嘴壳体内。 喷嘴头具有终止于截头圆锥形部分的圆柱形部分。 多个第一流动管道沿着圆柱形部分的表面如螺纹布置在螺钉上,用于引导诸如空气的压力介质。 多个第二管道布置在喷嘴头的圆柱形部分和截锥形部分之间,并将高粘度液体介质供应到离开多个第一管道下游端的压力介质。 混合的高粘度液体和压力介质通过喷嘴头的截头圆锥形部分供应到喷嘴出口,喷嘴头的锥形部分由喷嘴盖的内表面配合,两者均被硬化和抛光到镜面 - 完。