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1. 发明授权

US5292971A Flourine-substituted vicinal and method for their preparation, and their use 失效
标题翻译：含氟取代的邻位及其制备方法及其应用
公开(公告)号：US5292971A
公开(公告)日：1994-03-08
申请号：US17687
申请日：1993-02-12
申请人： Jurgen Kulpe , Heinz Strutz
发明人： Jurgen Kulpe , Heinz Strutz
IPC分类号： C07C29/46 , C07C35/48 , C07C35/52 , C08G63/682 , C07C35/29
CPC分类号： C07C35/52 , C08G63/6826
摘要： Fluorine-substituted vicinal glycols of the formula ##STR1## in which the substituents R.sub.1 to R.sub.4, independently of one another, have the following meanings: R.sub.1 to R.sub.4 =H, fluorine, C.sub.1 - to C.sub.18 -alkyl in which some or all of the hydrogens may be substituted by fluorine, and at least one of the substituents R.sub.1 to R.sub.4 is a completely fluorinated alkyl or an alkyl of the formula--(CH.sub.2).sub.m --(C.sub.n F.sub.2n+1),in which m is 1 or 2, and n is an integer from 1 to 17, and x is 0 or 1.Furthermore, a method for the preparation of the fluorinated vicinal glycols is described. If the fluorinated vicinal glycols are condensed together with dicarboxylic acids, products having enhanced thermal stability are obtained.
摘要翻译：取代基R 1至R 4彼此独立地具有下列含义的式“IMAGE”的氟取代的连位二醇，其中R 1至R 4 = H，氟，C 1 -C 18烷基，其中部分或全部氢可以被氟取代，并且至少一个取代基R 1至R 4是完全氟化的烷基或式 - （CH 2）m - （C n F 2n + 1）的烷基，其中m是1或2，n 是1〜17的整数，x为0或1.此外，描述了制备氟化连二醇的方法。如果氟化连二醇与二羧酸一起冷凝，则获得具有增强的热稳定性的产物。

2. 发明授权

US5712350A Oxidation of polyarylene sulfides 失效
标题翻译：聚亚芳基硫化物的氧化
公开(公告)号：US5712350A
公开(公告)日：1998-01-27
申请号：US591162
申请日：1996-01-16
申请人： Dietrich Fleischer , Heinz Strutz , Jurgen Kulpe , Andreas Schleicher
发明人： Dietrich Fleischer , Heinz Strutz , Jurgen Kulpe , Andreas Schleicher
IPC分类号： C08G75/0236 , C08G75/0295 , C08G75/06 , C08G75/20 , C08F283/00 , C08L81/00
CPC分类号： C08G75/0295 , C08G75/0236 , C08G75/20
摘要： Process for oxidizing a polymer containing thioether groups, in which the polymer in solid form in a suspension medium is oxidized with ozone. The polymer obtained is suitable for the production of functional parts on which high demands are made.
摘要翻译：用于氧化含有硫醚基团的聚合物的方法，其中固体形式的悬浮介质中的聚合物被臭氧氧化。所得聚合物适用于生产要求高的功能部件。

3. 发明授权

US5423902A Filter material and process for removing ozone from gases and liquids 失效
标题翻译：用于从气体和液体中去除臭氧的过滤材料和工艺
公开(公告)号：US5423902A
公开(公告)日：1995-06-13
申请号：US110586
申请日：1993-08-23
申请人： Heinz Strutz , Dietrich Fleischer , Jurgen Kulpe , Andreas Schleicher
发明人： Heinz Strutz , Dietrich Fleischer , Jurgen Kulpe , Andreas Schleicher
IPC分类号： B01D19/00 , B01D53/14 , B01D53/66 , B01D53/86 , B01J20/26 , C08G75/02 , B01D53/04
CPC分类号： B01J20/26 , B01D19/0031 , B01D53/66 , C08G75/0204
摘要： A filter material based on a polyarylene thioether having repeating units of the formula--[(Ar.sup.1).sub.n --X)].sub.m --[(Ar.sup.2).sub.i --Y)].sub.j --[(Ar.sup.3).sub.k --Z)].sub.l --[(Ar.sup.4).sub.o --W)].sub.p --(I)in which Ar.sup.1, Ar.sup.2, Ar.sup.3, Ar.sup.4, W, X, Y and Z, independently of each other, are identical or different, the indices n, m, i, j, k, l, o and p, independently of each other, are zero or integers 1, 2, 3 or 4, their sum being at least 2, Ar.sup.1, Ar.sup.2, Ar.sup.3 and Ar.sup.4 are arylene systems having 6 to 18 carbon atoms, and W, X, Y and Z are divalent linking groups, selected from --SO.sub.2 --, --S--, --SO--, --CO--, --O--, --CO.sub.2 --, or alkylene groups or alkylidene groups having 1 to 6 carbon atoms is suitable for removing ozone from gases or liquids. The removal proceeds quantitatively, no volatile products being formed.
摘要翻译：基于具有式[[（Ar 1）n X）] m - [（Ar 2）i Y）] j - [（Ar 3）k Z）] - [（Ar 4）o W）] p]的重复单元的聚芳硫醚的过滤材料 - （I）其中Ar1，Ar2，Ar3，Ar4，W，X，Y和Z彼此独立地相同或不同，指数n，m，i，j，k，l，o和p，彼此独立，为零或整数1,2,3或4，它们的和为至少2，Ar 1，Ar 2，Ar 3和Ar 4为具有6至18个碳原子的亚芳基体系，W，X，Y和Z分别为选自-SO 2 - ， - S - ， - SO - ， - CO - ， - O - ， - CO 2 - 或具有1至6个碳原子的亚烷基或亚烷基的二价连接基团适用于从气体或液体。清除量定量进行，不形成挥发性物质。

4. 发明授权

US5331084A Fluorine-substituted epoxides and a method for their preparation 失效
标题翻译：氟取代的环氧化物及其制备方法
公开(公告)号：US5331084A
公开(公告)日：1994-07-19
申请号：US16901
申请日：1993-02-12
申请人： Jurgen Kulpe , Heinz Strutz
发明人： Jurgen Kulpe , Heinz Strutz
IPC分类号： C07D301/14 , C07D303/08 , C07D301/19 , C07D303/04 , C07D303/06
CPC分类号： C07D303/08
摘要： Fluorine-substituted epoxides of the formula ##STR1## in which the substituents R.sub.1 to R.sub.4, independently of one another, have the following meanings:R.sub.1 to R.sub.4 =H, fluorine, C.sub.1 - to C.sub.18 -alkyl in which some or all of the hydrogens may be substituted by fluorine, and at least one of the substituents R.sub.1 to R.sub.4 is a completely fluorinated alkyl or an alkyl of the formula--(CH.sub.2).sub.m --(C.sub.n F.sub.2n+1),in which m is 1 or 2, and n is an integer from 1 to 17, and x is 0 or 1.Furthermore, a method for the preparation of fluorine-substituted epoxides is described.
摘要翻译：取代基R 1至R 4彼此独立的氟取代的环氧化物具有如下含义：R 1至R 4 = H，氟，C 1至C 18烷基，其中部分或全部氢可以被氟取代，并且至少一个取代基R 1至R 4是完全氟化的烷基或式 - （CH 2）m - （C n F 2n + 1）的烷基，其中m为1或2，n为 1〜17的整数，x为0或1.此外，描述了制备氟取代的环氧化物的方法。

5. 发明授权

US6020442A Oxidized polyarylene sulfides 失效
标题翻译：氧化聚亚芳基硫化物
公开(公告)号：US6020442A
公开(公告)日：2000-02-01
申请号：US585267
申请日：1996-01-11
申请人： Dietrich Fleischer , Heinz Strutz , Jurgen Kulpe , Andreas Schleicher
发明人： Dietrich Fleischer , Heinz Strutz , Jurgen Kulpe , Andreas Schleicher
IPC分类号： C08G75/00 , C08G75/0236 , C08G75/0295 , C08G75/06 , C08G75/18 , C08L81/00
CPC分类号： C08G75/0236 , C08G75/0295 , C08G75/18
摘要： Oxidation product of polyarylene sulfides comprising recurring units of the formula.brket open-st.C.sub.6 H.sub.4 --S.brket close-st. (I)in the form of a compound comprising recurring units of the formula.brket open-st..paren open-st.C.sub.6 H.sub.4 --S.paren close-st..sub.a .paren open-st.C.sub.6 H.sub.4 --SO.paren close-st..sub.b .brket close-st.(II)in which the sulfur/oxygen ratio is from 1:0.1 to 1:1, the sum of a and b always being 1 and a and b each being greater than zero or with the proviso that a is zero if b is 1.
摘要翻译：包含式+ 547 C6H4-S + 548（I）的重复单元的聚亚芳基硫化物的氧化产物为包含式+ 547 +545 C6H4-S + 546a + 545C6H4-SO + 546的重复单元的化合物形式 b + 548（II），其中硫/氧比为1:0.1至1:1，a和b之和始终为1，a和b各自大于零，或者条件是a为0，如果 b为1。

6. 发明授权

US08664444B2 Method for producing primary aliphatic amines from aldehydes 有权
标题翻译：从醛生产伯脂肪族胺的方法
公开(公告)号：US08664444B2
公开(公告)日：2014-03-04
申请号：US13817155
申请日：2011-08-18
申请人： Kurt Schalapski , Norman Nowotny , Matthias Eisenacher , Dirk Bermann , Thorsten Kreickmann , Peter Heymanns , Heinz Strutz
发明人： Kurt Schalapski , Norman Nowotny , Matthias Eisenacher , Dirk Bermann , Thorsten Kreickmann , Peter Heymanns , Heinz Strutz
IPC分类号： C07C209/26
CPC分类号： C07B43/04 , B01J21/08 , B01J23/40 , B01J23/70 , B01J23/866 , C07C209/26 , C07C211/07
摘要： A continuous process for producing primary aliphatic amines having 9 to 18 carbon atoms by reaction of corresponding aliphatic aldehydes with ammonia and hydrogen in the presence of a hydrogenation catalyst in the liquid phase, characterized in that the reaction is carried out solventlessly at a molar ratio of aliphatic aldehyde:ammonia of at least 1:30, at a temperature of 100 to 200° C. and at a pressure of 6 to 11 MPa.
摘要翻译：在液相中在氢化催化剂存在下，通过相应的脂族醛与氨和氢的反应制备具有9至18个碳原子的伯脂肪族胺的连续方法，其特征在于该反应以脂肪醛：氨至少1:30，温度为100〜200℃，压力为6〜11MPa。

7. 发明申请

US20130131391A1 Method for obtaining ditrimethylolpropane and trimethylolpropane-enriched product streams from the side-streams in trimethylolpropane production 有权
公开(公告)号：US20130131391A1
公开(公告)日：2013-05-23
申请号：US13810723
申请日：2011-07-28
申请人： Thorsten Kreickmann , Guido D. Frey , Norman Nowotny , Heinz Strutz
发明人： Thorsten Kreickmann , Guido D. Frey , Norman Nowotny , Heinz Strutz
IPC分类号： C07C29/74 , C07C41/34
CPC分类号： C07C29/74 , C07C29/10 , C07C29/80 , C07C29/90 , C07C41/34 , C07C41/42 , C07C41/44 , C07C31/22 , C07C43/132
摘要： The present invention relates to a process for obtaining ditrimethylolpropane and trimethylolpropane-enriched product streams from the high-boiling fractions and residues which are obtained in the distillative purification of trimethylolpropane, wherein an aqueous solution of these fractions and residues is catalytically hydrogenated in the presence of an acidic compound and, after removing solids, contacted both with basic and with acidic ion exchangers. A trimethylolpropane-enriched product stream can be distilled out of the aqueous eluate obtained, leaving ditrimethylolpropane as the distillation residue.

8. 发明申请

US20130116467A1 Process for Aftertreating Polyolesters 有权
标题翻译：后置聚酯的工艺
公开(公告)号：US20130116467A1
公开(公告)日：2013-05-09
申请号：US13805693
申请日：2011-06-29
申请人： Guido D. Frey , Heyko Jürgen Schultz , Heinz Strutz
发明人： Guido D. Frey , Heyko Jürgen Schultz , Heinz Strutz
IPC分类号： C07C67/48
CPC分类号： C07C67/60 , C07C69/28
摘要： A process for aftertreatment of polyol esters prepared by reacting polyols of the general formula H—(—O—[—CR1R2—]m—)o—OH in which R1 and R2 are each independently hydrogen, an alkyl radical having 1 to 5 carbon atoms, or a hydroxyalkyl radical having 1 to 5 carbon atoms, m is an integer of 1 to 10, o is an integer of 2 to 15, with linear or branched aliphatic monocarboxylic acids having 3 to 20 carbon atoms in the presence of an adsorbent and in the presence of metal compounds selected from the group of titanium compounds, zirconium compounds, tin compounds, zinc compounds, iron compounds and aluminium compounds as a catalyst while removing the water formed and subsequently treating with steam, characterized in that the polyol ester obtained is aftertreated first with an oxidizing or reducing compound and immediately thereafter with steam at a temperature of 150 to 250° C. and over a period of 0.5 to 5 hours.
摘要翻译：一种通过使通式为H - （ - O - [ - CR 1 R 2 - ] m - ）o-OH的多元醇反应制备的多元醇酯的方法，其中R 1和R 2各自独立地为氢，具有1至5个碳原子的烷基原子或具有1至5个碳原子的羟烷基，m是1至10的整数，o是2至15的整数，在吸附剂存在下具有3至20个碳原子的直链或支链脂肪族单羧酸在选择钛化合物，锆化合物，锡化合物，锌化合物，铁化合物和铝化合物作为催化剂的金属化合物的存在下，同时除去形成的水并随后用蒸汽处理，其特征在于获得的多元醇酯首先用氧化或还原化合物进行后处理，然后立即用蒸汽在150至250℃的温度和0.5至5小时的时间内进行处理。

9. 发明授权

US08357824B2 Process for preparing neopentyl glycol by cracking high boilers occurring in the production process 有权
标题翻译：通过裂解在生产过程中发生的高锅炉来制备新戊二醇的方法
公开(公告)号：US08357824B2
公开(公告)日：2013-01-22
申请号：US12737388
申请日：2009-06-25
申请人： Rolf-Peter Schulz , Horst Scholz , Thomas Hupperich , Peter Heymanns , Tonia Weber , Alexander Kaufmann , Kurt Schalapski , Heinz Strutz
发明人： Rolf-Peter Schulz , Horst Scholz , Thomas Hupperich , Peter Heymanns , Tonia Weber , Alexander Kaufmann , Kurt Schalapski , Heinz Strutz
IPC分类号： C07C31/18
CPC分类号： C07C29/132 , C07C29/149 , C07C31/20
摘要： The present invention relates to a process for obtaining neopentyl glycol by hydrogenating cracking of high-boilers occurring in the production process in the presence of copper-chromite catalysts. The hydrogenating cracking proceeds in the absence of solvent at a temperature of 140 to 220° C. and at pressures of 7 to 28 MPa.
摘要翻译：本发明涉及通过在亚铬酸铜催化剂的存在下，在生产过程中发生的高锅炉的氢化氢化获得新戊二醇的方法。在不存在溶剂的情况下，在140〜220℃的温度和7〜28MPa的压力下进行氢化裂化。

10. 发明授权

US06423856B1 Process for preparing ester plasticizers 有权
标题翻译：酯增塑剂的制备方法
公开(公告)号：US06423856B1
公开(公告)日：2002-07-23
申请号：US09644913
申请日：2000-08-24
申请人： Helmut Springer , Klaus-Dieter Merscher , Rudolf Heumuller , Klaus Schimmer , Heinz Strutz
发明人： Helmut Springer , Klaus-Dieter Merscher , Rudolf Heumuller , Klaus Schimmer , Heinz Strutz
IPC分类号： C07C5100
CPC分类号： C07C67/08 , B32B17/10605 , C07C69/28 , C07C69/75
摘要： The present invention relates to a process for preparing ester plasticizers from ethylene glycol or the dimers, trimers or tetramers of this compound and linear or branched aliphatic monocarboxylic acids having from 3 to 20 carbon atoms. The reaction is carried out in the presence of organic substances having a boiling point of
摘要翻译：本发明涉及一种由乙二醇或该化合物的二聚体，三聚体或四聚物和具有3-20个碳原子的直链或支链脂族一元羧酸制备酯增塑剂的方法。反应在沸点<112℃的有机物质，特别是环己烷存在下，作为除去反应水的共沸物（夹带剂）进行。

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