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1. 发明授权

US07393987B2 Process for producing adamantane 失效
标题翻译：生产金刚烷的方法
公开(公告)号：US07393987B2
公开(公告)日：2008-07-01
申请号：US10582607
申请日：2004-12-16
申请人： Akio Kojima , Masao Saito , Shinji Miyamoto , Jun Mase , Toyozo Fujioka
发明人： Akio Kojima , Masao Saito , Shinji Miyamoto , Jun Mase , Toyozo Fujioka
IPC分类号： C07C13/28
CPC分类号： C07C5/29 , C07C2603/74 , C07C13/615
摘要： The present invention provides a process of an industrially advantageous production of high-purity adamantane at a low cost and with a high efficiency by isomerizing trimethylenenorbornane contained in a raffinate obtained from a platfinate.
摘要翻译：本发明提供了一种以低成本工业上有利地生产高纯度金刚烷的方法，并且通过异构化得自平板料的萃余液中所含的三亚甲基降冰片烷具有高效率。

2. 发明授权

US07381855B2 Process for producing adamantane 失效
标题翻译：生产金刚烷的方法
公开(公告)号：US07381855B2
公开(公告)日：2008-06-03
申请号：US10590995
申请日：2005-02-28
申请人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
发明人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
IPC分类号： C07C13/28 , C07C7/14
CPC分类号： C07C5/29 , B01J29/126 , C07C7/14 , C07C2603/74 , C07C13/615
摘要： An industrially advantageous process for producing adamantane by which high-purity adamantane reduced in coloration is efficiently produced while minimizing the loss. The process, which is for producing adamantane by isomerizing trimethylenenorbornane, includes (A) a reaction step of isomerizing the starting material, (B) a concentration step of concentrating the adamantane contained in the resultant liquid reaction mixture, (C) a crystallization step of precipitating the concentrated adamantane, (D) a solid-liquid separation step of separating the adamantane crystals from the slurry resulting from the crystallization, (E) a washing step of washing the isolated adamantane crystals, and (F) a drying step of drying the adamantane crystals washed, characterized in that the mass ratio of the endo-trimethylenenorbornane to the adamantane each contained in the materials to be subjected to the crystallization step (C) (endo-trimethylenenorbornane/adamantane) is 0.25 or lower.
摘要翻译：在生产金刚烷的工业上有利的方法是高效率地生产高纯度金刚烷，降低了损失。用于通过异亚丙基降冰片烷生产金刚烷的方法包括（A）使原料异构化的反应步骤，（B）浓缩所得液体反应混合物中所含金刚烷的浓缩步骤，（C）结晶步骤沉淀浓缩金刚烷，（D）从结晶得到的浆料中分离金刚烷结晶的固液分离步骤，（E）洗涤分离的金刚烷结晶的洗涤步骤，和（F）干燥步骤金刚烷晶体洗涤，其特征在于，待进行结晶步骤（C）（内 - 三亚甲基降冰片烷/金刚烷）的材料中含有的内 - 三亚甲基降冰片烷与金刚烷的质量比为0.25以下。

3. 发明申请

US20070173678A1 Process for producing adamantane 失效
标题翻译：生产金刚烷的方法
公开(公告)号：US20070173678A1
公开(公告)日：2007-07-26
申请号：US10590995
申请日：2005-02-28
申请人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
发明人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
IPC分类号： C07C5/13
CPC分类号： C07C5/29 , B01J29/126 , C07C7/14 , C07C2603/74 , C07C13/615
摘要： An industrially advantageous process for producing adamantane by which high-purity adamantane reduced in coloration is efficiently produced while minimizing the loss. The process, which is for producing adamantane by isomerizing trimethylenenorbornane, includes (A) a reaction step of isomerizing the starting material, (B) a concentration step of concentrating the adamantane contained in the resultant liquid reaction mixture, (C) a crystallization step of precipitating the concentrated adamantane, (D) a solid-liquid separation step of separating the adamantane crystals from the slurry resulting from the crystallization, (E) a washing step of washing the isolated adamantane crystals, and (F) a drying step of drying the adamantane crystals washed, characterized in that the mass ratio of the endo-trimethylenenorbornane to the adamantane each contained in the materials to be subjected to the crystallization step (C) (endo-trimethylenenorbornane/adamantane) is 0.25 or lower.
摘要翻译：在生产金刚烷的工业上有利的方法是高效率地生产高纯度金刚烷，降低了损失。用于通过异亚丙基降冰片烷生产金刚烷的方法包括（A）使原料异构化的反应步骤，（B）浓缩所得液体反应混合物中所含金刚烷的浓缩步骤，（C）结晶步骤沉淀浓缩金刚烷，（D）从结晶得到的浆料中分离金刚烷结晶的固液分离步骤，（E）洗涤分离的金刚烷结晶的洗涤步骤，和（F）干燥步骤金刚烷晶体洗涤，其特征在于，待进行结晶步骤（C）（内 - 三亚甲基降冰片烷/金刚烷）的材料中含有的内 - 三亚甲基降冰片烷与金刚烷的质量比为0.25以下。

4. 发明申请

US20070156002A1 Process for producing adamantane 失效
标题翻译：生产金刚烷的方法
公开(公告)号：US20070156002A1
公开(公告)日：2007-07-05
申请号：US10582607
申请日：2004-12-16
申请人： Akio Kojima , Masao Saito , Shinji Miyamoto , Jun Mase , Toyozo Fujioka
发明人： Akio Kojima , Masao Saito , Shinji Miyamoto , Jun Mase , Toyozo Fujioka
IPC分类号： C07C5/13
CPC分类号： C07C5/29 , C07C2603/74 , C07C13/615
摘要： The present invention provides a process of an industrially advantageous production of high-purity adamantane at a low cost and with a high efficiency by isomerizing trimethylenenorbornane contained in a raffinate obtained from a platfinate.
摘要翻译：本发明提供了一种以低成本工业上有利地生产高纯度金刚烷的方法，并且通过异构化得自平板料的萃余液中所含的三亚甲基降冰片烷具有高效率。

5. 发明申请

US20060111596A1 Process for the preparation of adamantanes 审中-公开
标题翻译：制备金刚烷的方法
公开(公告)号：US20060111596A1
公开(公告)日：2006-05-25
申请号：US10522338
申请日：2003-07-25
申请人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito
发明人： Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito
IPC分类号： C07C13/28
CPC分类号： C07C13/615 , C07C5/29 , C07C2529/22
摘要： According to the present invention, there is provided a process for producing adamantanes by isomerizing a tricyclic saturated hydrocarbon compound having 10 or more carbon atoms, comprising (A) a reaction step for isomerizing a raw material, (B) a concentration step for concentrating the adamantanes in a reaction product liquid, (C) a crystallization step for crystallizing the concentrated adamantanes, (D) a solid-liquid separation step for separating the crystallized adamantanes from slurry having precipitated crystals, (E) a washing step for washing the crystal of adamantanes obtained by the solid-liquid separation step, and (F) a drying step for drying the washed crystals of adamantanes. According to the present invention, there is provided a process for producing adamantanes by using a solid catalyst, wherein the obtained adamantanes are purified by a crystallization operation. There is provided a process for producing adamantanes by isomerizing a tricyclic saturated hydrocarbon compound, wherein the obtained adamantanes are washed by a washing solvent after separating the adamantanes by a crystallization step and a solid-liquid separation step. There is provided a process for producing adamantanes by isomerizing a tricyclic saturated hydrocarbon compound, wherein the crystal of the adamantanes which contains a liquid fraction in the range from 5 to 50% by mass is dried.
摘要翻译：根据本发明，提供了通过异构化具有10个或更多个碳原子的三环饱和烃化合物来生产金刚烷的方法，包括（A）用于使原料异构化的反应步骤，（B）浓缩步骤反应产物液中的金刚烷，（C）结晶浓缩金刚烷的结晶步骤，（D）用于将结晶金刚烷与具有析出晶体的浆料分离的固液分离步骤，（E）洗涤步骤，通过固液分离步骤获得的金刚烷，（F）干燥洗涤的金刚烷晶体的干燥步骤。根据本发明，提供了一种使用固体催化剂制备金刚烷的方法，其中所得金刚烷通过结晶操作进行纯化。提供了通过使三环饱和烃化合物异构化生产金刚烷的方法，其中通过结晶步骤和固液分离步骤分离金刚烷后，通过洗涤溶剂洗涤所获得的金刚烷。提供了通过使三环饱和烃化合物异构化生产金刚烷的方法，其中将含有5至50质量％的液体部分的金刚烷的晶体干燥。

6. 发明申请

US20090177019A1 PROCESS FOR PRODUCING ADAMANTANE 审中-公开
标题翻译：生产ADAMANTANE的方法
公开(公告)号：US20090177019A1
公开(公告)日：2009-07-09
申请号：US12299785
申请日：2007-05-09
申请人： Masao Saito , Akio Kojima , Toshiaki Kusaba , Jun Mase
发明人： Masao Saito , Akio Kojima , Toshiaki Kusaba , Jun Mase
IPC分类号： C07C13/28
CPC分类号： B01J29/126 , B01J29/088 , B01J2229/186 , C07C5/29 , C07C2529/08 , C07C2529/12 , C07C2603/74 , C07C13/615
摘要： Provided is a method for production of adamantane which enables producing a high-purity adamantane at low cost and with high efficiency by using effectively trimethylenenorbornane contained in a heavy raffinate heavy and having conventionally been no use other than fuels and the like, and which enables alleviating poisoning of a catalyst used in isomerization and corrosion of devices, whereby an industrially advantageous adamantane can be produced. In addition, the process for producing adamantane including an isomerization process of isomerizing trimethylenenorbornane contained in a raffinate obtained from a platfinate is characterized by including a water-washing removal process of removing sulfolane in a trimethylenenorbornane concentrate to be supplied in the isomerization process by water-washing.
摘要翻译：本发明提供一种金刚烷的制造方法，其能够低成本且高效率地制造高纯度金刚烷，其特征在于，使用重质提余液重金属中含有的三甲基降冰片烷，并且以往除了燃料等以外没有其他用途，能够缓和用于装置的异构化和腐蚀的催化剂的中毒，由此可以生产工业上有利的金刚烷。另外，含有由平板化合物得到的残液中异构化亚烷基降冰片烷异构化方法的金刚烷的制造方法的特征在于，在异氰酸酯化方法中，通过水洗方法，在三亚甲基降冰片烷烷浓缩物中除去环丁砜，洗涤。

7. 发明申请

US20090131729A1 METHOD FOR PRODUCTION OF ADAMANTANE 审中-公开
标题翻译：生产ADAMANTANE的方法
公开(公告)号：US20090131729A1
公开(公告)日：2009-05-21
申请号：US12298916
申请日：2007-05-02
申请人： Masao Saito , Akio Kojima , Jun Mase , Toshiaki Kusaba
发明人： Masao Saito , Akio Kojima , Jun Mase , Toshiaki Kusaba
IPC分类号： C07C5/27
CPC分类号： B01J29/126 , B01J29/088 , B01J2229/186 , C07C5/29 , C07C2529/08 , C07C2529/12 , C07C2603/74 , C07C13/615
摘要： Provided is a method for production of adamantanes, in which, when a tricyclic saturated hydrocarbon compound having 10 or more carbon atoms is isomerized in the presence of a solid catalyst to give adamantanes, no solid matter derived from an oxygen-containing compound is formed or accumulated in the inlet or the bottom of an isomerization reactor by providing a pre-reactor in an isomerization step even if the oxygen-containing compound is present in a raw material to be supplied.
摘要翻译：本发明提供一种生产金刚烷的方法，其中当在固体催化剂存在下将具有10个或更多个碳原子的三环饱和烃化合物异构化以产生金刚烷时，不形成由含氧化合物衍生的固体物质，或通过在异构化步骤中提供预反应器，即使含氧化合物存在于待供应的原料中，也积聚在异构化反应器的入口或底部。

8. 发明授权

US06268543B1 Method of removing mercury in liquid hydrocarbon 有权
标题翻译：去除液态碳氢化合物中的汞的方法
公开(公告)号：US06268543B1
公开(公告)日：2001-07-31
申请号：US09435209
申请日：1999-11-05
申请人： Tsunenori Sakai , Hidetoshi Ono , Jun Mase , Tetsuya Saruwatari
发明人： Tsunenori Sakai , Hidetoshi Ono , Jun Mase , Tetsuya Saruwatari
IPC分类号： C07C710
CPC分类号： C10G29/06 , C10G31/08
摘要： In a method of efficiently removing mercury from a liquid hydrocarbon, the liquid hydrocarbon is contacted with water contacted in advance with a crude oil and a sludge contacted in advance with a crude oil. Alternatively, the liquid hydrocarbon is contacted with a substance having ability of ionizing elemental mercury and a sulfur compound having the formula: MM′S, wherein M and M′ are identical or different and are each hydrogen, alkali metal or ammonium group. When the liquid hydrocarbon to be treated contains no dissolved oxygen or contains dissolved oxygen in an amount in equilibrium with a gas containing 8% by volume of oxygen, the increase in the mercury concentration of a liquid hydrocarbon after the removing treatment is effectively prevented.
摘要翻译：在从液体烃中有效地除去汞的方法中，液态烃与预先与原油接触的水与预先与原油接触的污泥接触。或者，使液体烃与具有离子化元素汞的物质和具有下式的MM'S的硫化合物接触，其中M和M'相同或不同，并且各自为氢，碱金属或铵基团。当待处理的液体烃不含有溶解氧或含有与含有8体积％氧气的气体平衡的溶解氧时，有效地防止了除去处理后的液态烃的汞浓度的增加。

9. 发明申请

US20080045764A1 Method of Preventing Adamantane Consolidation 审中-公开
标题翻译：防止金刚烷合并的方法
公开(公告)号：US20080045764A1
公开(公告)日：2008-02-21
申请号：US11571937
申请日：2005-07-11
申请人： Jun Mase , Toshiaki Kusaba
发明人： Jun Mase , Toshiaki Kusaba
IPC分类号： C07C13/28
CPC分类号： C07C7/00 , C07C13/615
摘要： The present invention provides a method of controlling the amount of the solvent contained in adamantane purified by using a naphthene-based solvent to 0.35% by mass or less, or controlling the amount of the solvent contained in adamantane purified by using a non-naphthene-based solvent to 0.05% by mass or less and storing adamantane at 35° C. or lower. By this method, adamantane whose particles do not agglomerate together or cake and having stable quality can be obtained.
摘要翻译：本发明提供一种控制通过使用环烷烃系溶剂纯化的金刚烷中含有的溶剂的含量为0.35质量％以下的方法，或者通过使用非环烷烃系溶剂来控制金刚烷中所含的溶剂的量，基于0.05质量％以下的溶剂，在35℃以下储存金刚烷。通过这种方法，可以获得其颗粒不聚集在一起或者蛋糕质量稳定的金刚烷。

10. 发明授权

US09056931B2 Method for producing olefin polymer 有权
标题翻译：烯烃聚合物的制备方法
公开(公告)号：US09056931B2
公开(公告)日：2015-06-16
申请号：US14124933
申请日：2012-06-27
申请人： Jun Kohiruimaki , Masao Aida , Jun Mase , Kana Minamimoto
发明人： Jun Kohiruimaki , Masao Aida , Jun Mase , Kana Minamimoto
IPC分类号： C08J3/09 , C08F4/6592 , C08F10/14 , C08F210/14 , C08F2/06 , C08F6/00 , C08F6/02 , C08F4/659
CPC分类号： C08F210/14 , C08F2/06 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F6/003 , C08F6/02 , C08J3/09 , C08L23/0815
摘要： A method for producing an olefin polymer including: polymerizing one or more α-olefins each having 6 to 20 carbon atoms in the presence of a metallocene catalyst to obtain an olefin polymer, and diluting a polymerization reaction liquid with a solvent before or simultaneously with deactivation of the catalyst, thereby to lower the liquid viscosity of the polymerization reaction liquid to 10 mPa·s or less to promote deactivation and decalcification of the catalyst.
摘要翻译：一种烯烃聚合物的制造方法，其特征在于，在金属茂催化剂的存在下，使一种以上的碳原子数为6〜20的α-烯烃聚合，得到烯烃系聚合物，在失活前或同时使溶剂稀释的催化剂，从而将聚合反应液体的液体粘度降低至10mPa·s以下，以促进催化剂的失活和脱钙。

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