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1. 发明授权

US06211422B1 Enzyme catalysis in carbon dioxide fluids 失效
标题翻译：二氧化碳液体中的酶催化
公开(公告)号：US06211422B1
公开(公告)日：2001-04-03
申请号：US09352249
申请日：1999-07-13
申请人： Joseph M. DeSimone , Ruben G. Carbonell , Stephanie A. Crette , Jonathan L. Kendall
发明人： Joseph M. DeSimone , Ruben G. Carbonell , Stephanie A. Crette , Jonathan L. Kendall
IPC分类号： C12P100
CPC分类号： C12P41/001 , C12P1/00 , Y02P20/544
摘要： A method for the enzymatic production of a desired product in a liquid or supercritical carbon dioxide fluid. The method comprises: (a) providing a reaction mixture comprising at least one reaction substrate and a crosslinked enzyme crystal catalyst in a liquid or supercritical carbon dioxide fluid; and (b) reacting said substrate with said crosslinked enzyme crystal catalyst in said carbon dioxide fluid to produce said product. The reacting step is typically followed by the step of (c) separating the product from said reaction mixture. The crosslinked enzyme crystal catalyst preferably comprises an enzyme crystal crosslinked with a multifunctional crosslinking agent, said crosslinked enzyme crystal having resistance to exogeneous proteolysis, such that the crosslinked enzyme crystal retains at least about 80 percent of its initial activity after incubation for three hours in the presence of a concentration of Pronase™ protease that causes the soluble uncrosslinked form of the enzyme that is crystallized to form said enzyme crystal that is crosslinked to lose at least about 80 percent of its initial activity under the same conditions. Reaction mixtures useful for carrying out the foregoing method and product mixtures produced by the foregoing method are also disclosed.
摘要翻译：在液体或超临界二氧化碳流体中酶促生产所需产物的方法。该方法包括：（a）在液体或超临界二氧化碳流体中提供包含至少一个反应底物和交联的酶晶体催化剂的反应混合物; 和（b）使所述底物与所述交联的酶晶体催化剂在所述二氧化碳流体中反应以产生所述产物。反应步骤通常是（c）从所述反应混合物中分离产物的步骤。交联酶晶体催化剂优选包含与多官能交联剂交联的酶晶体，所述交联酶晶体具有对外源性蛋白水解的抗性，使得交联的酶晶体在孵育3小时后保留其初始活性的至少约80％存在一种浓度的Pronase TM蛋白酶，其引起可溶性的未交联形式的酶，其被结晶以形成所述交联的酶晶体，以在相同条件下损失其初始活性的至少约80％。还公开了可用于实施上述方法的反应混合物和通过前述方法制备的产物混合物。

2. 发明授权

US06500273B2 Spin cleaning methods 失效
标题翻译：旋转清洗方法
公开(公告)号：US06500273B2
公开(公告)日：2002-12-31
申请号：US10068139
申请日：2002-02-06
申请人： Joseph M. DeSimone , Ruben G. Carbonell
发明人： Joseph M. DeSimone , Ruben G. Carbonell
IPC分类号： B08B302
CPC分类号： H01L21/6715 , B05C11/08 , B05D1/005 , B08B7/0021
摘要： Spin cleaning methods include applying carbon dioxide liquid to surface portions of substrates and then rotating the substrates about axes to distribute the carbon dioxide liquid on the substrates.
摘要翻译：旋转清洁方法包括将二氧化碳液体施加到基板的表面部分，然后将基板绕轴线旋转以将二氧化碳液体分布在基板上。

3. 发明授权

US6083565A Method for meniscus coating with liquid carbon dioxide 失效
标题翻译：液体二氧化碳弯液面涂覆方法
公开(公告)号：US6083565A
公开(公告)日：2000-07-04
申请号：US188053
申请日：1998-11-06
申请人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
发明人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
IPC分类号： B01J19/00 , B05C3/02 , B05C11/04 , B05C11/10 , B05C13/00 , B05D1/18 , B05D3/00 , B05D7/24 , C09D7/00 , C09D201/00 , D06B1/08 , D06B3/10 , D06M23/00 , D06M23/10
CPC分类号： D06M23/105 , B05D1/18 , D06B1/08 , D06B3/10 , D06M23/00 , D06M23/10 , B05D2401/90
摘要： A method of coating a substrate comprises immersing a surface portion of a substrate in a liquid or supercritical first phase. The first phase comprises carbon dioxide and a coating component such as a polymer. The substrate is then withdrawn from the first phase into a distinct second phase such as a gas atmosphere so that the coating component is deposited on said surface portion. The withdrawal step is followed by separating the carbon dioxide from the coating component (e.g., by evaporation, venting, heating, etc.) so that the coating component is retained as a coating layer formed on the surface portion. Apparatus for carrying out the method by free meniscus coating, or employing a metering element such as a knife, blade, or roll, are also disclosed.
摘要翻译：涂覆基材的方法包括将基材的表面部分浸入液体或超临界第一相中。第一相包括二氧化碳和涂料组分如聚合物。然后将衬底从第一相排出到不同的第二相，例如气体气氛中，使得涂层组分沉积在所述表面部分上。撤回步骤之后是将二氧化碳与涂料组分分离（例如，通过蒸发，排气，加热等），使得涂料组分作为形成在表面部分上的涂层而被保留。还公开了通过自由弯液面涂覆或采用诸如刀，刀片或辊的计量元件来执行该方法的装置。

4. 发明授权

US6127000A Method and compositions for protecting civil infrastructure 失效
标题翻译：保护民用基础设施的方法和组成
公开(公告)号：US6127000A
公开(公告)日：2000-10-03
申请号：US948733
申请日：1997-10-10
申请人： Ruben G. Carbonell , Joseph M. DeSimone , Florence E. Henon
发明人： Ruben G. Carbonell , Joseph M. DeSimone , Florence E. Henon
IPC分类号： E04F13/07 , B05D1/02 , B05D5/08 , B05D7/00 , B05D7/06 , B05D7/24 , B08B17/00 , C04B41/48 , C04B41/50 , C04B41/63 , C04B41/83 , C08G65/00 , C09D127/12 , C09D167/00 , C09D171/00 , C09D171/02 , C09D177/00 , B05D3/02
CPC分类号： C09D171/02 , B05D1/025 , B05D5/083 , C04B41/4842 , C04B41/5072 , C08G65/007 , Y10S526/942
摘要： A method of protecting a civil infrastructure substrate from the damaging effects of pollution, noxious fumes, weather, and the like. The method comprises (a) providing a composition comprising carbon dioxide and a fluorocarbon such as a fluoropolyether (preferably a perfluoropolyether) or a fluorocarbon elastomer, optionally having at least one anchoring group such as an amide covalently joined thereto, and then (b) applying that composition to the civil infrastructure substrate to form a protective coating thereon. The applying step is preferably carried out by spraying. Compositions useful for carrying out the process of the invention are also disclosed.
摘要翻译：一种保护民用基础设施基材免受污染，有害烟雾，天气等的破坏性影响的方法。该方法包括（a）提供包含二氧化碳和氟碳化合物的组合物，例如氟聚醚（优选全氟聚醚）或氟碳弹性体，任选具有至少一个与其共价连接的锚定基团如酰胺，然后（b）该组合物到民用基础设施基材上以在其上形成保护涂层。施涂步骤优选通过喷雾进行。还公开了可用于实施本发明方法的组合物。

5. 发明授权

US06517633B1 Apparatus for meniscus coating with liquid carbon dioxide 失效
标题翻译：液体二氧化碳弯液面涂装设备
公开(公告)号：US06517633B1
公开(公告)日：2003-02-11
申请号：US09567646
申请日：2000-05-09
申请人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
发明人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
IPC分类号： B05C302
CPC分类号： D06M23/105 , B05D1/18 , B05D2401/90 , D06B1/08 , D06B3/10 , D06M23/00 , D06M23/10
摘要： A method of coating a substrate comprises immersing a surface portion of a substrate in a liquid or supercritical first phase. The first phase comprises carbon dioxide and a coating component such as a polymer. The substrate is then withdrawn from the first phase into a distinct second phase such as a gas atmosphere so that the coating component is deposited on said surface portion. The withdrawal step is followed by separating the carbon dioxide from the coating component (e.g., by evaporation, venting, heating, etc.) so that the coating component is retained as a coating layer formed on the surface portion. Apparatus for carrying out the method by free meniscus coating, or employing a metering element such as a knife, blade, or roll, are also disclosed.
摘要翻译：涂覆基材的方法包括将基材的表面部分浸入液体或超临界第一相中。第一相包括二氧化碳和涂料组分如聚合物。然后将衬底从第一相中排出到不同的第二相，例如气体气氛中，使得涂层组分沉积在所述表面部分上。撤回步骤之后是将二氧化碳与涂料组分分离（例如，通过蒸发，排气，加热等），使得涂料组分作为形成在表面部分上的涂层而被保留。还公开了通过自由弯液面涂覆或采用诸如刀，刀片或辊的计量元件来执行该方法的装置。

6. 发明授权

US06497921B1 Method for meniscus coating with liquid carbon dioxide 失效
标题翻译：液体二氧化碳弯液面涂覆方法
公开(公告)号：US06497921B1
公开(公告)日：2002-12-24
申请号：US09589557
申请日：2000-06-07
申请人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
发明人： Ruben G. Carbonell , Joseph M. DeSimone , Brian J. Novick
IPC分类号： B05D118
CPC分类号： D06B1/08 , B05D1/18 , B05D2401/90 , D06B3/10 , D06M23/00 , D06M23/10 , D06M23/105
摘要： A method of coating a substrate comprises immersing a surface portion of a substrate in a first phase comprising carbon dioxide and a coating component comprising a polymeric precursor; then withdrawing the substrate from the first phase into a distinct second phase so that the coating component is deposited on the surface portion; and then subjecting the substrate to conditions sufficient to polymerize the polymeric precursor and form a polymerized coating.
摘要翻译：涂覆基材的方法包括将基材的表面部分浸入包含二氧化碳的第一相和包含聚合物前体的涂料组分; 然后将衬底从第一相中提取到不同的第二相中，使得涂层组分沉积在表面部分上; 然后使基底经受足以使聚合物前体聚合并形成聚合涂层的条件。

7. 发明授权

US06383289B2 Apparatus for liquid carbon dioxide systems 失效
标题翻译：液体二氧化碳系统装置
公开(公告)号：US06383289B2
公开(公告)日：2002-05-07
申请号：US09794294
申请日：2001-02-27
申请人： Joseph M. DeSimone , Ruben G. Carbonell
发明人： Joseph M. DeSimone , Ruben G. Carbonell
IPC分类号： B05D312
CPC分类号： H01L21/6715 , B05C11/08 , B05D1/005 , B08B7/0021
摘要： Spin coating apparatuses for applying liquid to substrates include pressure vessels having enclosed chambers therein, holders for rotating substrates positioned in the enclosed chambers, liquid dispensers positioned in the enclosed chambers for depositing a carbon dioxide liquid on the substrates, and pressure reservoirs in fluid communication with the liquid dispensers for storing a carbon dioxide liquid.
摘要翻译：用于将液体涂敷于基材的旋转涂布装置包括其中具有封闭室的压力容器，用于旋转位于封闭室内的基板的保持器，位于封闭室内的液体分配器，用于在基板上沉积二氧化碳液体;以及压力容器，用于储存二氧化碳液体的液体分配器。

8. 发明授权

US06764809B2 CO2-processes photoresists, polymers, and photoactive compounds for microlithography 失效
标题翻译：二氧化碳处理光刻胶，聚合物和光敏化合物用于微光刻
公开(公告)号：US06764809B2
公开(公告)日：2004-07-20
申请号：US09975211
申请日：2001-10-10
申请人： Joseph M. DeSimone , Ruben G. Carbonell , Jonathan Kendall , Christopher L. McAdams
发明人： Joseph M. DeSimone , Ruben G. Carbonell , Jonathan Kendall , Christopher L. McAdams
IPC分类号： C03F700
CPC分类号： G03F7/36 , G03F7/0046 , G03F7/0048 , G03F7/0392 , G03F7/0395 , G03F7/16 , G03F7/162 , G03F7/26 , G03F7/30 , G03F7/32 , G03F7/325 , G03F7/42 , G03F7/422 , Y10S430/126
摘要： A process of forming a resist image in a microelectronic substrate comprises the steps of contacting the substrate with a composition first comprising carbon dioxide and a component selected from the group consisting of at least one polymeric precursor, at least one monomer, at least one polymeric material, and mixtures thereof to deposit the component on the substrate and form a coating thereon; then imagewise exposing the coating to radiation such that exposed and unexposed coating portions are formed; then subjecting the coating to a second composition comprising carbon dioxide having such that either one of the exposed or the unexposed coating portions are removed from the substrate and the other coating portion is developed and remains on the coating to form an image thereon.
摘要翻译：在微电子衬底中形成抗蚀剂图像的方法包括以下步骤：使基底与首先包含二氧化碳和选自至少一种聚合物前体，至少一种单体，至少一种聚合物材料及其混合物以将组分沉积在基材上并在其上形成涂层; 然后将涂层成像曝光到辐射，从而形成曝光和未曝光的涂层部分; 然后对涂层进行包含二氧化碳的第二组合物，所述二氧化碳具有使得暴露的或未曝光的涂层部分中的任一个从基板移除，并且另一个涂覆部分被显影并保留在涂层上以在其上形成图像。

9. 发明授权

US06747179B1 Carbon dioxide-soluble polymers and swellable polymers for carbon dioxide applications 失效
标题翻译：用于二氧化碳应用的二氧化碳可溶性聚合物和可溶胀聚合物
公开(公告)号：US06747179B1
公开(公告)日：2004-06-08
申请号：US09641815
申请日：2000-08-18
申请人： Joseph M. DeSimone , Eva Birnbaum , Ruben G. Carbonell , Stephanie Crette , James B. McClain , T. Mark McCleskey , Kimberly R. Powell , Timothy J. Romack , William Tumas
发明人： Joseph M. DeSimone , Eva Birnbaum , Ruben G. Carbonell , Stephanie Crette , James B. McClain , T. Mark McCleskey , Kimberly R. Powell , Timothy J. Romack , William Tumas
IPC分类号： C07C502
CPC分类号： B01J31/06 , B01J3/008 , B01J31/003 , B01J31/006 , B01J31/1658 , B01J31/1805 , B01J31/1845 , B01J31/2208 , B01J31/2404 , B01J2231/321 , B01J2231/4205 , B01J2231/645 , B01J2231/72 , B01J2531/64 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/828 , B01J2531/922
摘要： A method for carrying out a catalysis reaction in carbon dioxide comprising contacting a fluid mixture with a catalyst bound to a polymer, the fluid mixture comprising at least one reactant and carbon dioxide, wherein the reactant interacts with the catalyst to form a reaction product. A composition of matter comprises carbon dioxide and a polymer and a reactant present in the carbon dioxide. The polymer has bound thereto a catalyst at a plurality of chains along the length of the polymer, and wherein the reactant interacts with the catalyst to form a reaction product.
摘要翻译：一种在二氧化碳中进行催化反应的方法，包括使流体混合物与结合到聚合物上的催化剂接触，所述流体混合物包含至少一种反应物和二氧化碳，其中反应物与催化剂相互作用以形成反应产物。物质组合物包含二氧化碳和存在于二氧化碳中的聚合物和反应物。聚合物沿着聚合物的长度在多个链上结合有催化剂，并且其中反应物与催化剂相互作用以形成反应产物。

10. 发明授权

US06736996B1 Compositions for protecting civil infrastructure 失效
标题翻译：保护民用基础设施的组成部分
公开(公告)号：US06736996B1
公开(公告)日：2004-05-18
申请号：US09619993
申请日：2000-07-20
申请人： Ruben G. Carbonell , Joseph M. DeSimone , Florence E. Henon
发明人： Ruben G. Carbonell , Joseph M. DeSimone , Florence E. Henon
IPC分类号： C09K300
CPC分类号： C09D171/02 , B05D1/025 , B05D5/083 , C04B41/4842 , C04B41/5072 , C08G65/007 , Y10S526/942 , C04B41/4519
摘要： A method of protecting a civil infrastructure substrate from the damaging effects of pollution, noxious fumes, weather, and the like. The method comprises (a) providing a composition comprising carbon dioxide and a fluorocarbon such as a fluoropolyether (preferably a perfluoropolyether) or a fluorocarbon elastomer, optionally having at least one anchoring group such as an amide covalently joined thereto, and then (b) applying that composition to the civil infrastructure substrate to form a protective coating thereon. The applying step is preferably carried out by spraying. Compositions useful for carrying out the process of the invention are also disclosed.
摘要翻译：一种保护民用基础设施基材免受污染，有害烟雾，天气等的破坏性影响的方法。该方法包括（a）提供包含二氧化碳和氟碳化合物的组合物，例如氟聚醚（优选全氟聚醚）或氟碳弹性体，任选具有至少一个与其共价连接的锚定基团如酰胺，然后（b）该组合物到民用基础设施基材上以在其上形成保护涂层。施涂步骤优选通过喷雾进行。还公开了可用于实施本发明方法的组合物。

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