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1. 发明授权

US4404146A Metal oxyalkylates and method of making same 失效
标题翻译：金属烷氧基化物及其制备方法
公开(公告)号：US4404146A
公开(公告)日：1983-09-13
申请号：US304305
申请日：1981-09-21
申请人： Joseph E. Lionelle , Jeffrey A. Staffa
发明人： Joseph E. Lionelle , Jeffrey A. Staffa
IPC分类号： A23K1/175 , C07C53/06 , C07C53/10 , C07C53/122 , C07C53/124 , C07C53/126 , C07F3/06 , C07F13/00
CPC分类号： C07C53/126 , A23K20/30 , C07C53/06 , C07C53/10 , C07C53/122 , C07C53/124 , C07F13/005 , C07F3/06
摘要： Metal oxyalkylates are made by reacting a metal, a carboxylic acid, and hydrogen peroxide in aqueous reaction mixture. The metal oxyalkylate is precipitated and removed from the reaction mixture in high yield and with high purity. The compound is effective in supplying the metal to plants, animals and humans.
摘要翻译：金属烷氧基化物是通过在水性反应混合物中使金属，羧酸和过氧化氢反应制得的。以高产率和高纯度沉淀并从反应混合物中除去金属烷氧基化物。该化合物有效地将金属供应给植物，动物和人类。

2. 发明授权

US4407818A Anti viral, anti bacterial and/or anti fungal composition containing metal oxyalkylate 失效
标题翻译：含有金属烷氧基化物的抗病毒，抗细菌和/或抗真菌组合物
公开(公告)号：US4407818A
公开(公告)日：1983-10-04
申请号：US304303
申请日：1981-09-21
申请人： Joseph E. Lionelle , Jeffrey A. Staffa
发明人： Joseph E. Lionelle , Jeffrey A. Staffa
IPC分类号： A23K1/175 , C07C53/06 , C07C53/10 , C07C53/122 , C07C53/124 , C07C53/126 , C07F3/06 , C07F13/00 , A61K31/045 , A01N55/02
CPC分类号： C07C53/126 , A23K20/30 , C07C53/06 , C07C53/10 , C07C53/122 , C07C53/124 , C07F13/005 , C07F3/06 , Y10S514/934
摘要： An anti viral, anti bacterial and/or anti fungal composition comprises the reaction product of a metal, a carboxylic acid, and hydrogen peroxide. A typical composition comprises zinc, hexakis(acetato)oxotetra (or "zinc oxyacetate"). The composition is useful to treat several types of viruses, bacteria, and/or fungi. The zinc compound is particularly effective against Herpes virus, including Herpes simplex types I and II.
摘要翻译：抗病毒，抗细菌和/或抗真菌组合物包含金属，羧酸和过氧化氢的反应产物。典型的组合物包含锌，六（乙酰）氧基四（或“氧乙酸锌”）。该组合物可用于治疗几种类型的病毒，细菌和/或真菌。锌化合物对疱疹病毒特别有效，包括I型和II型单纯疱疹病毒。

3. 发明授权

US4347321A Method and apparatus for producing alcohol 失效
标题翻译：生产酒精的方法和设备
公开(公告)号：US4347321A
公开(公告)日：1982-08-31
申请号：US194850
申请日：1980-10-07
申请人： Joseph E. Lionelle , Jeffrey A. Staffa , William L. McCormick
发明人： Joseph E. Lionelle , Jeffrey A. Staffa , William L. McCormick
IPC分类号： B01D3/00 , B01D3/14 , C12M1/02 , C12P7/06
CPC分类号： B01D3/14 , B01D3/001 , C12M27/02 , C12M41/18 , C12M43/02 , Y02P20/59 , Y02P70/34 , Y10S203/06 , Y10S203/14 , Y10S203/17
摘要： A method and apparatus particularly suitable for the production of alcohol from fermentable substances such as grain. In this method, mash cooking, fermentation, and boiling are carried out sequentially in a single vessel. Boiling produces a first vapor rich in alcohol which is partially condensed to form a liquid condensate and a second vapor which is further enriched in alcohol. The liquid condensate is returned to the vessel and an alcohol product is recovered from the second vapor, preferably without the addition of external heat. Alcohol recovery is effected by passing the second vapor to a second vessel. Vapor from the second vessel is partially condensed to form a third vapor which is still further enriched in alcohol and a liquid condensate which is returned to the second vessel where it is contacted by the second vapor introduced thereto. The apparatus comprises a single vessel for effecting the heating, boiling and fermenting steps and is provided with heating and cooling means for establishing appropriate temperatures for these steps. Partial condensation is achieved in packed columns having cooling means in the upper regions thereof.
摘要翻译：特别适用于从可发酵物质如谷物生产醇的方法和装置。在这种方法中，在单个容器中依次进行醪烹饪，发酵和煮沸。沸腾产生富含醇的第一蒸汽，其部分冷凝以形成液体冷凝物和进一步富含醇的第二蒸气。液体冷凝物返回到容器中，从第二蒸气中回收醇产物，优选不加外加热。通过将第二蒸气传递到第二容器来实现酒精回收。来自第二容器的气体被部分冷凝以形成另外富含醇的第三蒸气和返回到第二容器的液体冷凝物，其中第二蒸气被引入其中的第二蒸气接触。该装置包括用于进行加热，沸腾和发酵步骤的单个容器，并且设置有用于为这些步骤建立适当温度的加热和冷却装置。在其上部区域具有冷却装置的填充柱中实现部分冷凝。

4. 再颁专利

USRE32909E Metal oxycarboxylates and method of making same 失效
标题翻译：金属羟基羧酸盐及其制备方法
公开(公告)号：USRE32909E
公开(公告)日：1989-04-18
申请号：US621859
申请日：1984-06-18
申请人： Joseph E. Lionelle , Jeffrey A. Staffa
发明人： Joseph E. Lionelle , Jeffrey A. Staffa
IPC分类号： C07C53/06 , C07F3/00 , C07F13/00
CPC分类号： C07C53/06 , C07F13/005 , C07F3/003
摘要： Metal oxycarboxylates are made by reacting a metal, a carboxylic acid, and hydrogen peroxide in aqueous reaction mixture. The metal oxycarboxylate is precipitated and removed from the reaction mixture in high yield and with high purity. The compound is effective in supplying the metal to plants, animals and humans.

5. 发明授权

US4297291A Method of preparing the methyl ester of .alpha.-eleostearic acid 失效
标题翻译：制备α-硬脂酸的甲酯的方法
公开(公告)号：US4297291A
公开(公告)日：1981-10-27
申请号：US164567
申请日：1980-06-30
申请人： Joseph E. Lionelle , Jeffrey A. Staffa
发明人： Joseph E. Lionelle , Jeffrey A. Staffa
IPC分类号： C09F7/00 , C11C3/04 , C09F5/02 , C11C3/02
CPC分类号： C09F7/00 , C11C3/04
摘要： A method of preparing the methyl ester of .alpha.-eleostearic acid comprises the following steps:providing a reaction mixture comprising tung oil, methanol, water and a saponification agent;maintaining the temperature of said reaction mixture at a temperature of not more than about 60.degree. C. for a time sufficient to effect saponification of said tung oil;acidifying the saponification reaction mixture while cooling to prevent excess temperature rise to form an aqueous phase and a non-aqueous phase comprising .alpha.-eleostearic acid;separating said aqueous and non aqueous phases;admixing said separated non-aqueous phase and methanol to form an esterification reactor mixture;heating said esterification reaction mixture in the presence of an acidic esterification catalyst to form an aqueous phase and a non-aqueous phase comprising the methyl ester of .alpha.-eleostearic acid; andseparating said aqueous and non aqueous phases of said esterification reaction mixture to provide a non-aqueous product phase comprising the methyl ester of .alpha.-eleostearic acid.
摘要翻译：制备α-硬脂酸的甲酯的方法包括以下步骤：提供包含桐油，甲醇，水和皂化剂的反应混合物; 将所述反应混合物的温度保持在不超过约60℃的温度下足以实现所述桐油皂化的时间; 在冷却时酸化皂化反应混合物以防止过度的温度升高以形成水相和包含α-硬脂酸的非水相; 分离所述水相和非水相; 混合所述分离的非水相和甲醇以形成酯化反应器混合物; 在酸性酯化催化剂的存在下加热所述酯化反应混合物以形成水相和包含α-硬脂酸的甲酯的非水相; 并分离所述酯化反应混合物的所述水相和非水相以提供包含α-硬脂酸的甲酯的非水产物相。

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