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1. 发明授权

US06852873B2 Preparation of styryl dyes 失效
标题翻译：苯乙烯基染料的制备
公开(公告)号：US06852873B2
公开(公告)日：2005-02-08
申请号：US10223547
申请日：2002-08-19
申请人： Josef-Walter Stawitz , Stephan Michaelis , Christoph Thiebes
发明人： Josef-Walter Stawitz , Stephan Michaelis , Christoph Thiebes
IPC分类号： C07C253/30 , C07C255/42 , C08K5/315 , C09B23/00 , C09B23/14 , D06P1/00 , D06P3/52 , C09B1/00
CPC分类号： C09B23/143
摘要： Process for preparing compounds of the formula (I) where R1, R2 and R3 are independently hydrogen, alkyl or cycloalkyl, characterized in that an aldehyde of the formula (II) is reacted with CH2(CN)2 in the presence of butanol.
摘要翻译：制备式（I）化合物的方法其中R 1，R 2和R 3独立地是氢，烷基或环烷基，其特征在于式（II）的醛与CH 2（CN） 2在丁醇存在下。

2. 发明授权

US06833455B2 Bridged perinones/quinophthalones 失效
标题翻译：桥联perinones / quinophthalones
公开(公告)号：US06833455B2
公开(公告)日：2004-12-21
申请号：US10302186
申请日：2002-11-22
申请人： Christoph Thiebes , Josef-Walter Stawitz , Ulrich Feldhues
发明人： Christoph Thiebes , Josef-Walter Stawitz , Ulrich Feldhues
IPC分类号： C07D40112
CPC分类号： C09B25/00 , C07D215/20 , C09B57/12
摘要： Disclosed herein are bridged perinones/quinophthalones of the general formula (I) or tautomeric forms thereof where X1, X2, Ar1 Ar2 and B are as described herein and are particularly characterized in that the bridging B is a radical of the formula —T1—W—T2—, where T1 and T2 are independently O or S and W is alkylene, especially C1-C6-alkylene, C6-C10-arylene, especially phenylene or cycloalkylene, which are each optionally substituted or is the radical of the formula (a) where the phenyl rings are optionally substituted and A is a radical of the formula O, S, SO, SO2 or CO, optionally substituted alkylene, or optionally substituted cycloalkylene, said alkylene or cycloalkylene being attached to the adjacent phenyl rings itself or else via its substitutents, or W is a radical of the formulae where s and t are independently from 1 to 6, the ends of the radical B each being attached to an aromatic carbon atom of the two radicals Ar1 and Ar2. EINBETTENEINBETTEN
摘要翻译：本文公开了通式（I）的桥联环戊二烯酮/喹酞酮或其互变异构体，其中X1，X2，Ar1Ar2和B如本文所述，其特征在于桥连B是式-T1-W- T2-，其中T1和T2独立地是O或S，W是亚烷基，特别是C1-C6-亚烷基，C6-C10-亚芳基，特别是亚苯基或亚环烷基，它们各自任选被取代或者是式（a）的基团，其中苯环任选被取代，并且A是式O，S，SO，SO 2或CO，任选取代的亚烷基或任选取代的亚环烷基的基团，所述亚烷基或亚环烷基本身连接至相邻的苯环，或通过其取代基或者W是式的基团，其中s和t独立地为1至6，基团B的末端各自连接到两个基团Ar 1和Ar 2的芳族碳原子上。 EINBETTENEINBETTEN

3. 发明授权

US06884899B2 Preparation of 1-amino-4-hydroxyanthraquinones 失效
标题翻译： 1-氨基-4-羟基蒽醌的制备
公开(公告)号：US06884899B2
公开(公告)日：2005-04-26
申请号：US10219795
申请日：2002-08-15
申请人： Christoph Thiebes , Josef-Walter Stawitz
发明人： Christoph Thiebes , Josef-Walter Stawitz
IPC分类号： C07B61/00 , C07C221/00 , C07C225/36 , C07C231/12 , C07C233/43 , C09B1/514 , C09B1/20
CPC分类号： C09B1/5145 , C07C221/00 , C07C231/12 , C07C2603/24 , C07C225/36 , C07C233/43
摘要： The present invention relates to a process for preparing 1-amino-4-hydroxyanthraquinones of the formula (I) wherein R is an aliphatic or aromatic radical, by reacting 1,4-dihydroxyanthraquinone, optionally as a mixture with 2,3-dihydro-1,4-dihydroxyanthraquinone, with aliphatic or aromatic amines in the presence of N-methyl-2-pyrrolidone.
摘要翻译：本发明涉及通过使1,4-二羟基蒽醌，任选地作为与2,3-二氢 - 吡喃酮的混合物反应制备式（I）的1-氨基-4-羟基蒽醌的方法，其中R是脂族或芳族基团， 1,4-二羟基蒽醌与脂族或芳族胺在N-甲基-2-吡咯烷酮的存在下反应。

4. 发明授权

US06465659B2 Process for preparing asymmetrical methine dyes 有权
标题翻译：制备不对称次甲基染料的方法
公开(公告)号：US06465659B2
公开(公告)日：2002-10-15
申请号：US10090684
申请日：2002-03-05
申请人： Josef-Walter Stawitz , Karl-Heinz Reinhardt , Christoph Thiebes
发明人： Josef-Walter Stawitz , Karl-Heinz Reinhardt , Christoph Thiebes
IPC分类号： C07D40306
CPC分类号： C09B23/105 , C08K5/3445 , C09B67/0033
摘要： Reaction of pyrazolones and methyleneindolines with orthoformic esters is an advantageous one-step process for preparing asymmetrical methine dyes.
摘要翻译：吡唑啉酮和亚甲基吲哚啉与原甲酸酯的反应是制备不对称次甲基染料的有利的一步法。

5. 发明申请

US20050070683A1 Solidification-stable blocked polyisocyanates 审中-公开
标题翻译：固化稳定的封端多异氰酸酯
公开(公告)号：US20050070683A1
公开(公告)日：2005-03-31
申请号：US10847529
申请日：2004-05-17
申请人： Christoph Thiebes , Frank Richter , Reinhard Halpaap , Beate Baumbach , Dieter Mager , Christian Fussel
发明人： Christoph Thiebes , Frank Richter , Reinhard Halpaap , Beate Baumbach , Dieter Mager , Christian Fussel
IPC分类号： C08G18/73 , C08G18/78 , C08G18/80 , C09D175/06 , C08G18/00
CPC分类号： C08G18/7831 , C08G18/73 , C08G18/808 , C08G18/8093 , C08G18/8096 , C09D175/06
摘要： Storage-stable Polyisocyanates based on aliphatic and/or cycloaliphatic diisocyanates including from 1 to 20% by weight of alkylamino groups of the formula R1R2N as a constituent of biuret groups, wherein R1 and R2 independently of one another are aliphatic or cycloaliphatic C1-C12 alkyl radicals, and where at least 95 mol % of the isocyanate groups are blocked with at least one blocking agent, and the polyisocyanates contain from 4.0 to 21.0% by weight of blocked and free NCO groups (calculated as NCO, molecular weight=42). The polyisocyanates are used to produce coating compositions, coatings, and coated substrates.
摘要翻译：基于脂族和/或脂环族二异氰酸酯的储存稳定的聚异氰酸酯，包括1至20重量％的式R 1 R 2 N的烷基氨基作为缩二脲基的组分，其中R 1和R 2， 2>彼此独立地是脂族或脂环族C 1 -C 12烷基，并且其中至少95摩尔％的异氰酸酯基团被至少一个封闭剂封闭，并且多异氰酸酯含有4.0至21.0重量％的封闭和游离NCO基团（按NCO计算，分子量= 42）。多异氰酸酯用于生产涂料组合物，涂料和涂布的基材。

6. 发明授权

US07087676B2 Blocked polyisocyanates 失效
标题翻译：封闭的多异氰酸酯
公开(公告)号：US07087676B2
公开(公告)日：2006-08-08
申请号：US10874716
申请日：2004-06-23
申请人： Jan Mazanek , Reinhard Halpaap , Markus Mechtel , Thomas Klimmasch , Christoph Thiebes
发明人： Jan Mazanek , Reinhard Halpaap , Markus Mechtel , Thomas Klimmasch , Christoph Thiebes
IPC分类号： C08G18/80 , C07C275/08 , C07C275/12 , C07C275/14 , C07C275/16
CPC分类号： C08G18/6216 , C08G18/792 , C08G18/807 , C09D175/04
摘要： Blocked polyisocyanates and one-component stoving systems containing these blocked polyisocyanates, and the preparation thereof and their use for the preparation of lacquers, paints, adhesives and elastomers, wherein blocked polyisocyanates are prepared by reacting polyisocyanates with secondary amines corresponding to the formula wherein R1—R4 can be identical or different and denote hydrogen, C1–C6-alkyl or cycloalkyl, R5 denotes C1–C10-alkyl, C3–C10-cycloalkyl, y denotes a number from 2 to 8, and B represents wherein R6–R8 can be identical or different and independently of one another denote C1–6-alkyl and/or C3–C6-cycloalkyl, R9 denotes hydrogen or C1–6-alkyl or C3–C6-cycloalkyl.
摘要翻译：封闭的多异氰酸酯和含有这些封端的多异氰酸酯的单组分烘烤系统及其制备及其用于制备漆，油漆，粘合剂和弹性体的用途，其中封端的多异氰酸酯是通过使多异氰酸酯与对应于下式的仲胺反应来制备的：可以相同或不同，表示氢，C 1 -C 6 - 烷基或环烷基， R 5表示C 1 -C 10 - 烷基，C 3 -C 10烷基，C 3 -C 10 - 烷基，C 3 -C 10 - > - 环烷基，y表示2至8的数，B表示其中R 6 -R 8可以相同或不同，并且彼此独立地表示C _{表示氢或C 1 -C 6 - 烷基或C 3 -C 6 - 环烷基。}

7. 发明申请

US20050129847A1 Coatings for food containers 有权
标题翻译：食品容器用涂料
公开(公告)号：US20050129847A1
公开(公告)日：2005-06-16
申请号：US10969144
申请日：2004-10-20
申请人： Christoph Thiebes , Beate Baumbach , Eduard Hansel , Wolfram Kuttner , Christian Wamprecht
发明人： Christoph Thiebes , Beate Baumbach , Eduard Hansel , Wolfram Kuttner , Christian Wamprecht
IPC分类号： B65D25/14 , B05D7/14 , B05D7/22 , B05D7/24 , B65D25/34 , B65D81/24 , C08G18/00 , C08G18/40 , C08G18/42 , C08G18/54 , C08G18/62 , C08G18/68 , C08G18/79 , C08G18/80 , C09D5/46 , C09D175/00 , C09D175/04 , C09D175/06 , C09D175/14 , C09D179/00
CPC分类号： C09D175/14 , C08G18/542 , C08G18/68 , C08G18/792 , C08G18/8074 , C08G2390/40
摘要： The present invention relates to inner coatings of metal food containers and packaging and to a process for their production. The coatings are appied to the inside of at least a portion of the surface area of containers that are in direct contact with foods or other consumable products and subsequently cured. The coatings include a) at least one polyisocyanate containing an average of at least two NCO groups per molecule, at least 95% of the NCO groups being blocked with a blocking agent, and b) at least one polyhydroxyl compound containing an average of at least two hydroxyl groups per molecule that react with NCO groups.
摘要翻译：本发明涉及金属食品容器和包装的内部涂层及其生产方法。将涂层施用到与食品或其他消耗品直接接触并随后固化的容器表面区域的至少一部分的内部。涂层包括a）至少一种每分子平均含有至少两个NCO基团的多异氰酸酯，至少95％的NCO基团用封闭剂封闭，和b）至少一种至少含有至少一个平均值的多羟基化合物每个分子的两个羟基与NCO基团反应。

8. 发明申请

US20050107565A1 Polyisocyanates with biuret structure, blocked with secondary amines 审中-公开
标题翻译：具有缩二脲结构的聚异氰酸酯，被仲胺封端
公开(公告)号：US20050107565A1
公开(公告)日：2005-05-19
申请号：US10966792
申请日：2004-10-15
申请人： Christoph Thiebes , Reinhard Halpaap , Beate Baumbach , Dieter Mager , Christian Fussel
发明人： Christoph Thiebes , Reinhard Halpaap , Beate Baumbach , Dieter Mager , Christian Fussel
IPC分类号： C07C275/62 , C07B61/00 , C07C211/02 , C07C263/18 , C07C265/14 , C07C275/00 , C08G18/00 , C08G18/02 , C08G18/28 , C08G18/32 , C08G18/78 , C08G18/79 , C08G18/80 , C08J7/04 , C09D175/04 , C09D175/12
CPC分类号： C08G18/7887 , C08G18/281 , C08G18/2865 , C08G18/7831 , C08G18/792 , C08G18/808
摘要： Storage-stable blocked polyisocyanates prepared by reacting one or more polyisocyanates with one or more biuretizing agents and optionally, catalysts such that in the blocked end product there are 5-45 equivalent percent of biuret groups according to formula (I) based on the sum total of all free and blocked NCO groups; optionally modifying the resulting biuret polyisocyanates with the aid of isocyanate-reactive compounds and/or catalysts, with further reaction of free NCO groups; and subsequently blocking at least 95 mol percent of the remaining free NCO groups with a blocking agent according to the formula R1R2NH, where R1 and R2 independently of one another are aliphatic or cycloaliphatic C1-C12 alkyl radicals. The blocked polyisocyanates can be used to make polyurethane polymers and coating compositions, which can be used to coat substrates.
摘要翻译：通过使一种或多种多异氰酸酯与一种或多种缩二脲化试剂和任选的催化剂反应制备的储存稳定的封端多异氰酸酯，使得在封端产物中，根据式（I），基于总计的总数为5-45当量的缩二脲基团的所有自由和封闭的NCO团体; 任选地在异氰酸酯反应性化合物和/或催化剂的帮助下改性所得缩二脲多异氰酸酯，进一步反应游离NCO基团; 随后用封闭剂将根据式R 1 R 2 NH封闭至少95mol％剩余的游离NCO基团，其中R 1，各自独立地是脂族或脂环族C 1 -C 12烷基。封端的多异氰酸酯可用于制备可用于涂覆基材的聚氨酯聚合物和涂料组合物。

9. 发明授权

US07517559B2 Coatings for food containers 有权
标题翻译：食品容器用涂料
公开(公告)号：US07517559B2
公开(公告)日：2009-04-14
申请号：US10969144
申请日：2004-10-20
申请人： Christoph Thiebes , Beate Baumbach , Eduard Hänsel , Wolfram Küttner , Christian Wamprecht
发明人： Christoph Thiebes , Beate Baumbach , Eduard Hänsel , Wolfram Küttner , Christian Wamprecht
IPC分类号： B05D3/02
CPC分类号： C09D175/14 , C08G18/542 , C08G18/68 , C08G18/792 , C08G18/8074 , C08G2390/40
摘要： The present invention relates to inner coatings of metal food containers and packaging and to a process for their production. The coatings are applied to the inside of at least a portion of the surface area of containers that are in direct contact with foods or other consumable products and subsequently cured. The coatings include a) at least one polyisocyanate containing an average of at least two NCO groups per molecule, at least 95% of the NCO groups being blocked with a blocking agent, and b) at least one polyhydroxyl compound containing an average of at least two hydroxyl groups per molecule that react with NCO groups.
摘要翻译：本发明涉及金属食品容器和包装的内部涂层及其生产方法。将涂层施加到与食品或其他消费品直接接触的容器表面区域的至少一部分的内部，并随后固化。涂层包括a）至少一种每分子平均含有至少两个NCO基团的多异氰酸酯，至少95％的NCO基团用封闭剂封闭，和b）至少一种至少含有至少一个平均值的多羟基化合物每个分子的两个羟基与NCO基团反应。

10. 发明授权

US07074852B2 Blocked polyisocyanates 失效
标题翻译：封闭的多异氰酸酯
公开(公告)号：US07074852B2
公开(公告)日：2006-07-11
申请号：US10874988
申请日：2004-06-23
申请人： Jan Mazanek , Christoph Thiebes , Jürgen Meixner , Olaf Fleck , Heino Müller
发明人： Jan Mazanek , Christoph Thiebes , Jürgen Meixner , Olaf Fleck , Heino Müller
IPC分类号： C08G18/80 , C08L75/00 , C09D175/00 , C08J3/03 , C07C275/06
CPC分类号： C09D175/06 , C08G18/0823 , C08G18/10 , C08G18/12 , C08G18/3206 , C08G18/348 , C08G18/6659 , C08G18/792 , Y10T428/31551 , Y10T428/31591 , Y10T428/31598 , Y10T428/31601 , Y10T428/31605 , C08G18/8048 , C08G18/2865
摘要： Blocked polyisocyanates and one-component stoving systems containing these blocked polyisocyanates, and the preparation thereof and their use for the preparation of lacquers, paints, adhesives and elastomers. The blocked polyisocyanates are derived from polyisocyanates reacted with secondary amines and cationic, anionic and/or nonionic hydrophilizing agents such that they are incorporated into the polyisocyanate at a ratio of from 20:1 to 1:1, wherein the blocking agents correspond to the formula R1–R4 can be identical or different and independently of one another denote hydrogen, C1–C6-alkyl or C3–C6-cycloalkyl, R5 denotes C1–C10-alkyl, C3–C10-cycloalkyl, and B represents wherein R6–R8 can be identical or different and independently of one another denote C1–C6-alkyl and/or C1–C6-cycloalkyl, R9 denotes hydrogen or C3–C6-alkyl or C3–C6-cycloalkyl.
摘要翻译：封闭的多异氰酸酯和含有这些封端多异氰酸酯的单组分烘烤系统及其制备方法及其用于制备漆，油漆，粘合剂和弹性体的用途。封端的多异氰酸酯衍生自与仲胺和阳离子，阴离子和/或非离子亲水剂反应的多异氰酸酯，使得它们以20:1至1:1的比例掺入多异氰酸酯中，其中封闭剂对应于式 R 1〜R 4可以相同或不同，彼此独立地表示氢，C 1 -C 6 > - 烷基或C 3 -C 6 - 环烷基，R 5表示C 1 -C 6 - 10个 - 烷基，C 3 -C 10 - 环烷基，B表示其中R 6 -R 8， / SUP>可以相同或不同，彼此独立地表示C 1 -C 6 - 烷基和/或C 1 -C 6 - R 6表示氢或C 3 -C 6 - 烷基或C 3 - C 6 -C 6 - 环烷基。

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