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1. 发明授权

US08093332B2 High impact polystyrene and process for preparing same 失效
标题翻译：高抗冲聚苯乙烯及其制备方法
公开(公告)号：US08093332B2
公开(公告)日：2012-01-10
申请号：US10674224
申请日：2003-09-29
申请人： Jose M. Sosa , Billy J. Ellis
发明人： Jose M. Sosa , Billy J. Ellis
IPC分类号： C08G63/48 , C08G63/91 , C08L51/00 , C08F2/00 , C08F4/04 , C08F4/32 , C08F4/38 , C08F281/00
CPC分类号： C08L25/06 , C08F279/02 , C08F287/00 , C08L9/00 , C08L51/006 , C08L51/04 , C08L2666/02
摘要： Disclosed are high impact polystyrenes prepared using mixed initiators. The mixed initiators include at least one grafting initiator and one non-grafting initiator. The high impact polystyrenes prepared therewith have a continuous polystyrene phase and dispersed therein particles of rubber predominantly having a honeycomb structure of rubber with polystyrene inclusions.
摘要翻译：公开了使用混合引发剂制备的高抗冲聚苯乙烯。混合的引发剂包括至少一个接枝引发剂和一个非接枝引发剂。由此制备的高冲击性聚苯乙烯具有连续的聚苯乙烯相，并且在其中分散有主要具有具有聚苯乙烯夹杂物的橡胶的蜂窝结构的橡胶颗粒。

2. 发明授权

US06437043B1 Process and apparatus for continuous manufacture of elastomer-modified monovinylaromatic compounds 失效
标题翻译：用于连续制造弹性体改性单乙烯基芳族化合物的方法和设备
公开(公告)号：US06437043B1
公开(公告)日：2002-08-20
申请号：US09951599
申请日：2001-09-13
申请人： Jose M. Sosa , Billy J. Ellis
发明人： Jose M. Sosa , Billy J. Ellis
IPC分类号： C08F27902
CPC分类号： C08F279/02 , C08F287/00 , C08F297/04
摘要： The present invention discloses processes and apparatus for the efficient and rapid conversion of an elastomeric monomer to a polymerized elastomer, and conjointly, reaction of the resultant rubbery polymer into a monovinylaromatic polymerization reaction to form a rubber-modified polymer; and more specifically teaches a method of polymerizing butadiene and reacting it with styrene monomer to form a transparent rubber-modified impact-resistant polystyrene material exhibiting elastomer concentrations that range from as low as 6 weight percent or lower, to as high as about 50 percent.
摘要翻译：本发明公开了将弹性体单体有效快速地转化成聚合弹性体的方法和装置，并且将所得的橡胶状聚合物共同反应成单乙烯基芳族聚合反应以形成橡胶改性的聚合物; 并且更具体地教导了聚合丁二烯并使其与苯乙烯单体反应的方法，以形成透明橡胶改性的耐冲击聚苯乙烯材料，其显示范围为低至6重量％或更低的弹性体浓度至高达约50％。

3. 发明申请

US20120208913A1 Use of Polar Additives for Enhancing Blowing Agent Solubility in Polystyrene 有权
标题翻译：使用极性添加剂提高聚苯乙烯中的发泡剂溶解度
公开(公告)号：US20120208913A1
公开(公告)日：2012-08-16
申请号：US13347704
申请日：2012-01-11
申请人： Wei Wang , Jose M. Sosa , David W. Knoeppel
发明人： Wei Wang , Jose M. Sosa , David W. Knoeppel
IPC分类号： C08J9/00 , C08L25/18
CPC分类号： C08J9/0014 , C08J9/12 , C08J9/142 , C08J2203/06 , C08J2203/12 , C08J2325/04 , C08J2325/08 , C08L25/06 , C08L35/06
摘要： Foamable polystyrene compositions with enhanced blowing agent solubility and methods of making such polystyrene compositions by incorporating a polar additive in styrenic polymer or copolymers.
摘要翻译：具有增强的发泡剂溶解度的可发泡聚苯乙烯组合物和通过将极性添加剂掺入苯乙烯聚合物或共聚物中制备这种聚苯乙烯组合物的方法。

4. 发明申请

US20120178873A1 Copolymers of Styrene With Alkyl Acrylates and/or Alkyl Methacrylates 审中-公开
标题翻译：苯乙烯与丙烯酸烷基酯和/或烷基甲基丙烯酸酯的共聚物
公开(公告)号：US20120178873A1
公开(公告)日：2012-07-12
申请号：US13323853
申请日：2011-12-13
申请人： Jay Reimers , Jose M. Sosa
发明人： Jay Reimers , Jose M. Sosa
IPC分类号： C08L25/14 , C08K5/01 , C08F220/18
CPC分类号： C08L25/14 , C08L91/00
摘要： A styrenic copolymer composition including at least one alkyl acrylate and/or alkyl methacrylate comonomer, in which the styrenic copolymer composition is optically clear and has at least two times the impact strength compared to general-purpose polystyrene.
摘要翻译：包含至少一种丙烯酸烷基酯和/或甲基丙烯酸烷基酯共聚单体的苯乙烯共聚物组合物，其中苯乙烯共聚物组合物是光学透明的并且具有与通用聚苯乙烯相比的冲击强度的至少两倍。

5. 发明申请

US20100197843A1 Composites Comprising a Polymer and a Selected Layered Compound and Methods of Preparing and Using Same 审中-公开
标题翻译：包含聚合物和选择的分层化合物的复合材料及其制备和使用方法
公开(公告)号：US20100197843A1
公开(公告)日：2010-08-05
申请号：US12365113
申请日：2009-02-03
申请人： Jose M. Sosa , Luyi Sun , Billy Ellis
发明人： Jose M. Sosa , Luyi Sun , Billy Ellis
IPC分类号： C08K9/00 , C08K5/16 , C08K5/098 , C08K5/101 , C08K3/34
CPC分类号： C08F2/44 , B82Y30/00 , C08F290/06 , C08F292/00 , C08K3/346 , C08K5/098 , C08K5/19 , C08K9/04 , C08L21/00 , C08F220/04 , C08F220/20 , C08F212/08 , C08L51/04
摘要： A method of producing a polymer and layered compound composition having a high degree of exfoliation of the layered compound is disclosed. The layered compound is treated with chemicals having an affinity with the polymer or the monomer of the polymer. The monomer and the layered compound can be combined prior to polymerization. The polymer and layered compound can be combined by solution mixing in a solvent. The layered compound can also be incorporated into the mixture by compounding a polymer product with the layered compound.
摘要翻译：公开了一种具有高分层化合物剥离性的聚合物和层状化合物组合物的制造方法。层状化合物用与聚合物或聚合物单体具有亲和性的化学品处理。单体和层状化合物可以在聚合之前进行组合。聚合物和层状化合物可以通过在溶剂中的溶液混合来组合。层状化合物也可以通过将聚合物产物与层状化合物混合而掺入混合物中。

6. 发明授权

US07754817B2 Low temperature initiators for improving the rubber phase volume of HIPS formulations 有权
标题翻译：用于改善HIPS配方橡胶相体积的低温引发剂
公开(公告)号：US07754817B2
公开(公告)日：2010-07-13
申请号：US11262641
申请日：2005-10-31
申请人： Jose M. Sosa , Shazia Ullah
发明人： Jose M. Sosa , Shazia Ullah
IPC分类号： C08F263/00 , C08F293/00
CPC分类号： C08F279/02 , C08L51/04 , C08L2666/02
摘要： Peroxide initiators are disclosed that can be used at lower temperatures during HIPS production. Enhanced formation of graft polymers between polystyrene and polybutadiene (rubber) can be accomplished by using these lower temperature peroxide initiators that have a 1 hour half-life period at one or more temperatures from 95° C. to less than 111° C. during the pre-inversion stage. “Higher” temperature initiators are used during and/or after inversion. The use of such “low” temperature initiators improves polymerization rates and grafting values, while reducing the swell index and the amount of rubber used, thereby producing improved HIPS more rapidly and at a lower cost. Also disclosed are HIPS compositions and products produced by such “low” temperature initiators as well as a method of producing improved HIPS.
摘要翻译：公开了可以在HIPS生产期间在较低温度下使用的过氧化物引发剂。在聚苯乙烯和聚丁二烯（橡胶）之间增强的接枝聚合物的形成可以通过使用这些低温过氧化物引发剂来实现，该引发剂在一个或多个温度从95℃到小于111℃的时间内具有1小时的半衰期预转换阶段。在反转期间和/或之后使用“较高”的温度引发剂。使用这种“低”温度引发剂提高了聚合速率和接枝值，同时降低了溶胀指数和使用的橡胶的量，从而以更低的成本更快速地生产改进的HIPS。还公开了由这种“低”温度引发剂生产的HIPS组合物和产物以及生产改进的HIPS的方法。

7. 发明申请

US20080021157A1 POLYSTYRENE HAVING IMPROVED COLOR AND METHODS OF MAKING SAME 审中-公开
标题翻译：具有改进颜色的聚苯乙烯及其制备方法
公开(公告)号：US20080021157A1
公开(公告)日：2008-01-24
申请号：US11456297
申请日：2006-07-10
申请人： Jose M. Sosa , Billy Ellis , Steven D. Gray
发明人： Jose M. Sosa , Billy Ellis , Steven D. Gray
IPC分类号： C08L9/00 , C08L25/04 , B32B27/00
CPC分类号： C08F279/02 , C08K5/005 , C08K5/0091 , C08L51/04 , C08L2666/04 , C08L2666/02
摘要： A method of improving the color of a high impact polystyrene comprising preparing a reaction mixture comprising styrene, elastomer and at least one antioxidant, and introducing to the reaction mixture a color improving additive prior to the addition of any oxidizing agents to the reaction mixture. A high impact polystyrene comprising a color improving additive, an elastomer and at least one antioxidant wherein the color improving additive is present in the reaction process for production of the high impact polystyrene prior to the introduction of an oxidizing agent and wherein the high impact polystyrene has a 50% to 200% reduction in the Yellowness index as determined in accordance with ASTM E 313 when compared to an otherwise identical polystyrene lacking a color improving additive.
摘要翻译：一种改善高抗冲聚苯乙烯颜色的方法，包括制备包含苯乙烯，弹性体和至少一种抗氧化剂的反应混合物，并在向反应混合物中加入任何氧化剂之前向反应混合物中引入增色剂。包含改色添加剂，弹性体和至少一种抗氧化剂的高抗冲聚苯乙烯，其中在引入氧化剂之前，用于生产高抗冲聚苯乙烯的反应过程中存在改色添加剂，其中高抗冲聚苯乙烯具有当与没有改色添加剂的其他相同的聚苯乙烯相比时，根据ASTM E 313测定的黄度指数降低50％至200％。

8. 发明授权

US07179873B2 Branched ionomers 有权
公开(公告)号：US07179873B2
公开(公告)日：2007-02-20
申请号：US11043595
申请日：2005-01-26
申请人： Jay Reimers , Jose M. Sosa
发明人： Jay Reimers , Jose M. Sosa
IPC分类号： C08F30/04 , C08F20/00 , C08I31/00
CPC分类号： C08F212/08 , C08F220/06 , C08K5/0091 , C08L35/00
摘要： A branched aromatic ionomer is prepared by co-polymerizing a first monomer having an aromatic moiety and an unsaturated alkyl moiety and a second monomer having an ionic moiety and at least one unsaturated moiety. The ionic moiety may have a cationic group having a valence of +1 or greater. Styrene is among the useful first monomers and sodium methacrylate and zinc dimethacrylate are among the useful second monomers. The branched aromatic ionomers may be used to prepare articles including foamed polystyrene and microwave save dishes and utensils.

9. 发明授权

US5540813A Method for reducing volatiles in polymerized styrene 失效
标题翻译：降低聚合苯乙烯挥发物的方法
公开(公告)号：US5540813A
公开(公告)日：1996-07-30
申请号：US184085
申请日：1994-01-19
申请人： Jose M. Sosa , Robert M. Scates , James N. Weguespack , Bruce P. Blackmar , Scott W. Davis
发明人： Jose M. Sosa , Robert M. Scates , James N. Weguespack , Bruce P. Blackmar , Scott W. Davis
IPC分类号： C08F6/10 , C08F6/00 , C08F6/06 , B01D1/00
CPC分类号： C08F6/001
摘要： Methods and apparatus are disclosed for purifying polymerized monovinyl aromatic compounds such as polystyrene by reducing the residual monomer content of the finished polymer, said methods and apparatus including a combination of heat exchangers and devolatilizers used in conjunction with a monovinyl aromatic polymerization reactor system.
摘要翻译：公开了通过降低成品聚合物的残余单体含量来纯化聚合的单乙烯基芳族化合物如聚苯乙烯的方法和装置，所述方法和设备包括与单乙烯基芳族聚合反应器系统结合使用的热交换器和脱挥发份的组合。

10. 发明授权

US4857587A Continuous process including recycle stream treatment for the production of high impact polystyrene 失效
标题翻译：连续工艺包括用于生产高抗冲聚苯乙烯的循环流处理
公开(公告)号：US4857587A
公开(公告)日：1989-08-15
申请号：US137743
申请日：1987-12-24
申请人： Jose M. Sosa , Jeffrey Morris
发明人： Jose M. Sosa , Jeffrey Morris
IPC分类号： C08F2/00 , C08F279/02
CPC分类号： C08F279/02
摘要： A continuous flow process for the production of high impact polystyrene, wherein specific types of polymerization inhibiting impurities are removed from a recycle stream prior to feeding or introducing the recycle stream into a styrene polymerization zone. Preferably, the process further comprises the step of monitoring the acidity of the recycle stream.
摘要翻译：用于生产高抗冲聚苯乙烯的连续流动方法，其中在将循环物流进料或引入苯乙烯聚合区之前，将循环流中的特定类型的聚合抑制杂质除去。优选地，该方法还包括监测再循环流的酸度的步骤。

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