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1. 发明授权

US08389636B2 Polystyrene blends 有权
标题翻译：聚苯乙烯共混物
公开(公告)号：US08389636B2
公开(公告)日：2013-03-05
申请号：US13530212
申请日：2012-06-22
申请人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corletto
发明人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corletto
IPC分类号： C08L25/02
CPC分类号： C08L25/06 , C08L2205/02 , C08L2207/20
摘要： A method of preparing a polystyrene blend that includes combining a first polystyrene composition having a first melt flow index with a second polystyrene composition having a second melt flow index and forming a polystyrene blend, the second melt flow index being at least 2 dg/min higher that the first melt flow index. The polystyrene blend has an observed tensile strength value greater than 3% above the expected tensile strength value. The second polystyrene composition can include a recycled polystyrene material, which can include expanded polystyrene. An alternate method of preparing the polystyrene blend includes combining a polystyrene composition with a styrene monomer to form a reaction mixture, polymerizing the reaction mixture and obtaining a polystyrene blend, where the polystyrene containing composition has a melt flow index at least 2 dg/min higher than the melt flow index of the styrene monomer after it has been polymerized.
摘要翻译：一种制备聚苯乙烯共混物的方法，其包括将具有第一熔体流动指数的第一聚苯乙烯组合物与具有第二熔体流动指数的第二聚苯乙烯组合物组合并形成聚苯乙烯共混物，所述第二熔体流动指数至少为2dg / min 第一个熔体流动指数。聚苯乙烯共混物的观测拉伸强度值大于预期拉伸强度值的3％以上。第二聚苯乙烯组合物可以包括再循环的聚苯乙烯材料，其可以包括发泡聚苯乙烯。制备聚苯乙烯共混物的替代方法包括将聚苯乙烯组合物与苯乙烯单体组合以形成反应混合物，使反应混合物聚合并获得聚苯乙烯共混物，其中含聚苯乙烯的组合物的熔体流动指数至少为2dg / min 比苯乙烯单体聚合后的熔体流动指数高。

2. 发明申请

US20120259071A1 Polystyrene Blends 有权
标题翻译：聚苯乙烯共混物
公开(公告)号：US20120259071A1
公开(公告)日：2012-10-11
申请号：US13530212
申请日：2012-06-22
申请人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corleto
发明人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corleto
IPC分类号： C08L25/06
CPC分类号： C08L25/06 , C08L2205/02 , C08L2207/20
摘要： A method of preparing a polystyrene blend that includes combining a first polystyrene composition having a first melt flow index with a second polystyrene composition having a second melt flow index and forming a polystyrene blend, the second melt flow index being at least 2 dg/min higher that the first melt flow index. The polystyrene blend has an observed tensile strength value greater than 3% above the expected tensile strength value. The second polystyrene composition can include a recycled polystyrene material, which can include expanded polystyrene. An alternate method of preparing the polystyrene blend includes combining a polystyrene composition with a styrene monomer to form a reaction mixture, polymerizing the reaction mixture and obtaining a polystyrene blend, where the polystyrene containing composition has a melt flow index at least 2 dg/min higher than the melt flow index of the styrene monomer after it has been polymerized.
摘要翻译：一种制备聚苯乙烯共混物的方法，其包括将具有第一熔体流动指数的第一聚苯乙烯组合物与具有第二熔体流动指数的第二聚苯乙烯组合物组合并形成聚苯乙烯共混物，所述第二熔体流动指数至少为2dg / min 第一个熔体流动指数。聚苯乙烯共混物的观测拉伸强度值大于预期拉伸强度值的3％以上。第二聚苯乙烯组合物可以包括再循环的聚苯乙烯材料，其可以包括发泡聚苯乙烯。制备聚苯乙烯共混物的替代方法包括将聚苯乙烯组合物与苯乙烯单体组合以形成反应混合物，使反应混合物聚合并获得聚苯乙烯共混物，其中含聚苯乙烯的组合物的熔体流动指数至少为2dg / min 比苯乙烯单体聚合后的熔体流动指数高。

3. 发明申请

US20110306691A1 Foamed Articles Exhibiting Improved Thermal Properties 有权
标题翻译：展示改善热性能的发泡制品
公开(公告)号：US20110306691A1
公开(公告)日：2011-12-15
申请号：US13153776
申请日：2011-06-06
申请人： Jose Sosa , David W. Knoeppel
发明人： Jose Sosa , David W. Knoeppel
IPC分类号： C08J9/35 , C08L25/06 , C08K3/22
CPC分类号： C08J9/28 , B29C44/08 , C08J9/0066 , C08J9/122 , C08J9/125 , C08J2201/03 , C08J2203/06 , C08J2203/10 , C08J2203/182 , C08J2205/042 , C08J2205/044 , C08J2205/048 , C08J2325/04 , C08J2325/06
摘要： Cellular and multi-cellular polystyrene and polystyrenic foams and methods of forming such foams are disclosed. The foams include an expanded polystyrene formed from expansion of an expandable polystyrene including an adsorbent comprising alumina, wherein the multi-cellular polystyrene exhibits a multi-cellular size distribution. The process for forming a foamed article includes providing a formed styrenic polymer and contacting the formed styrenic polymer with a first blowing agent and an adsorbent comprising alumina to form extrusion polystyrene. The process further includes forming the extrusion styrenic polymer into an expanded styrenic polymer and forming the expanded styrenic polymer into a foamed article.
摘要翻译：公开了细胞和多细胞聚苯乙烯和聚苯乙烯泡沫以及形成这种泡沫的方法。泡沫包括由可膨胀聚苯乙烯膨胀形成的发泡聚苯乙烯，其包括包含氧化铝的吸附剂，其中多孔聚苯乙烯表现出多孔尺寸分布。形成发泡制品的方法包括提供形成的苯乙烯类聚合物并使形成的苯乙烯类聚合物与第一发泡剂和包含氧化铝的吸附剂接触以形成挤出聚苯乙烯。该方法还包括将挤出苯乙烯聚合物形成膨胀的苯乙烯聚合物，并将膨胀的苯乙烯聚合物形成发泡制品。

4. 发明授权

US09850357B2 Use of polar additives for enhancing blowing agent solubility in polystyrene 有权
公开(公告)号：US09850357B2
公开(公告)日：2017-12-26
申请号：US13347704
申请日：2012-01-11
申请人： Wei Wang , Jose M. Sosa , David W. Knoeppel
发明人： Wei Wang , Jose M. Sosa , David W. Knoeppel
IPC分类号： C08J9/00 , C08J9/12 , C08J9/14 , C08L25/06 , C08L35/06
CPC分类号： C08J9/0014 , C08J9/12 , C08J9/142 , C08J2203/06 , C08J2203/12 , C08J2325/04 , C08J2325/08 , C08L25/06 , C08L35/06
摘要： Foamable polystyrene compositions with enhanced blowing agent solubility and methods of making such polystyrene compositions by incorporating a polar additive in styrenic polymer or copolymers.

5. 发明授权

US08957152B2 Polarity manipulation in polystyrene for enhanced bio-polymer miscibility 有权
标题翻译：在聚苯乙烯中的极性操作提高了生物聚合物的混溶性
公开(公告)号：US08957152B2
公开(公告)日：2015-02-17
申请号：US13171828
申请日：2011-06-29
申请人： Wei Wang , David W. Knoeppel , Jose Sosa
发明人： Wei Wang , David W. Knoeppel , Jose Sosa
IPC分类号： C08L25/14 , C08L35/06 , C08L67/04 , C08L29/04 , C08L35/00 , C08L67/00 , C08K5/053 , C08K5/00
CPC分类号： C08L25/14 , C08K5/0016 , C08L1/00 , C08L3/00 , C08L5/00 , C08L25/08 , C08L29/04 , C08L35/06 , C08L67/04 , C08L2201/06
摘要： A styrenic composition including a polar modified styrenic co-polymer resulting from the polymerization of a combined mixture of at least one styrenic monomer and at least one comonomer and a biodegradable component is disclosed. The at least one comonomer includes a polar functional group and the polar modified styrenic co-polymer and the biodegradable component are combined to obtain a styrenic composition having a biodegradable component. Also disclosed is a method of enhancing bio-polymer miscibility in a styrenic based polymer. The polarity of a blend is manipulated by combining a styrenic monomer and a polar co-monomer to form a combined mixture and subjecting the combined mixture to polymerization to obtain a styrenic polymer blend to which a bio-polymer is added.
摘要翻译：公开了一种苯乙烯组合物，其包含由至少一种苯乙烯类单体和至少一种共聚单体和可生物降解的组分的组合混合物的聚合产生的极性改性苯乙烯共聚物。所述至少一种共聚单体包括极性官能团和极性改性的苯乙烯类共聚物，并且所述可生物降解的组分被组合以获得具有可生物降解的组分的苯乙烯组合物。还公开了一种提高苯乙烯类聚合物中生物聚合物混溶性的方法。通过组合苯乙烯类单体和极性共聚单体来混合共混物的极性，以形成组合的混合物，并将合并的混合物进行聚合，得到加入生物聚合物的苯乙烯聚合物共混物。

6. 发明申请

US20130005912A1 High Melt Strength Polystyrene and Methods of Making Same 有权
标题翻译：高熔体聚苯乙烯及其制备方法
公开(公告)号：US20130005912A1
公开(公告)日：2013-01-03
申请号：US13171823
申请日：2011-06-29
申请人： Wei Wang , David W. Knoeppel
发明人： Wei Wang , David W. Knoeppel
IPC分类号： C08F267/04 , C08F222/20 , C08F212/08 , C08F220/28
CPC分类号： C08F267/04 , C08F212/08 , C08F220/20 , C08F220/28 , C08F290/061 , C08L25/14 , C08F2220/1825 , C08F2222/1073 , C08F222/06 , C08L35/06
摘要： A method of making a styrenic composition having a high melt strength including combining a styrenic monomer and a second monomer to form a combined mixture and subjecting the combined mixture to polymerization to obtain a styrenic co-polymer, wherein the second monomer comprises a hydroxyl functional group and wherein the styrenic composition has a greater melt strength than that of general purpose polystyrene.
摘要翻译：一种制备具有高熔体强度的苯乙烯组合物的方法，包括组合苯乙烯类单体和第二单体以形成组合的混合物，并使合并的混合物聚合以获得苯乙烯共聚物，其中第二单体包含羟基官能团并且其中所述苯乙烯组合物具有比通用聚苯乙烯更大的熔体强度。

7. 发明授权

US08063159B2 Process for controlling morphology of Ziegler-Natta catalysts 失效
标题翻译：控制齐格勒 - 纳塔催化剂形态的方法
公开(公告)号：US08063159B2
公开(公告)日：2011-11-22
申请号：US11778262
申请日：2007-07-16
申请人： Kayo Vizzini , Henry Enriquez , Steven D. Gray , Tim J. Coffy , David W. Knoeppel
发明人： Kayo Vizzini , Henry Enriquez , Steven D. Gray , Tim J. Coffy , David W. Knoeppel
IPC分类号： C08F4/00
CPC分类号： C08F10/00 , C08F210/16 , Y10T428/1345 , Y10T428/139 , C08F4/6546 , C08F4/6541
摘要： Disclosed is a process for making a Ziegler-Natta catalyst having controlled particle size and distribution. It comprises altering the precipitation of a catalyst component from a catalyst synthesis solution including a soluble magnesium containing catalyst precursor by controlling the concentration of either the soluble magnesium containing catalyst precursor, wherein the average particle size of the catalyst component is increased, and the particle size distribution increased, with a decreased concentration of the soluble magnesium containing catalyst precursor; or of the precipitating agent, wherein the average particle size of the catalyst component is increased, and the particle size distribution increased with an increased concentration of the precipitating agent. Use of the invention enables improved catalyst consistency regardless of production scale and customizing of catalyst morphology to desired polymer morphology. The novel catalyst components may be used to prepare polymers, and end-use articles therefrom, having desirable properties.
摘要翻译：公开了一种制备具有受控粒度和分布的齐格勒 - 纳塔催化剂的方法。其包括通过控制可溶性含镁催化剂前体的浓度来改变催化剂组分从包括可溶性镁的催化剂前体的催化剂合成溶液中的沉淀，其中催化剂组分的平均粒径增加，并且颗粒尺寸分布增加，可溶性含镁催化剂前体的浓度降低; 或沉淀剂，其中催化剂组分的平均粒度增加，并且随着沉淀剂浓度的增加，粒度分布增加。使用本发明能够改善催化剂的一致性，而不管生产规模如何，催化剂形态定制成所需的聚合物形态。新颖的催化剂组分可用于制备聚合物及其最终用途制品，具有期望的性能。

8. 发明申请

US20110245428A1 Polystyrene Blends 有权
标题翻译：聚苯乙烯共混物
公开(公告)号：US20110245428A1
公开(公告)日：2011-10-06
申请号：US13074763
申请日：2011-03-29
申请人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corleto
发明人： Camille Grossetete , David W. Knoeppel , Jose M. Sosa , Shane Steagall , Carlos Corleto
IPC分类号： C08L25/06
CPC分类号： C08L25/06 , C08L2205/02 , C08L2207/20
摘要： A method of preparing a polystyrene blend that includes combining a first polystyrene composition having a first melt flow index with a second polystyrene composition having a second melt flow index and forming a polystyrene blend, the second melt flow index being at least 2 dg/min higher that the first melt flow index. The polystyrene blend has an observed tensile strength value greater than 3% above the expected tensile strength value. The second polystyrene composition can include a recycled polystyrene material, which can include expanded polystyrene. An alternate method of preparing the polystyrene blend includes combining a polystyrene composition with a styrene monomer to form a reaction mixture, polymerizing the reaction mixture and obtaining a polystyrene blend, where the polystyrene containing composition has a melt flow index at least 2 dg/min higher than the melt flow index of the styrene monomer after it has been polymerized.
摘要翻译：一种制备聚苯乙烯共混物的方法，其包括将具有第一熔体流动指数的第一聚苯乙烯组合物与具有第二熔体流动指数的第二聚苯乙烯组合物组合并形成聚苯乙烯共混物，所述第二熔体流动指数至少为2dg / min 第一个熔体流动指数。聚苯乙烯共混物的观测拉伸强度值大于预期拉伸强度值的3％以上。第二聚苯乙烯组合物可包括再循环的聚苯乙烯材料，其可包括发泡聚苯乙烯。制备聚苯乙烯共混物的替代方法包括将聚苯乙烯组合物与苯乙烯单体组合以形成反应混合物，使反应混合物聚合并获得聚苯乙烯共混物，其中含聚苯乙烯的组合物的熔体流动指数至少为2dg / min 比苯乙烯单体聚合后的熔体流动指数高。

9. 发明授权

US06930071B2 Ziegler-natta catalyst for polyolefins 有权
公开(公告)号：US06930071B2
公开(公告)日：2005-08-16
申请号：US10667578
申请日：2003-09-22
申请人： David W. Knoeppel , Tim J. Coffy , Henry Enriquez , Steven D. Gray
发明人： David W. Knoeppel , Tim J. Coffy , Henry Enriquez , Steven D. Gray
IPC分类号： C08F4/654 , B01J31/00 , B01J31/02 , C08F4/44 , C08F4/658 , C08F10/00 , C08F10/02 , C08F110/02 , C08F4/60 , C08F4/602
CPC分类号： B01J31/0212 , B01J2231/122 , B01J2531/31 , B01J2531/46 , C08F10/00 , C08F110/02 , C08F4/6557 , C08F2500/04 , C08F2500/12 , C08F4/6546 , C08F4/651 , C08F4/6567 , C08F2500/02 , C08F2500/23 , C08F2500/07 , C08F2500/18
摘要： A Ziegler-Natta type catalyst component can be produced by a process comprising contacting a magnesium dialkoxide compound with a halogenating agent to form a reaction product A, and contacting reaction product A with a first, second and third halogenating/titanating agents. Catalyst components, catalysts, catalyst systems, polyolefin, products made therewith, and methods of forming each are disclosed. The reaction products can be washed with a hydrocarbon solvent to reduce titanium species [Ti] content to less than about 100 mmol/L.

10. 发明授权

US08912242B2 Polar polystyrene copolymers for enhanced foaming 有权
标题翻译：极性聚苯乙烯共聚物，用于增强发泡
公开(公告)号：US08912242B2
公开(公告)日：2014-12-16
申请号：US13347706
申请日：2012-01-11
申请人： Wei Wang , David W. Knoeppel , Melissa Greenberg
发明人： Wei Wang , David W. Knoeppel , Melissa Greenberg
IPC分类号： C08J9/06 , C08J9/10 , C08F212/08 , C08J9/12 , C08J9/00 , C08J9/14
CPC分类号： C08J9/122 , C08F212/08 , C08J9/0023 , C08J9/12 , C08J9/142 , C08J2203/06 , C08J2203/10 , C08J2203/12 , C08J2325/08 , C08J2351/00 , C08F2220/281 , C08F222/08 , C08F2220/1825 , C08F2220/325
摘要： A method of making a foamable polystyrene composition includes combining a styrenic monomer and a co-monomer containing a polar functional group to obtain a mixture, subjecting the mixture to polymerization to obtain a styrenic co-polymer, and combining the styrenic co-polymer with a blowing agent in a foaming process to obtain foamed articles.
摘要翻译：制备可发泡聚苯乙烯组合物的方法包括将苯乙烯单体和含有极性官能团的共聚单体混合以获得混合物，使混合物聚合以获得苯乙烯共聚物，并将苯乙烯共聚物与发泡剂中发泡剂得到泡沫制品。

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