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1. 发明授权

US5998327A Zinc/metal hexacyanocobaltate complex compounds, a process for their preparation, and their use in a process for the production of polyether polyols 失效
标题翻译：锌/金属六氰合钴酸盐络合物，其制备方法及其在制备聚醚多元醇的方法中的用途
公开(公告)号：US5998327A
公开(公告)日：1999-12-07
申请号：US114359
申请日：1998-07-13
申请人： Jorg Hofmann , Pramod Gupta , Harald Pielartzik , Pieter Ooms , Walter Schafer
发明人： Jorg Hofmann , Pramod Gupta , Harald Pielartzik , Pieter Ooms , Walter Schafer
IPC分类号： B01J31/22 , B01J27/16 , B01J27/26 , B01J37/04 , C07C41/02 , C07F19/00 , C08G65/10 , C08G65/26 , C08G65/28
CPC分类号： B01J27/26 , C08G65/2663
摘要： The invention relates to novel zinc/metal hexacyanocobaltate complex compounds corresponding to the formula:Zn.sub.3-v M.sub.v [Co(CN).sub.6 ].sub.2.w(H.sub.2 O).x(L).y[Zn(X).sub.n ].z[M(Y).sub.m)].These complex compounds are suitable catalysts. This invention also relates to a process for the production of the compounds, and to the use of the compounds in a process for the production of polyether polyols.These novel zinc/metal hexacyanocobaltate complex compounds when used as catalysts in a process for the production of polyether polyols substantially reduce the induction period of the polyaddition reaction of alkylene oxides to starter compounds containing hydrogen atoms. Furthermore, the resultant polyether polyols have a significantly narrower molecular weight distribution.
摘要翻译：本发明涉及对应于式Zn3-vMv [Co（CN）6] 2.w（H2O）.x（L）.y [Zn（X）n] .z [M]的新型锌/金属六氰合钴酸盐络合物（Y）m）]。这些络合物是合适的催化剂。本发明还涉及一种生产该化合物的方法，以及该化合物在制备聚醚多元醇的方法中的用途。当在制备聚醚多元醇的方法中用作催化剂时，这些新型的锌/金属六氰合钴酸盐络合物基本上降低了环氧烷烃与起始化合物含氢原子的加成反应的诱导期。此外，所得聚醚多元醇具有明显较窄的分子量分布。

2. 发明授权

US6093793A Process for the production of polyether polyols 失效
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US6093793A
公开(公告)日：2000-07-25
申请号：US8986
申请日：1998-01-20
申请人： Jorg Hofmann , Pramod Gupta , Harald Pielartzik
发明人： Jorg Hofmann , Pramod Gupta , Harald Pielartzik
IPC分类号： C08G65/26 , C08G65/28 , C08G65/30 , C08G65/34
CPC分类号： C08G65/266
摘要： Polyether polyols are produced by acid-catalyzed polyaddition of alkylene oxides to starter compounds having active hydrogen atoms. Perfluoroalkylsulfonic acid salts of metals from Group IIIA of the Periodic Table of Elements (corresponding to the IUPAC Convention of 1970) are used as the catalyst. The polyaddition reaction is carried out at a temperature of from 40 to 200.degree. C. at normal pressure or pressures from 0 to 20 mbar (absolute). An inert organic solvent may optionally be included in the reaction mixture. Substantially all of the catalyst is removed from the polyether polyol-containing reaction mixture by lowering the temperature and/or by addition of a precipitating agent and/or by extraction with water. If desired, the recovered catalyst may be used in subsequent polyaddition reactions.
摘要翻译：聚醚多元醇通过酸式催化加成环氧烷生成具有活性氢原子的起始化合物来制备。使用元素周期表IIIA族金属的全氟烷基磺酸盐（对应于1970年的IUPAC公约）作为催化剂。加成反应在常压或0至20毫巴（绝对）的压力下在40至200℃的温度下进行。惰性有机溶剂可以任选地包括在反应混合物中。通过降低温度和/或通过加入沉淀剂和/或通过用水萃取，将基本上所有的催化剂从含聚醚多元醇的反应混合物中除去。如果需要，回收的催化剂可用于随后的加聚反应。

3. 发明授权

US06458918B1 Method for producing partially crystalline polyether polyols 失效
标题翻译：部分结晶聚醚多元醇的制备方法
公开(公告)号：US06458918B1
公开(公告)日：2002-10-01
申请号：US09530304
申请日：2000-04-27
申请人： Walter Schäfer , Jörg Hofmann , Pramod Gupta , Hanns-Peter Müller , Harald Pielartzik
发明人： Walter Schäfer , Jörg Hofmann , Pramod Gupta , Hanns-Peter Müller , Harald Pielartzik
IPC分类号： C08G6512
CPC分类号： C08G65/269 , B01J31/068 , B01J31/165 , B01J31/2226 , B01J2231/48 , B01J2531/0216 , B01J2531/0219 , B01J2531/26 , B01J2531/31 , B01J2531/46 , B01J2531/62 , B01J2531/64 , B01J2531/70 , B01J2531/842 , B01J2531/845 , C08G65/12 , C08G65/2642 , C08G2250/00
摘要： The present invention relates to a process for the preparation of novel, partially crystalline polyether polyols with a functionality of ≧2, an average molecular weight Mn of 500 to 100,000 and a molar proportion of isotactic triads determining the crystallinity of >28%. The new polyether polyols are prepared by polymerizing alkylene oxides in the presence of a bimetallic :-oxoalkoxide modified with hydroxyl compounds.
摘要翻译：本发明涉及一种制备具有官能度> = 2，平均分子量Mn为500至100,000的新型部分结晶的聚醚多元醇和确定结晶度> 28％的全同立构三单元组的摩尔比例的方法。新的聚醚多元醇通过在用羟基化合物改性的双金属氧化物存在下聚合烯化氧来制备。

4. 发明授权

US06878661B1 Bimetallic-cyanide catalysts used for preparing polyether polyols 失效
标题翻译：用于制备聚醚多元醇的双金属氰化物催化剂
公开(公告)号：US06878661B1
公开(公告)日：2005-04-12
申请号：US09744357
申请日：1999-07-20
申请人： Pieter Ooms , Jörg Hofmann , Pramod Gupta , Walter Schäfer
发明人： Pieter Ooms , Jörg Hofmann , Pramod Gupta , Walter Schäfer
IPC分类号： C08G65/10 , C08G65/26 , B01J31/00
CPC分类号： B01J27/26 , C08G65/10 , C08G65/2663
摘要： The invention relates to novel double metal cyanide (DMC) catalysts for the preparation of polyether polyols by polyaddition of alkylene oxides to starter compounds containing active hydrogen atoms, wherein the catalyst contains a) double metal cyanide compounds, b) organic complex ligands other than c), and c) complex ligands formed by introduction of a glycidyl ether into the catalyst. The catalysts according to the invention have greatly increased activity in the preparation of polyether polyols.
摘要翻译：本发明涉及用于制备聚醚多元醇的新型双金属氰化物（DMC）催化剂，其通过将环氧烷加成到含有活性氢原子的起始化合物中，其中催化剂含有a）双金属氰化物化合物，b）除c以外的有机络合物配体），和c）通过将缩水甘油醚引入催化剂而形成的复合配位体。根据本发明的催化剂在制备聚醚多元醇中的活性大大增加。

5. 发明授权

US06858655B1 High-resilient polyurethane foams produced from polyether polyols 有权
标题翻译：由聚醚多元醇生产的高弹性聚氨酯泡沫
公开(公告)号：US06858655B1
公开(公告)日：2005-02-22
申请号：US10018332
申请日：2000-06-06
申请人： Jörg Hofmann , Pramod Gupta , Manfred Dietrich , Hansjürgen Rabe , Jürgen Grönen , Pieter Ooms
发明人： Jörg Hofmann , Pramod Gupta , Manfred Dietrich , Hansjürgen Rabe , Jürgen Grönen , Pieter Ooms
IPC分类号： C08G18/48 , C08G65/26 , C08G101/00 , C08G18/28
CPC分类号： C08G65/2663 , C08G18/4845 , C08G18/485 , C08G18/4866 , C08G2101/0008 , C08G2101/0083
摘要： Flexible polyurethane foams are produced from a polyisocyanate and a polyether polyol which has been alkoxylated in the presence of a double metal cyanide catalyst and that has at least one ethylene oxide-propylene oxide mixed block.
摘要翻译：柔性聚氨酯泡沫由多异氰酸酯和聚醚多元醇生产，所述多异氰酸酯和聚醚多元醇在双金属氰化物催化剂存在下被烷氧基化，并且具有至少一个环氧乙烷 - 环氧丙烷混合嵌段。

6. 发明授权

US06323375B1 Crystalline double metal cyanide catalysts for producing polyether polyols 有权
标题翻译：用于生产聚醚多元醇的结晶双金属氰化物催化剂
公开(公告)号：US06323375B1
公开(公告)日：2001-11-27
申请号：US09509979
申请日：2000-04-05
申请人： Jörg Hofmann , Pramod Gupta , Robert-Joseph Kumpf , Pieter Ooms , Walter Schäfer , Michael Schneider
发明人： Jörg Hofmann , Pramod Gupta , Robert-Joseph Kumpf , Pieter Ooms , Walter Schäfer , Michael Schneider
IPC分类号： C07C4311
CPC分类号： C08G65/2663 , B01J27/26
摘要： The present invention relates to highly active, substantially crystalline double metal cyanide (DMC) catalysts, a process for the preparation of these double metal cyanide catalysts, a process for producing polyether polyols by the polyaddition of alcohol ethers onto starter compounds containing active hydrogen atoms from these DMC catalysts, and to the polyether polyols produced by this process. The DMC catalysts of the invention comprise a) double metal cyanide compounds, b) organic complexing ligands, and c) functionalized polymers. These catalysts exhibit increased activity in the process for the production of polyether polyols.
摘要翻译：本发明涉及高活性，基本上结晶的双金属氰化物（DMC）催化剂，制备这些双金属氰化物催化剂的方法，通过将醇醚加成到含有活性氢原子的起始化合物上制备聚醚多元醇的方法这些DMC催化剂，以及通过该方法制备的聚醚多元醇。本发明的DMC催化剂包括a）双金属氰化物化合物，b）有机络合配体，和c）官能化聚合物。这些催化剂在制备聚醚多元醇的方法中表现出增加的活性。

7. 发明授权

US06528616B1 Double metal cyanide catalysts for the production of polyther polyols 失效
标题翻译：用于生产聚醚多元醇的双金属氰化物催化剂
公开(公告)号：US06528616B1
公开(公告)日：2003-03-04
申请号：US10030771
申请日：2001-10-29
申请人： Pieter Ooms , Jörg Hofmann , Pramod Gupta
发明人： Pieter Ooms , Jörg Hofmann , Pramod Gupta
IPC分类号： B01J2726
CPC分类号： C08G65/2663 , B01J27/26 , B01J31/0202 , B01J31/0209 , B01J31/04 , B01J31/06 , B01J31/2208 , B01J31/2213 , B01J2531/26 , B01J2531/845 , B01J2531/96
摘要： The invention relates to new double metal cyanide (DMC) catalysts for the production of polyether polyols by polyaddition of alkylene oxides to starter compounds containing active hydrogen atoms, wherein the catalyst contains a) double metal cyanide compounds, b) organic complex ligands different from c), and c) &agr;,&bgr;-unsaturated carboxylic acid esters. The catalysts according to the invention have a significantly improved activity in the production of polyether polyols.
摘要翻译：本发明涉及用于生产聚醚多元醇的新型双金属氰化物（DMC）催化剂，其通过将环氧烷加成到含有活性氢原子的起始化合物中，其中催化剂含有a）双金属氰化物化合物，b）与c不同的有机络合物配体）和c）α，β-不饱和羧酸酯。根据本发明的催化剂在聚醚多元醇的生产中具有显着改善的活性。

8. 发明授权

US06376420B1 Double-metal cyanide catalysts for producing polyether polyols 失效
标题翻译：用于生产聚醚多元醇的双金属氰化物催化剂
公开(公告)号：US06376420B1
公开(公告)日：2002-04-23
申请号：US09787053
申请日：2001-03-13
申请人： Pieter Ooms , Jörg Hofmann , Pramod Gupta
发明人： Pieter Ooms , Jörg Hofmann , Pramod Gupta
IPC分类号： B01J2726
CPC分类号： C08G65/10 , C08G65/2663
摘要： The invention relates to novel double metal cyanide (DMC) catalysts for the preparation of polyether polyols by polyaddition of alkylene oxides to starter compounds containing active hydrogen atoms, wherein the catalyst contains a) double metal cyanide compounds, b) organic complex ligands other than c), and c) polyalkylene glycol sorbitan esters. The catalysts according to the invention have greatly increased activity in the preparation of polyether polyols.
摘要翻译：本发明涉及用于制备聚醚多元醇的新型双金属氰化物（DMC）催化剂，其通过将环氧烷加成到含有活性氢原子的起始化合物中，其中催化剂含有a）双金属氰化物化合物，b）除c以外的有机络合物配体），和c）聚亚烷基二醇脱水山梨糖醇酯。根据本发明的催化剂在制备聚醚多元醇中的活性大大增加。

9. 发明授权

US06291388B1 Double metal cyanide catalysts for producing polyether polyols 有权
标题翻译：用于生产聚醚多元醇的双金属氰化物催化剂
公开(公告)号：US06291388B1
公开(公告)日：2001-09-18
申请号：US09623648
申请日：2000-09-06
申请人： Jörg Hofmann , Pieter Ooms , Pramod Gupta , Walter Schäfer
发明人： Jörg Hofmann , Pieter Ooms , Pramod Gupta , Walter Schäfer
IPC分类号： B01J3106
CPC分类号： B01J27/26 , C08G65/10 , C08G65/2663
摘要： The invention relates to new, improved double metal cyanide (DMC) catalysts for preparing polyetherpolyols by polyaddition of alkylene oxides to starter compounds containing active hydrogen atoms, wherein the catalyst contains a double metal cyanide compound, an organic coordination ligand and 5 to 80 wt. %, with respect to the amount of catalyst, of an ethylene oxide polyether with a number average molecular weight greater than 500. The new, improved catalysts have a greatly increased reactivity for polyetherpolyol preparation.
摘要翻译：本发明涉及新的改进的双金属氰化物（DMC）催化剂，其用于通过将环氧烷烃加成到含有活性氢原子的起始化合物中制备聚醚多元醇，其中催化剂含有双金属氰化物化合物，有机配位配体和5-80wt。相对于催化剂的数量，数均分子量大于500的环氧乙烷聚醚的数量。新的改进的催化剂对于聚醚多元醇制备具有大大增加的反应性。

10. 发明授权

US06624286B2 Double-metal cyanide catalysts containing polyester for preparing polyether polyols 失效
标题翻译：含有制备聚醚多元醇的聚酯的双金属氰化物催化剂
公开(公告)号：US06624286B2
公开(公告)日：2003-09-23
申请号：US10006065
申请日：2001-12-05
申请人： Jörg Hofmann , Pramod Gupta , Robert-Joseph Kumpf , Pieter Ooms , Walter Schäfer
发明人： Jörg Hofmann , Pramod Gupta , Robert-Joseph Kumpf , Pieter Ooms , Walter Schäfer
IPC分类号： C08G6504
CPC分类号： C08G65/2663 , B01J27/26
摘要： The invention relates to new improved double-metal cyanide (DMC) catalysts for the preparation of polyether-polyols by polyaddition of alkylene oxides on to starter compounds containing active hydrogen atoms, the catalyst comprising a double-metal cyanide compound, an organic complexing ligand and 5-80 wt. %, based on the amount of catalyst, of a polyester. For the preparation of polyether-polyols, the new improved catalysts have significantly shortened induction times and at the same time a greatly increased activity.
摘要翻译：本发明涉及新的改进的双金属氰化物（DMC）催化剂，用于通过将环氧烷烃加成到含有活性氢原子的起始化合物上制备聚醚多元醇，催化剂包含双金属氰化物化合物，有机络合配体和 5-80重量％基于催化剂量的聚酯。对于聚醚多元醇的制备，新的改进的催化剂具有显着缩短的诱导时间，同时活性大大增加。

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