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1. 发明授权

US5069994A Use of colorless, intensely fluorinated ammonium and iminium compounds as charge control agents for electrophotographic recording processes 失效
标题翻译：作为电子记录记录过程的充电控制剂，使用无色，强力氟化氨和铱化合物
公开(公告)号：US5069994A
公开(公告)日：1991-12-03
申请号：US430732
申请日：1989-11-02
申请人： Jorg Gitzel , Hans-Tobias Macholdt , Alexander Sieber , Frank Wehowsky , Gunther Prossel
发明人： Jorg Gitzel , Hans-Tobias Macholdt , Alexander Sieber , Frank Wehowsky , Gunther Prossel
IPC分类号： C09D5/03 , C09D5/46 , G03G9/09 , G03G9/097 , G03G9/113
CPC分类号： G03G9/09741 , C09D5/034 , G03G9/09766
摘要： The use of intensely fluorinated ammonium compounds of the general formula (I) ##STR1## in which R.sub.1 to R.sub.4 denote hydrogen atoms or organic radicals, at least one of the radicals R.sub.1 to R.sub.4 denoting a straight-chain or branched fluorine-containing alkyl radical or fluorine-containing alkenyl radical which contains 1 to 69 carbon atoms and 3 to 66 fluorine atoms and which may be substituted, and at most three of the radicals R.sub.1 to R.sub.4 are, independently of one another, hydrogen atoms, straight-chain or branched alkyl radicals or alkenyl radicals containing 1 to 30 carbon atoms, aryl radicals or aralkyl radicals, and X.sup.- denotes an organic or inorganic anion, and of intensely fluorinated iminium compounds of the general formula (II) ##STR2## in which R.sub.9 to R.sub.12 denote hydrogen atoms or organic radicals, at least one of the radicals R.sub.9 to R.sub.12 denoting a straight-chain or branched fluorine-containing alkyl radical or fluorine-containing alkenyl radical which contains 1 to 69 carbon atoms and 3 to 66 fluorine atoms and which may be substituted, and at most three of the radicals R.sub.9 to R.sub.12 denote, independently of one another, hydrogen, straight-chain or branched alkyl radicals or alkenyl radicals containing 1 to 30 carbon atoms, aryl or aralkyl radicals and Y.sup.- is an organic or inorganic anion, as colorless charge control agents having positive or negative control effect in toners and developers for electrophotographic recording processes.
摘要翻译：使用通式（I）的高度氟化的铵化合物，其中R 1至R 4表示氢原子或有机基团，基团R 1至R 4中的至少一个表示直链或支链的氟 - 含有1至69个碳原子和3至66个氟原子且可以被取代的烷基或含氟烯基，并且至少三个基团R 1至R 4彼此独立地为氢原子，含有1至30个碳原子的链或支链烷基或烯基，芳基或芳烷基，X表示有机或无机阴离子，以及通式（II）的强氟化亚胺化合物。（II）其中R9至R12表示氢原子或有机基团，表示含有1至69个碳原子的直链或支链含氟烷基或含氟烯基的基团R 9至R 12中的至少一个和3至66个氟原子并且其可以被取代，并且至少三个基团R 9至R 12彼此独立地表示氢，直链或支链烷基或含有1至30个碳原子的烯基，芳基或芳烷基和Y-是有机或无机阴离子，作为在调色剂和电子照相记录方法的显影剂中具有正或负控制效果的无色电荷控制剂。

2. 发明授权

US5053537A Ammonium and iminium compounds 失效
标题翻译：氨和化合物
公开(公告)号：US5053537A
公开(公告)日：1991-10-01
申请号：US430740
申请日：1989-11-02
申请人： Jorg Gitzel , Hans-Tobias Macholdt , Frank Wehowsky , Gunther Prossel
发明人： Jorg Gitzel , Hans-Tobias Macholdt , Frank Wehowsky , Gunther Prossel
IPC分类号： C07C211/63 , C07D213/20 , C07D215/10 , C07F5/02
CPC分类号： C07D213/20 , C07C211/63 , C07D215/10 , C07F5/027
摘要： Ammonium compounds of the formula (I) ##STR1## in which at least one of the radicals R.sub.1 to R.sub.4 denotes a fluorine-containing alkyl radical having 4 to 30 carbon atoms and not more than three of the radicals R.sub.1 to R.sub.4 independently of one another denote hydrogen atoms or alkyl or hydroxyalkyl radicals having 1 to 30 carbon atoms, and R.sub.5 to R.sub.8 denote aryl, alkylaryl or halogenoaryl radicals or fluorine atoms, and iminium compounds of the formula (II) ##STR2## in which Q, together with the constituent ##STR3## forms a ring system having 4 to 17 carbon atoms, which can be interrupted by 1 to 4 hetero atoms and contain 2 to 9 double bonds, and which can be substituted by fluorine, chlorine, bromine or iodine atoms or alkyl (C.sub.1 -C.sub.6), alkoxy (C.sub.1 -C.sub.6), nitro or amino groups, R.sub.9 denotes a fluorine-containing alkyl (C.sub.1 -C.sub.30) radical, R.sub.10 denotes a hydrogen, fluorine, chlorine, bromine or iodine atom or an alkyl(C.sub.1 -C.sub.6), alkoxy (C.sub.1 -C.sub.6), nitro or amino group and the radicals R.sub.11 to R.sub.14 denote aryl radicals, alkylaryl radicals, halogenoaryl radicals or fluorine atoms, and mixtures of these compounds and processes for their preparation.
摘要翻译：式（I）的铵化合物其中至少一个基团R 1至R 4表示独立地具有4至30个碳原子且不超过3个基团R 1至R 4的含氟烷基彼此表示氢原子或具有1至30个碳原子的烷基或羟烷基，R5至R8表示芳基，烷基芳基或卤代芳基或氟原子，以及式（II）的亚铵化合物其中 Q与组分“IMAGE”一起形成具有4至17个碳原子的环系，其可被1至4个杂原子间隔并含有2至9个双键，并且可被氟，氯，溴或碘原子或烷基（C1-C6），烷氧基（C1-C6），硝基或氨基，R9表示含氟烷基（C1-C30）基，R10表示氢，氟，氯，溴或碘原子或烷基（C1-C6），烷氧基（C1-C6），硝基或氨基，基团R11至R14表示芳基自由基，烷基芳基，卤代芳基或氟原子，以及这些化合物的混合物及其制备方法。

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