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1. 发明授权

US06376640B1 Melt polycarbonate catalyst systems 失效
标题翻译：熔融聚碳酸酯催化剂体系
公开(公告)号：US06376640B1
公开(公告)日：2002-04-23
申请号：US09760100
申请日：2001-01-12
申请人： John Patrick Lemmon , Patrick Joseph McCloskey , Oltea Puica Siclovan
发明人： John Patrick Lemmon , Patrick Joseph McCloskey , Oltea Puica Siclovan
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： This invention provides a method for preparing polycarbonates, which utilizes polycondensation catalysts of the formula Cs+An−, wherein An− represents anions such as CH3SO3−, NH2SO3−, C2H2O4−, BF4−, B(C6H5CH3)4−, and CH3C6H4SO3−. We have found that this new class of catalysts provides excellent polymerization rates for the preparation of Bisphenol A polycarbonate from the melt polymerization of diphenyl carbonate and Bisphenol A. Moreover, the catalysts of the invention were found to be very selective in substantially reducing the level of branching side reaction, i.e., formation of Fries product, normally associated with the melt polycarbonate process.
摘要翻译：本发明提供一种制备聚碳酸酯的方法，该方法采用式为Cs + An-的缩聚催化剂，其中An-表示阴离子如CH 3 SO 3 - ，NH 2 SO 3 - ，C 2 H 2 O 4 - ，BF 4 - ，B（C 6 H 5 CH 3）4 - 和CH 3 C 6 H 4 SO 3 - 。我们已经发现，这种新型催化剂由于碳酸二苯酯和双酚A的熔融聚合而提供了用于制备双酚A聚碳酸酯的优异的聚合速率。此外，发现本发明的催化剂在显着降低分支侧反应，即通常与熔融聚碳酸酯方法相关的Fries产物的形成。

2. 发明授权

US06323304B1 Melt polycarbonate catalyst systems 有权
标题翻译：熔融聚碳酸酯催化剂体系
公开(公告)号：US06323304B1
公开(公告)日：2001-11-27
申请号：US09760086
申请日：2001-01-12
申请人： John Patrick Lemmon , Patrick Joseph McCloskey , Oltea Puica Siclovan
发明人： John Patrick Lemmon , Patrick Joseph McCloskey , Oltea Puica Siclovan
IPC分类号： C08G6378
CPC分类号： C08G64/307
摘要： This invention provides a method for preparing polycarbonates, which utilizes polycondensation catalysts of the formula Ax+MF6−x, wherein A is an alkali metal or alkaline earth cation; M is a transition metal of group IVA or VA, or M is a p-block metal of group IIIB, IVB or VB; and x is 1, 2, or 3. We have found that this new class of catalysts provide excellent polymerization rates for the preparation of Bisphenol A polycarbonate from the melt polymerization of diphenyl carbonate and Bisphenol A. Moreover, the catalysts of the invention were found to be very selective in substantially reducing the level of branching side reaction, i.e., formation of Fries product, normally associated with the melt polycarbonate process.
摘要翻译：本发明提供一种制备聚碳酸酯的方法，其使用式Ax + MF6-x的缩聚催化剂，其中A为碱金属或碱土金属阳离子; M是IVA或VA族的过渡金属，或M是IIIB，IVB或VB族的p型金属; 我们已经发现，这种新型催化剂从碳酸二苯酯和双酚A的熔融聚合制备双酚A聚碳酸酯提供了极好的聚合速率。此外，发现了本发明的催化剂在大大降低支化反应的水平方面非常有选择性，即通常与熔融聚碳酸酯方法相关的Fries产物的形成。

3. 发明授权

US06610814B2 Compounds of antimony and germanium as catalysts for melt polycarbonate 失效
标题翻译：锑和锗的化合物作为熔融聚碳酸酯的催化剂
公开(公告)号：US06610814B2
公开(公告)日：2003-08-26
申请号：US10007347
申请日：2001-10-25
申请人： John Patrick Lemmon , Oltea Puica Siclovan
发明人： John Patrick Lemmon , Oltea Puica Siclovan
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： The present invention relates to a synthetic method in which one or more diaryl carbonates is reacted with one or more dihydroxy aromatic compounds in the presence of a transesterification catalyst under melt polymerization conditions to afford a product polycarbonate. The transesterifcation catalysts used according to the method of the present invention are alkali metal salts and alkaline earth metal salts of antimony oxides or germanium oxides in combination with tetraalkyl ammonium or tetraalkyl phosphonium compounds which serve as co-catalysts. The antimony oxide derivative “tartar emetic”, structure IV, was shown to possess excellent activity as a transesterifcation catalyst for the preparation of polycarbonate under melt polymerization conditions. The catalysts employed according to the method of the present invention provide polycarbonates having substantial molecular weight (Mn˜7000-10000 daltons) and reduced levels of Fries rearrangement product relative to conventionally prepared melt polycarbonate having a similar molecular weight.
摘要翻译：本发明涉及在熔融聚合条件下，在酯交换催化剂存在下，使一种或多种碳酸二芳基酯与一种或多种二羟基芳族化合物反应以得到产物聚碳酸酯的合成方法。根据本发明方法使用的酯交换催化剂是用作助催化剂的四烷基铵或四烷基鏻化合物的氧化锑或氧化锗的碱金属盐和碱土金属盐。显示结构IV的氧化锑衍生物“鞑靼呕吐物”在熔融聚合条件下作为用于制备聚碳酸酯的酯交换催化剂具有优异的活性。根据本发明的方法使用的催化剂相对于具有相似分子量的常规制备的熔融聚碳酸酯提供具有相当大分子量（Mn〜7000-10000道尔顿）的聚碳酸酯和降低的Fries重排产物含量。

4. 发明授权

US06569986B1 Salts of organic polyacids as polymerization catalysts 失效
标题翻译：有机多元酸作为聚合催化剂的盐
公开(公告)号：US06569986B1
公开(公告)日：2003-05-27
申请号：US10007228
申请日：2001-10-25
申请人： John Patrick Lemmon , Ronald James Wroczynski , Oltea Puica Siclovan
发明人： John Patrick Lemmon , Ronald James Wroczynski , Oltea Puica Siclovan
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： The present invention relates to a synthetic method comprising contacting at least one diaryl carbonate with one or more dihydroxy aromatic compounds in the presence of a transesterification catalyst under melt polymerization conditions to afford a product polycarbonate. The transesterifcation catalysts used according to the method of the present invention are alkali metal salts and alkaline earth metal salts of organic polyacids in combination with tetraalkyl ammonium or tetraalkyl phosphonium compounds which serve as co-catalysts. The transesterification catalysts are derived from polyacids containing both CO2H groups and SO3H groups and from polyacids containing exclusively CO2H groups or exclusively SO3H groups. The catalysts employed according to the method of the present invention provide polycarbonates having reduced levels of Fries rearrangement product relative to conventionally employed catalysts such as sodium hydroxide.
摘要翻译：本发明涉及一种合成方法，其包括在熔融聚合条件下在酯基转移催化剂存在下使至少一种碳酸二芳基酯与一种或多种二羟基芳族化合物接触，得到产物聚碳酸酯。根据本发明方法使用的酯交换催化剂是作为助催化剂的四烷基铵或四烷基鏻化合物的有机多酸的碱金属盐和碱土金属盐。酯交换催化剂衍生自含有CO 2 H基团和SO 3 H基团的多酸和仅含有CO 2 H基团或仅含有SO 3 H基团的多酸。根据本发明的方法使用的催化剂提供了相对于常规使用的催化剂如氢氧化钠具有降低的Fries重排产物含量的聚碳酸酯。

5. 发明申请

US20100196236A1 TEMPLATED CATALYST COMPOSITION AND ASSOCIATED METHOD 审中-公开
标题翻译：模拟催化剂组合物和相关方法
公开(公告)号：US20100196236A1
公开(公告)日：2010-08-05
申请号：US12362520
申请日：2009-01-30
申请人： Larry Neil Lewis , Dan Hancu , Oltea Puica Siclovan , Ming Yin
发明人： Larry Neil Lewis , Dan Hancu , Oltea Puica Siclovan , Ming Yin
IPC分类号： B01D53/56 , B01J23/50 , B01J21/04 , B01J21/08
CPC分类号： B01J23/50 , B01D53/9418 , B01D2255/104 , B01J35/002 , B01J35/023 , B01J37/0018 , B01J37/0201 , B01J37/033 , B01J37/036
摘要： A composition includes a templated metal oxide substrate having a plurality of pores and a catalyst material includes silver. The composition under H2 at 30 degrees Celsius, the composition at a wavelength that is in a range of from about 350 nm to about 500 nm has a VIS-UV absorbance intensity that is at least 20 percent less than a standard silver alumina catalyst (Ag STD). The standard alumina is Norton alumina, and which has the same amount of silver by weight.
摘要翻译：组合物包括具有多个孔的模板化金属氧化物衬底，催化剂材料包括银。在30摄氏度的H 2下的组合物，波长在约350nm至约500nm范围内的组成具有比标准银氧化铝催化剂（Ag）至少少20％的VIS-UV吸收强度 STD）。标准氧化铝为诺顿氧化铝，其重量含量相同。

6. 发明申请

US20080296596A1 NOVEL GREEN EMITTING PHOSPHORS AND BLENDS THEREOF 失效
标题翻译：新型绿色发光荧光粉及其混合物
公开(公告)号：US20080296596A1
公开(公告)日：2008-12-04
申请号：US11755495
申请日：2007-05-30
申请人： Anant Achyut Setlur , Oltea Puica Siclovan , Prasanth Kumar Nammalwar , Ramesh Rao Sathyanarayan , Digamber G. Porob , Ramachandran Gopi Chandran , William Jordan Heward , Emil Vergilov Radkov , Linda Jane Valyou Briel
发明人： Anant Achyut Setlur , Oltea Puica Siclovan , Prasanth Kumar Nammalwar , Ramesh Rao Sathyanarayan , Digamber G. Porob , Ramachandran Gopi Chandran , William Jordan Heward , Emil Vergilov Radkov , Linda Jane Valyou Briel
IPC分类号： H01L33/00 , C01F17/00 , C09K11/77
CPC分类号： C09K11/7792 , B82Y30/00 , C01F17/0012 , C01F17/0043 , C01P2002/72 , C01P2002/84 , C01P2004/64 , C09K11/0883 , C09K11/7734 , H01L33/502 , H01L2224/48247 , H01L2224/48257 , Y02B20/181
摘要： Phosphor compositions, blends thereof and light emitting devices including white light emitting LED based devices, and backlights, based on such phosphor compositions. The devices include a light source and a phosphor material as described. Also disclosed are phosphor blends including such a phosphor and devices made therefrom.
摘要翻译：基于这样的荧光体组合物的荧光体组合物，其共混物和包括基于白光发光的LED基装置的发光器件和背光源。这些装置包括如所述的光源和荧光体材料。还公开了包括这样的荧光体和由其制成的器件的荧光体掺合物。

7. 发明授权

US08530369B2 Catalyst and method of manufacture 有权
标题翻译：催化剂及其制造方法
公开(公告)号：US08530369B2
公开(公告)日：2013-09-10
申请号：US12123070
申请日：2008-05-19
申请人： Larry Neil Lewis , Oltea Puica Siclovan , Hrishikesh Keshavan , Dan Hancu , Benjamin Hale Winkler
发明人： Larry Neil Lewis , Oltea Puica Siclovan , Hrishikesh Keshavan , Dan Hancu , Benjamin Hale Winkler
IPC分类号： B01J23/00 , B01J21/00 , B01J20/00
CPC分类号： B01D53/9418 , B01D2251/208 , B01D2255/1021 , B01D2255/1023 , B01D2255/104 , B01D2255/106 , B01D2255/20738 , B01D2255/20746 , B01D2255/20753 , B01D2255/2092 , B01D2255/9205 , B01D2257/404 , B01D2258/012 , B01J21/04 , B01J23/38 , B01J23/40 , B01J23/48 , B01J23/50 , B01J23/74 , B01J31/063 , B01J31/065 , B01J35/1061 , B01J37/0018 , B01J37/0201 , B01J37/0203 , B01J37/0242 , B01J37/033 , B01J37/036
摘要： A catalyst composition is provided that includes a catalytic metal secured to a substrate, and the substrate is mesoporous and has pores that are templated. A catalyst composition includes a catalytic metal secured to a mesoporous substrate. The mesoporous substrate is a reaction product of a reactive solution, a solvent, a modifier, and a templating agent. A method includes reacting a reactive solution and a templating agent to form a gel; and calcining the gel to form a substrate having a mesoporous template that is capable to support a catalyst composition.
摘要翻译：提供了一种催化剂组合物，其包括固定到基底上的催化金属，并且该基底是中孔的并且具有模板化的孔。催化剂组合物包括固定到介孔基材上的催化金属。介孔底物是反应溶液，溶剂，改性剂和模板剂的反应产物。一种方法包括使反应性溶液和模板剂反应以形成凝胶; 并煅烧凝胶以形成具有能够支持催化剂组合物的介孔模板的基材。

8. 发明申请

US20120329644A1 CATALYST COMPOSITION AND CATALYTIC REDUCTION SYSTEM 审中-公开
标题翻译：催化剂组合物和催化还原体系
公开(公告)号：US20120329644A1
公开(公告)日：2012-12-27
申请号：US13165184
申请日：2011-06-21
申请人： Oltea Puica Siclovan , Daniel George Norton , Larry Neil Lewis , Dan Hancu , Xiaoying Bao , Robert Burch , Christopher Hardacre , Sarayute Chansai
发明人： Oltea Puica Siclovan , Daniel George Norton , Larry Neil Lewis , Dan Hancu , Xiaoying Bao , Robert Burch , Christopher Hardacre , Sarayute Chansai
IPC分类号： B01J23/04 , B01J21/04 , B01J21/08 , B01J21/06 , B01J23/78 , F01N3/10 , B01J23/30 , B01J23/06 , B01J23/58 , B01J37/08 , B01D53/48 , B01J23/66 , B01J23/08
CPC分类号： B01J23/66 , B01D53/8603 , B01D53/9418 , B01D2255/104 , B01D2255/2022 , B01D2255/2025 , B01D2255/2027 , B01D2257/302 , B01D2257/404 , B01D2258/012 , B01J23/50 , B01J35/10 , B01J35/1061 , B01J35/1066 , B01J37/0018
摘要： A catalyst composition, a method of preparation of catalyst composition, a catalytic reduction system including the catalyst composition and a system using the catalytic reduction system are provided. The catalyst composition includes a templated amorphous metal oxide substrate, a catalyst material, and a sulfur scavenger material. The catalyst material includes a catalyst metal disposed on the templated metal oxide substrate and the sulfur scavenger includes an alkali metal.
摘要翻译：提供催化剂组合物，催化剂组合物的制备方法，包括催化剂组合物的催化还原体系和使用催化还原体系的体系。催化剂组合物包括模板化的无定形金属氧化物衬底，催化剂材料和除硫剂材料。催化剂材料包括设置在模板化金属氧化物基底上的催化剂金属，硫清除剂包括碱金属。

9. 发明申请

US20100196237A1 TEMPLATED CATALYST COMPOSITION AND ASSOCIATED METHOD 审中-公开
标题翻译：模拟催化剂组合物和相关方法
公开(公告)号：US20100196237A1
公开(公告)日：2010-08-05
申请号：US12362533
申请日：2009-01-30
申请人： Ming Yin , Larry Neil Lewis , Dan Hancu , Oltea Puica Siclovan
发明人： Ming Yin , Larry Neil Lewis , Dan Hancu , Oltea Puica Siclovan
IPC分类号： B01D53/86 , B01J23/50 , B01J21/04 , B01J21/12 , B01J23/745 , B01J23/68 , B01J23/06 , B01D53/56
CPC分类号： B01J23/50 , B01D53/8628 , B01D53/9418 , B01D2255/1021 , B01D2255/1025 , B01D2255/104 , B01D2255/2092 , B01D2255/90 , B01J21/04 , B01J23/002 , B01J23/60 , B01J23/687 , B01J35/002 , B01J35/04 , B01J35/1004 , B01J37/031 , B01J2523/00 , B01J2523/18 , B01J2523/27 , B01J2523/31 , B01J2523/32 , B01J2523/33 , B01J2523/69 , B01J2523/842 , B01J2523/822 , B01J2523/48
摘要： A composition includes a templated metal oxide, at least 3 weight percent of silver, and at least one catalytic metal. A method of making and a method of using are included.
摘要翻译：组合物包括模板化金属氧化物，至少3重量％的银和至少一种催化金属。包括制作方法和使用方法。

10. 发明申请

US20100086457A1 CATALYST AND METHOD OF MANUFACTURE 审中-公开
标题翻译：催化剂及其制造方法
公开(公告)号：US20100086457A1
公开(公告)日：2010-04-08
申请号：US12247728
申请日：2008-10-08
申请人： Grigorii Lev Soloveichik , Oltea Puica Siclovan
发明人： Grigorii Lev Soloveichik , Oltea Puica Siclovan
IPC分类号： B01D53/86 , B01J23/50 , B01J23/06 , B01J27/043 , B01J27/045 , B01J31/12 , B01J31/18 , B01J27/24
CPC分类号： B01D53/8628 , B01D2255/1021 , B01D2255/1023 , B01D2255/104 , B01J21/04 , B01J23/50 , B01J23/681 , B01J23/89 , B01J31/226 , B01J31/2404 , B01J37/0201 , B01J37/036 , B01J2531/0208 , B01J2531/17 , B01J2531/824 , B01J2531/828 , Y02C20/10
摘要： Disclosed herein is a catalyst composition comprising a bimetallic complex of silver and a second metal; the bimetallic complex being disposed upon a porous substrate; where the second metal is platinum, palladium, iron, cobalt, nickel, copper, cadmium or mercury and where atoms of silver and the second metal are bound by one or more bridging ligands.
摘要翻译：本文公开了包含银和第二金属的双金属络合物的催化剂组合物; 双金属络合物设置在多孔基材上; 其中第二金属是铂，钯，铁，钴，镍，铜，镉或汞，并且其中银和第二金属的原子被一个或多个桥连配体结合。

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