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1. 发明申请

US20100291302A1 ARTICLE PROTECTED BY A THERMAL BARRIER COATING HAVING A GROUP 2 OR 3/GROUP 5 STABILIZATION-COMPOSITION-ENRICHED SURFACE 审中-公开
标题翻译：具有2组或3组/ 5组稳定表面的热障涂层保护的物品
公开(公告)号：US20100291302A1
公开(公告)日：2010-11-18
申请号：US11684981
申请日：2007-03-12
申请人： John Frederick Ackerman , Venkat Subramanian Venkataramani , Irene T. Spitsberg , Brett Allen Rohrer Boutwell , Ramgopal Darolia
发明人： John Frederick Ackerman , Venkat Subramanian Venkataramani , Irene T. Spitsberg , Brett Allen Rohrer Boutwell , Ramgopal Darolia
IPC分类号： B05D3/10
CPC分类号： C23C28/3215 , C23C28/321 , C23C28/325 , C23C28/345 , C23C28/3455
摘要： A protected article is prepared by providing the article, depositing a bond coat onto an exposed surface of the article, and producing a thermal barrier coating on an exposed surface of the bond coat. The step of producing the thermal barrier coating includes the steps of depositing a primary ceramic coating onto an exposed surface of the bond coat, and depositing a stabilization composition onto an exposed surface of the primary ceramic coating. The stabilization composition includes a first element selected from Group 2 or Group 3 of the periodic table, and a second element selected from Group 5 of the periodic table. The atomic ratio of the amount of the first element to the amount of the second element is at least 1.3, more preferably at least 1:1.
摘要翻译：通过提供制品来制备受保护制品，将粘合涂层沉积在制品的暴露表面上，并在粘合涂层的暴露表面上产生热障涂层。生产热障涂层的步骤包括以下步骤：将初级陶瓷涂层沉积在粘合涂层的暴露表面上，并将稳定化组合物沉积到初级陶瓷涂层的暴露表面上。稳定化组合物包括选自元素周期表第2族或第3族的第一元素和选自元素周期表第5族的第二元素。第一元素的量与第二元素的量的原子比为至少1.3，更优选至少1:1。

2. 发明授权

US06482469B1 Method of forming an improved aluminide bond coat for a thermal barrier coating system 失效
标题翻译：形成用于热障涂层系统的改进的铝化物粘结涂层的方法
公开(公告)号：US06482469B1
公开(公告)日：2002-11-19
申请号：US09546518
申请日：2000-04-11
申请人： Irene T. Spitsberg , Ramgopal Darolia
发明人： Irene T. Spitsberg , Ramgopal Darolia
IPC分类号： C23C1606
CPC分类号： C23C14/588 , C23C4/02 , C23C10/60 , C23C14/025 , C23C14/028 , C23C14/083 , C23C28/00
摘要： A thermal barrier coating (TBC) system and method for improving the thermal fatigue life of a thermal barrier coating. The invention entails modifying the surface morphology of an aluminide bond coat that adheres the thermal barrier coating to a substrate of a superalloy component. The aluminide bond coat has columnar grains, such that grain boundaries are exposed at the surface of the bond coat and define ridges. The surface of the bond coat is then treated so that a sufficient amount of material is removed from the grain boundary ridges and other surface peaks to flatten the bond coat surface, i.e., the ridges and peaks are replaced with flattened surfaces that are nearly parallel to the diffusion zone of the bond coat. By removing these surface irregularities, it is believed that a more stable bond coat surface is created where the critical alumina-bond coat interface will exist following a thermal treatment, such as TBC deposition.
摘要翻译：一种用于改善热障涂层的热疲劳寿命的隔热涂层（TBC）系统和方法。本发明需要改变将热障涂层粘附到超级合金部件的基底上的铝化物粘结涂层的表面形态。铝化物接合涂层具有柱状晶粒，使得晶界在接合涂层的表面暴露并限定脊。然后处理粘合涂层的表面，使得从晶界脊和其他表面峰除去足够量的材料以使粘合涂层表面平坦化，即，脊和峰被替换为几乎平行于粘结涂层的扩散区。通过去除这些表面不规则性，据信在热处理如TBC沉积之后，将产生更稳定的粘合涂层表面，其中临界氧化铝粘合涂层界面将存在。

3. 发明授权

US06455167B1 Coating system utilizing an oxide diffusion barrier for improved performance and repair capability 有权
标题翻译：涂层系统利用氧化物扩散阻挡层提高性能和修复能力
公开(公告)号：US06455167B1
公开(公告)日：2002-09-24
申请号：US09345002
申请日：1999-07-02
申请人： Joseph D. Rigney , Irene T. Spitsberg , Ramgopal Darolia
发明人： Joseph D. Rigney , Irene T. Spitsberg , Ramgopal Darolia
IPC分类号： B32B1500
CPC分类号： C23C28/00
摘要： A coating is described for use on a superalloy substrate comprising a diffusion barrier as an intermediate layer overlying the substrate and underlying a protective coating having a high aluminum content. The diffusion barrier layer is characterized by having low interdiffusivity for elements from the substrate and the coating, a minimal impact on the mechanical properties of the article which is coated, and can be achieved readily using existing coating application techniques or post heat treat processes. The diffusion barrier layer is preferably an oxide ceramic.
摘要翻译：描述了一种用于超级合金基底的涂层，其包括扩散阻挡层作为覆盖在基底上的中间层，并且具有高铝含量的保护涂层。扩散阻挡层的特征在于对于来自基底和涂层的元件的相互扩散性低，对被涂覆的制品的机械性能的影响最小，并且可以容易地使用现有的涂布应用技术或后热处理工艺来实现。扩散阻挡层优选为氧化物陶瓷。

4. 发明授权

US06306524B1 Diffusion barrier layer 失效
标题翻译：扩散阻挡层
公开(公告)号：US06306524B1
公开(公告)日：2001-10-23
申请号：US09275096
申请日：1999-03-24
申请人： Irene T. Spitsberg , Ramgopal Darolia , Melvin R. Jackson , Ji-Cheng Zhao , Jon C. Schaeffer
发明人： Irene T. Spitsberg , Ramgopal Darolia , Melvin R. Jackson , Ji-Cheng Zhao , Jon C. Schaeffer
IPC分类号： B32B1500
CPC分类号： C23C28/321 , B32B15/01 , C22C5/04 , C22C27/00 , C23C28/3215 , C23C28/3455 , Y10T428/12535 , Y10T428/12611 , Y10T428/12743 , Y10T428/1275 , Y10T428/12764 , Y10T428/12875 , Y10T428/12944
摘要： A coating for use on a superalloy substrate comprising a diffusion barrier as an intermediate layer overlying the substrate and underlying a protective coating having a high aluminum content. The diffusion barrier layer is characterized by having low solubility for aluminum from either the substrate or the protective coating. Further, the diffusion barrier layer has low interdiffusivity for elements from the substrate and the coating, a minimal impact on the mechanical properties of the article which is coated, a minimal thermal expansion mismatch with both the substrate and the high aluminum content protective coating, and can be applied readily using existing coating application techniques. The diffusion barrier is preferably a single phase alloy or intermetallic compound.
摘要翻译：一种用于超级合金基底上的涂层，包括扩散阻挡层作为覆盖在基底上的中间层，并且具有高铝含量的保护涂层。扩散阻挡层的特征在于从基底或保护涂层对铝的溶解度低。此外，扩散阻挡层对于来自基底和涂层的元件具有低的相互扩散性，对被涂覆的制品的机械性能的最小影响与基底和高铝含量保护涂层的最小热膨胀失配，以及可以使用现有的涂布应用技术容易地应用。扩散阻挡层优选为单相合金或金属间化合物。

5. 发明授权

US5985470A Thermal/environmental barrier coating system for silicon-based materials 失效
标题翻译：硅基材料的热/环境屏障涂层系统
公开(公告)号：US5985470A
公开(公告)日：1999-11-16
申请号：US39477
申请日：1998-03-16
申请人： Irene T. Spitsberg , Hongyu Wang
发明人： Irene T. Spitsberg , Hongyu Wang
IPC分类号： C23C14/02 , C23C28/04 , B32B17/06
CPC分类号： C04B41/89 , C04B41/009 , C04B41/52 , C23C14/024 , C23C28/04 , C23C28/042
摘要： A coating system for a substrate containing a silicon-based material, such as silicon carbide-containing ceramic matrix materials containing silicon carbide and used to form articles exposed to high temperatures, including the hostile thermal environment of a gas turbine engine. The coating system includes a layer of barium strontium aluminosilicate (BSAS) as a bond coat for a thermal-insulating top coat. As a bond coat, the BSAS layer serves to adhere the top coat to a SiC-containing substrate. The BSAS bond coat exhibits sufficient environmental resistance such that, if the top coat should spall, the BSAS bond coat continues to provide a level of environmental protection to the underlying SiC-containing substrate.
摘要翻译：一种用于包含硅基材料的基底的涂层系统，例如含有碳化硅的含碳化硅的陶瓷基体材料，用于形成暴露于高温的制品，包括燃气涡轮发动机的恶劣热环境。涂层系统包括作为绝热顶涂层的粘合涂层的硅酸钡锶钡（BSAS）层。作为粘合涂层，BSAS层用于将顶涂层粘附到含SiC基材上。 BSAS粘合涂层表现出足够的耐环境性，使得如果顶涂层应该剥落，BSAS粘合涂层继续为下面的含SiC基材提供一定程度的环境保护。

6. 发明授权

US06296909B1 Method for thermally spraying crack-free mullite coatings on ceramic-based substrates 失效
标题翻译：在陶瓷基底上热喷涂无裂纹莫来石涂层的方法
公开(公告)号：US06296909B1
公开(公告)日：2001-10-02
申请号：US09569289
申请日：2000-05-11
申请人： Irene T. Spitsberg , Hongyu Wang , Raymond W. Heidorn
发明人： Irene T. Spitsberg , Hongyu Wang , Raymond W. Heidorn
IPC分类号： C23C410
CPC分类号： C04B41/87 , C04B41/009 , C04B41/5037 , C23C4/11 , C04B41/0072 , C04B41/4527 , C04B35/565 , C04B35/806
摘要： A process for depositing a mullite coating on a silicon-based material, such as those used to form articles exposed to high temperatures and including the hostile thermal environment of a gas turbine engine. The process is generally to thermally spray a mullite powder to form a mullite layer on a substrate, in which the thermal spraying process is performed so that the mullite powder absorbs a sufficient low level of energy from the thermal source to prevent evaporation of silica from the mullite powder. Processing includes deposition parameter adjustments or annealing to maintain or reestablish phase equilibrium in the mullite layer, so that through-thickness cracks in the mullite layer are avoided.
摘要翻译：用于在硅基材料上沉积莫来石涂层的方法，例如用于形成暴露于高温并且包括燃气涡轮发动机的恶劣热环境的制品的那些。该方法通常是将莫来石粉末热喷涂以在基材上形成莫来石层，其中进行热喷涂工艺，使得莫来石粉末从热源吸收足够的低水平的能量以防止二氧化硅从莫来石粉。处理包括沉积参数调整或退火以维持或重新建立莫来石层中的相平衡，从而避免莫来石层中的贯穿厚度的裂纹。

7. 发明授权

US06444335B1 Thermal/environmental barrier coating for silicon-containing materials 有权
标题翻译：含硅材料的热/环境屏障涂层
公开(公告)号：US06444335B1
公开(公告)日：2002-09-03
申请号：US09543956
申请日：2000-04-06
申请人： Hongyu Wang , Irene T. Spitsberg , Bangalore A. Nagaraj
发明人： Hongyu Wang , Irene T. Spitsberg , Bangalore A. Nagaraj
IPC分类号： B32B900
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C23C28/04 , F01D5/288 , C04B41/5037 , C04B41/5024 , C04B41/5042 , C04B41/522 , C04B41/5031 , C04B35/565 , C04B35/584 , C04B35/806
摘要： A coating system for Si-containing material, such as those used to form articles exposed to high temperatures, including the hostile thermal environment of a gas turbine engine. The coating system is a compositionally-graded thermal/environmental barrier coating (T/EBC) system that exhibits improved mechanical integrity for high application temperatures that necessitate thick protective coatings. The T/EBC system includes an intermediate layer containing YSZ and BSAS, mullite and/or alumina, which is preferably used in combination with a mullite-containing layer that overlies the surface of the Si-containing material, a layer of BSAS between the mullite-containing layer and the intermediate layer, and a thermal-insulating top coat of YSZ overlying the intermediate layer.
摘要翻译：用于含Si材料的涂层系统，例如用于形成暴露于高温的制品的涂层系统，包括燃气涡轮发动机的恶劣热环境。涂层系统是一种组分梯度的热/环境屏障涂层（T / EBC）系统，其在高应用温度下表现出改善的机械完整性，这需要厚的保护涂层。 T / EBC系统包括含有YSZ和BSAS，富铝红柱石和/或氧化铝的中间层，其优选与在含Si材料的表面上的含莫来石层的组合使用，莫来石之间的BSAS层中间层和覆盖中间层的YSZ绝热顶涂层。

8. 发明授权

US06387456B1 Silicon based substrate with environmental/thermal barrier layer 有权
标题翻译：具有环境/热障层的硅基衬底
公开(公告)号：US06387456B1
公开(公告)日：2002-05-14
申请号：US09655123
申请日：2000-09-05
申请人： Harry Edwin Eaton, Jr. , William Patrick Allen , Nathan S. Jacobson , Narottam P. Bansal , Elizabeth J. Opila , James L. Smialek , Kang N. Lee , Irene T. Spitsberg , Hongyu Wang , Peter Joel Meschter , Krishan Lal Luthra
发明人： Harry Edwin Eaton, Jr. , William Patrick Allen , Nathan S. Jacobson , Narottam P. Bansal , Elizabeth J. Opila , James L. Smialek , Kang N. Lee , Irene T. Spitsberg , Hongyu Wang , Peter Joel Meschter , Krishan Lal Luthra
IPC分类号： C23C406
CPC分类号： C04B41/009 , C04B41/5024 , C04B41/52 , C04B41/85 , C04B41/89 , C23C4/02 , C23C4/11 , C23C4/18 , C23C28/042 , C04B41/0072 , C04B41/4527 , C04B41/53 , C04B41/5096 , C04B41/4529 , C04B41/4556 , C04B41/5035 , C04B41/522 , C04B41/5037 , C04B35/565 , C04B35/584 , C04B35/806 , C04B35/597
摘要： A barrier layer for a silicon containing substrate which inhibits the formation of gaseous species of silicon when exposed to a high temperature aqueous environment comprises a barium-strontium alumino silicate.
摘要翻译：用于含硅衬底的阻挡层，其在暴露于高温水溶液环境中时抑制气态物质的形成包括钡 - 锶铝硅酸盐。

9. 发明授权

US06551423B1 Preparation of low-sulfur platinum and platinum aluminide layers in thermal barrier coatings 失效
标题翻译：在热障涂层中制备低硫铂和铂铝化物层
公开(公告)号：US06551423B1
公开(公告)日：2003-04-22
申请号：US09149018
申请日：1998-09-08
申请人： Irene T. Spitsberg , William S. Walston , Jon C. Schaeffer
发明人： Irene T. Spitsberg , William S. Walston , Jon C. Schaeffer
IPC分类号： C25D510
CPC分类号： C23C28/321 , C23C26/00 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： A method for preparing a coated nickel-base superalloy article reduces the sulfur content of the surface region of the metallic coating layers to low levels, thereby improving the adhesion of the coating layers to the article. The method includes depositing a first layer of platinum overlying the surface of a substrate, depositing a second layer of aluminum over the platinum, and final desulfurizing the article by heating the article to elevated temperature, preferably in hydrogen, and removing a small amount of material from the surface that was exposed during the step of heating. A ceramic layer may be deposited over the desulfurized article. The article may also be similarly desulfurized at other points in the fabrication procedure.
摘要翻译：制备涂覆的镍基超级合金制品的方法将金属涂层的表面区域的硫含量降低到低水平，从而改善涂层对制品的粘附性。该方法包括沉积覆盖衬底表面的铂的第一层，在铂上沉积第二层铝，并通过将制品加热至升高的温度，优选在氢气中，并最终除去少量的材料，使制品最终脱硫从在加热步骤期间暴露的表面。陶瓷层可以沉积在脱硫制品上。该制品也可以在制造过程中的其它点类似地脱硫。

10. 发明授权

US06391475B1 Modified aluminum-containing protective coating and its preparation 失效
标题翻译：改性含铝保护涂料及其制备
公开(公告)号：US06391475B1
公开(公告)日：2002-05-21
申请号：US09522875
申请日：2000-03-10
申请人： Irene T. Spitsberg , David J. Wortman , Jon C. Schaeffer , Joseph D. Rigney
发明人： Irene T. Spitsberg , David J. Wortman , Jon C. Schaeffer , Joseph D. Rigney
IPC分类号： B32B1504
CPC分类号： F01D5/288 , C23C10/02 , C23C10/58 , C23C26/00 , C23C28/00 , Y02T50/67 , Y02T50/671 , Y10T428/12611 , Y10T428/1275 , Y10T428/12944
摘要： A nickel-base superalloy substrate has an overlying protective coating including a modified aluminum-containing protective layer. The modified aluminum-containing protective layer is formed of nickel, aluminum, calcium in an amount of from about 50 to about 300 parts per million by weight, and, optionally, elements interdiffused into the modified aluminum-containing protective layer from the substrate. Magnesium or barium may be used instead of or in addition to the calcium. A ceramic layer may overlie the modified aluminum-containing protective layer.
摘要翻译：镍基超合金基板具有覆盖保护涂层，其包括改性的含铝保护层。改性的含铝保护层由镍，铝，钙的重量百分比约为50〜300重量％，可选地，从基材相互扩散到改性含铝保护层中的元素形成。可以使用镁或钡代替钙或除钙之外。陶瓷层可以覆盖改性的含铝保护层。

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