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1. 发明授权

US08187566B2 Continuous method and apparatus of functionalizing carbon nanotube 有权
标题翻译：功能化碳纳米管的连续方法和装置
公开(公告)号：US08187566B2
公开(公告)日：2012-05-29
申请号：US12453947
申请日：2009-05-28
申请人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
发明人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： C01B31/04 , D01F9/12
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/174 , C01P2004/133 , Y02P20/544 , Y10S977/843 , Y10S977/847
摘要： The present invention relates to a continuous method for functionalizing a carbon nanotube, and more specifically, to a continuous method for functionalizing a carbon nanotube by feeding functional compounds having one or more functional group into a functionalizing reactor into which a carbon nanotube mixture including oxidizer is fed under a pressure of 50 to 400 atm and a temperature of 100 to 600° C. to a subcritical water or supercritical water condition of a pressure of 50 to 40 atm by using a continuously functionalizing apparatus to obtain the functionalized products, such that the functional group of the functional compound can be easily introduced to the carbon nanotube, thereby increasing the functionalized effect of the carbon nanotube and increasing the dispersibility accordingly.
摘要翻译：本发明涉及一种用于官能化碳纳米管的连续方法，更具体地说，涉及通过将具有一个或多个官能团的官能化合物加入到包含氧化剂的碳纳米管混合物的官能化反应器中来进行功能化的碳纳米管的连续方法在50〜400atm的压力和100〜600℃的温度下，通过使用连续的官能化装置，在压力为50〜40atm的亚临界水或超临界水条件下进料，得到官能化产物，功能性化合物的官能团可以容易地引入到碳纳米管中，从而增加碳纳米管的功能化作用并相应地提高分散性。

2. 发明申请

US20090269267A1 Continuous method and apparatus for functionalizing carbon nanotube 有权
标题翻译：用于碳纳米管功能化的连续方法和装置
公开(公告)号：US20090269267A1
公开(公告)日：2009-10-29
申请号：US12385820
申请日：2009-04-21
申请人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
发明人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： D01F9/12 , B01J19/00
CPC分类号： B82Y30/00 , B01J3/008 , B82Y40/00 , C01B32/174 , C01B2202/28 , Y02P20/544
摘要： The present invention relates to a continuous method and apparatus for functionalizing a carbon nanotube, and more specifically, to a continuous method and apparatus for functionalizing a carbon nanotube including preparing a functionalized product by functionalizing a carbon nanotube solution including nitro compound according to the following Chemical Formula 1 and carbon nanotube mixture including an oxidizer for forming nitric acid under subcritical water or supercritical water condition of 50 to 400 atm and a continuous method and apparatus for functionalizing a carbon nanotube under subcritical water or supercritical water condition using nitro compound without using strong acids or strong bases. R—(NOx)y [Chemical Formula 1] wherein Chemical Formula 1, R is alkyl group of C1 to C7 or aryl group of C6 to C20 and x and y are integers of 1 to 3 independently.
摘要翻译：本发明涉及一种用于碳纳米管的官能化的连续方法和装置，更具体地说，涉及一种用于官能化碳纳米管的连续方法和装置，包括通过官能化含有硝基化合物的碳纳米管溶液来制备官能化产物式1和碳纳米管混合物，其包括在亚临界水或超临界水条件下形成硝酸的氧化剂为50至400atm，以及使用硝基化合物而不使用强酸在亚临界水或超临界水条件下官能化碳纳米管的连续方法和装置或强碱。 R-（NOx）y [化学式1]其中化学式1，R是C1至C7的烷基或C6至C20的芳基，x和y独立地为1至3的整数。

3. 发明授权

US07998450B2 Continuous methods and apparatus of functionalizing carbon nanotube 有权
标题翻译：功能化碳纳米管的连续方法和装置
公开(公告)号：US07998450B2
公开(公告)日：2011-08-16
申请号：US12382949
申请日：2009-03-27
申请人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
发明人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： D01F9/12
CPC分类号： B01J3/008 , B01J2203/0625 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/28 , Y02P20/544 , Y10S977/742
摘要： The present invention relates to a continuous method and apparatus of functionalizing a carbon nanotube, and more specifically, to a continuous method of functionalizing a carbon nanotube under subcritical water or supercritical water conditions without additional functionalizing processes, comprising: a) continuously feeding the carbon nanotube solution and an oxidizer under a pressure of 50 to 400 atm, respectively or together, and then preheating the mixture of said carbon nanotube solution and said oxidizer; b) functionalizing the carbon nanotube in the preheated said mixture under the subcritical water or the supercritical water condition of 50 to 400 atm; c) cooling down the functionalized product into 0 to 100° C. and depressurizing the functionalized product into 1 to 10 atm; and d) recovering the cooled down and depressurized product.
摘要翻译：本发明涉及一种使碳纳米管官能化的连续方法和装置，更具体地说，涉及在亚临界水或超临界水条件下官能化碳纳米管的连续方法，而无需另外的官能化方法，包括：a）连续供给碳纳米管溶液和50〜400atm压力下的氧化剂一起，然后预热所述碳纳米管溶液和所述氧化剂的混合物; b）在亚临界水或超临界水条件下将预热的所述混合物中的碳纳米管官能化为50〜400atm; c）将官能化产物冷却至0至100℃，并将官能化产物减压至1至10atm; 和d）回收冷却和减压的产品。

4. 发明授权

US09567222B2 Blending improvement carbon-composite having carbon-nanotube and its continuous manufacturing method and apparatus 有权
标题翻译：具有碳纳米管的混合改进碳复合材料及其连续制造方法和装置
公开(公告)号：US09567222B2
公开(公告)日：2017-02-14
申请号：US13381451
申请日：2010-06-30
申请人： Man Woo Jung , Seong Yun Jeon , Seong Cheol Hong , Joo Hee Han , Joo Seok Oh , Jin Seo Lee , Seung Hoe Do
发明人： Man Woo Jung , Seong Yun Jeon , Seong Cheol Hong , Joo Hee Han , Joo Seok Oh , Jin Seo Lee , Seung Hoe Do
IPC分类号： H01B1/04 , H01B1/20 , B82Y30/00 , C01B31/02 , B82Y40/00
CPC分类号： C01B31/0273 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/174 , C01B2202/06 , Y02P20/544
摘要： Provided area carbon nanotube composite material obtained by treating a mixture including carbon nanotubes, at least one carbon compound other than carbon nanotubes and a dispersion medium under a sub-critical or super-critical condition of 50-400 atm, and a method for producing the same. More particularly, the method for producing a carbon nanotube composite material, includes: introducing a mixture including carbon nanotubes, at least one carbon compound other than carbon nanotubes and a dispersion medium into a preheating unit under a pressure of 1-400 atm to preheat the mixture; treating the preheated mixture under a sub-critical or super-critical condition of 50-400 atm; cooling and depressurizing the resultant product to 0-1000 C and 1-10 atm; and recovering the cooled and depressurized product. Provided also is an apparatus for producing a carbon nanotube composite material in a continuous manner.
摘要翻译：提供的区域碳纳米管复合材料，其通过在50-400atm的亚临界或超临界条件下处理包括碳纳米管，至少一种碳纳米管之外的碳化合物和分散介质的混合物而获得，相同。更具体地说，碳纳米管复合材料的制造方法包括：在1-400atm的压力下将包含碳纳米管，至少一种碳纳米管以外的碳化合物和分散介质的混合物引入预热单元中，以预热混合物; 在50-400大气压的亚临界或超临界条件下处理预热混合物; 将所得产物冷却和减压至0-1000℃和1-10atm; 并回收冷却和减压的产品。还提供连续地制造碳纳米管复合材料的装置。

5. 发明授权

US09051179B2 Continuous method and apparatus for functionalizing carbon nanotube 有权
标题翻译：用于碳纳米管功能化的连续方法和装置
公开(公告)号：US09051179B2
公开(公告)日：2015-06-09
申请号：US12385820
申请日：2009-04-21
申请人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
发明人： Jin Seo Lee , Joo Hee Han , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： B82Y30/00 , B01J3/00 , B82Y40/00 , C01B31/02
CPC分类号： B82Y30/00 , B01J3/008 , B82Y40/00 , C01B32/174 , C01B2202/28 , Y02P20/544
摘要： A continuous method for functionalizing a carbon nanotube includes preparing a carbon nanotube solution containing a nitro compound represented by chemical formula 1 as R—(NOx)y wherein R is an alkyl group of C1 to C7 or an aryl group of C6 to C20 and x and y are integers of 1 to 3 independently, a carbon nanotube and a solvent. An oxidizer for forming a nitric acid selected from the group consisting of the carbon nanotube, oxygen, air, ozone, hydrogen peroxide and a mixture thereof is mixed with the carbon nanotube solution at a front end of a functionalizing reactor and the carbon nanotube mixture is fed into the functionalizing reactor. A functionalized carbon nanotube is prepared by treating the carbon nanotube mixture fed into the functionalizing reactor under a subcritical water or supercritical water condition of 50 to 400 atm.
摘要翻译：用于官能化碳纳米管的连续方法包括制备含有由化学式1表示的硝基化合物作为R-（NO x）y的碳纳米管溶液，其中R是C1至C7的烷基或C6至C20的芳基，x y分别为1〜3的整数，碳纳米管和溶剂。将形成选自碳纳米管，氧气，空气，臭氧，过氧化氢及其混合物的硝酸的氧化剂与官能化反应器前端的碳纳米管溶液混合，碳纳米管混合物为进料到功能化反应器中。通过在50〜400atm的亚临界水或超临界水条件下处理进入官能化反应器的碳纳米管混合物制备官能化碳纳米管。

6. 发明申请

US20120112134A1 Blending Improvement Carbon-Composite having Carbon-Nanotube and its Continuous Manufacturing Method and Apparatus 有权
标题翻译：具有碳纳米管的共混改进碳复合材料及其连续制造方法和装置
公开(公告)号：US20120112134A1
公开(公告)日：2012-05-10
申请号：US13381451
申请日：2010-06-30
申请人： Man Woo Jung , Seong Yun Jeon , Seong Cheol Hong , Joo Hee Han , Joo Seok Oh , Jin Seo Lee , Seung Hoe Do
发明人： Man Woo Jung , Seong Yun Jeon , Seong Cheol Hong , Joo Hee Han , Joo Seok Oh , Jin Seo Lee , Seung Hoe Do
IPC分类号： H01B1/04 , B82Y30/00
CPC分类号： C01B31/0273 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/174 , C01B2202/06 , Y02P20/544
摘要： Provided area carbon nanotube composite material obtained by treating a mixture including carbon nanotubes, at least one carbon compound other than carbon nanotubes and a dispersion medium under a sub-critical or super-critical condition of 50-400 atm, and a method for producing the same. More particularly, the method for producing a carbon nanotube composite material, includes: introducing a mixture including carbon nanotubes, at least one carbon compound other than carbon nanotubes and a dispersion medium into a preheating unit under a pressure of 1-400 atm to preheat the mixture; treating the preheated mixture under a sub-critical or super-critical condition of 50-400 atm; cooling and depressurizing the resultant product to 0-1000 C and 1-10 atm; and recovering the cooled and depressurized product. Provided also is an apparatus for producing a carbon nanotube composite material in a continuous manner.
摘要翻译：提供的区域碳纳米管复合材料，其通过在50-400atm的亚临界或超临界条件下处理包括碳纳米管，至少一种碳纳米管之外的碳化合物和分散介质的混合物而获得，相同。更具体地说，碳纳米管复合材料的制造方法包括：在1-400atm的压力下将包含碳纳米管，至少一种碳纳米管以外的碳化合物和分散介质的混合物引入预热单元中，以预热混合物; 在50-400大气压的亚临界或超临界条件下处理预热混合物; 将所得产物冷却和减压至0-1000℃和1-10atm; 并回收冷却和减压的产品。还提供连续地制造碳纳米管复合材料的装置。

7. 发明申请

US20120093710A1 PURIFIED CARBON NANOTUBES 审中-公开
标题翻译：纯化碳纳米管
公开(公告)号：US20120093710A1
公开(公告)日：2012-04-19
申请号：US13323283
申请日：2011-12-12
申请人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
发明人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： D01F9/12 , B82Y30/00
CPC分类号： C01B32/17 , B82Y30/00 , B82Y40/00 , Y02P20/544 , Y10S977/843 , Y10S977/847
摘要： Provided is a continuous method and apparatus of purifying carbon nanotubes. The continuous method and apparatus of purifying carbon nanotubes is characterized in a first purifying step for injecting a carbon nanotube liquid mixture containing an oxidizer into a purifying reactor under a sub-critical water or supercritical water condition at a pressure of 50 to 400 atm and a temperature of 100 to 600° C. to obtain a purified product, thereby removing amorphous carbon and producing the carbon nanotube product.
摘要翻译：提供了一种净化碳纳米管的连续方法和装置。净化碳纳米管的连续方法和装置的特征在于，在亚临界水或超临界水条件下，在50〜400atm的压力下，将含有氧化剂的碳纳米管液体混合物注入净化反应器中，温度为100〜600℃，得到纯化物，除去无定形碳，生成碳纳米管制品。

8. 发明申请

US20100065776A1 Continuous methods and apparatus of functionalizing carbon nanotube 有权
标题翻译：功能化碳纳米管的连续方法和设备
公开(公告)号：US20100065776A1
公开(公告)日：2010-03-18
申请号：US12382949
申请日：2009-03-27
申请人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
发明人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： C09K3/00 , C01B31/00 , B01J3/00
CPC分类号： B01J3/008 , B01J2203/0625 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/28 , Y02P20/544 , Y10S977/742
摘要： The present invention relates to a continuous method and apparatus of functionalizing a carbon nanotube, and more specifically, to a continuous method of functionalizing a carbon nanotube under subcritical water or supercritical water conditions without additional functionalizing processes, comprising: a) continuously feeding the carbon nanotube solution and an oxidizer under a pressure of 50 to 400 atm, respectively or together, and then preheating the mixture of said carbon nanotube solution and said oxidizer; b) functionalizing the carbon nanotube in the preheated said mixture under the subcritical water or the supercritical water condition of to 400 atm; c) cooling down the functionalized product into 0 to 100° C. and depressurizing the functionalized product into 1 to 10 atm; and d) recovering the cooled down and depressurized product.
摘要翻译：本发明涉及一种使碳纳米管官能化的连续方法和装置，更具体地说，涉及在亚临界水或超临界水条件下官能化碳纳米管的连续方法，而无需另外的官能化方法，包括：a）连续供给碳纳米管溶液和50〜400atm压力下的氧化剂一起，然后预热所述碳纳米管溶液和所述氧化剂的混合物; b）在亚临界水或超临界水条件下将预热的所述混合物中的碳纳米管官能化至400atm; c）将官能化产物冷却至0至100℃，并将官能化产物减压至1至10atm; 和d）回收冷却和减压的产品。

9. 发明授权

US09624379B2 High-efficiency heat-dissipating paint composition using a carbon material 有权
公开(公告)号：US09624379B2
公开(公告)日：2017-04-18
申请号：US13814057
申请日：2011-08-05
申请人： Seung Hoe Do , Seong Cheol Hong , Jin Seo Lee , Joo Hee Han
发明人： Seung Hoe Do , Seong Cheol Hong , Jin Seo Lee , Joo Hee Han
IPC分类号： C09K13/00 , C09D5/00 , C09K5/00 , C09D7/12 , C09D133/04 , H01L23/373 , H05K7/20 , C08K3/04 , C08K5/544 , C08K7/24 , C08K9/02
CPC分类号： C09D5/00 , C08K3/04 , C08K3/041 , C08K3/042 , C08K3/046 , C08K5/544 , C08K7/24 , C08K9/02 , C09D7/62 , C09D7/65 , C09D7/70 , C09D133/04 , C09K5/00 , H01L23/373 , H01L23/3737 , H01L2924/0002 , H05K7/20427 , H01L2924/00
摘要： Provided is a heat-dissipating paint composition using a carbon material, the heat-dissipating paint composition including a dispersion solution containing a surface treated carbon material, a heat resistance additive, and an adhesion improving emulsion, so that the heat-dissipating paint composition can have excellent heat dissipation performance and can be applied to various industrial field requiring temperature control.

10. 发明授权

US09045345B2 Apparatus for purifying carbon nanotubes 有权
标题翻译：碳纳米管净化装置
公开(公告)号：US09045345B2
公开(公告)日：2015-06-02
申请号：US13323255
申请日：2011-12-12
申请人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
发明人： Joo Hee Han , Jin Seo Lee , Seung-Hoe Do , Seong Cheol Hong
IPC分类号： D01F9/12 , B82Y40/00 , C01B31/02 , B82Y30/00
CPC分类号： C01B31/026 , B82Y30/00 , B82Y40/00 , C01B32/17 , Y02P20/544 , Y10S977/843 , Y10S977/847
摘要： Provided is a continuous method and apparatus of purifying carbon nanotubes. The continuous method and apparatus of purifying carbon nanotubes is characterized in a first purifying step for injecting a carbon nanotube liquid mixture containing an oxidizer into a purifying reactor under a sub-critical water or supercritical water condition at a pressure of 50 to 400 atm and a temperature of 100 to 600° C. to obtain a purified product, thereby removing amorphous carbon and producing the carbon nanotube product.
摘要翻译：提供了一种净化碳纳米管的连续方法和装置。净化碳纳米管的连续方法和装置的特征在于，在亚临界水或超临界水条件下，在50〜400atm的压力下，将含有氧化剂的碳纳米管液体混合物注入净化反应器中，温度为100〜600℃，得到纯化物，除去无定形碳，生成碳纳米管制品。

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