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1. 发明授权

US5177181A Diamines and photosensitive polyimides made therefrom 失效
标题翻译： DIAMINES和光敏聚酰胺
公开(公告)号：US5177181A
公开(公告)日：1993-01-05
申请号：US710872
申请日：1991-06-06
申请人： Jerold Rosenfeld , Jin-O Choi , David Y. Tang , John Tyrell
发明人： Jerold Rosenfeld , Jin-O Choi , David Y. Tang , John Tyrell
IPC分类号： B05D7/24 , C07C217/80 , C07C229/54 , C07C229/60 , C07C235/46 , C07C237/30 , C08G73/10 , G03F7/038 , H01L21/027
CPC分类号： C08G73/1007 , C07C229/60 , C07C237/30 , C08G73/10 , C08G73/1039 , C08G73/1082 , G03F7/0387
摘要： Disclosed is an aromatic diamine having the general formula ##STR1## where A is a group containing at least one aromatic ring, each Y is independently selected from ##STR2## R is a group containing at least one olefinically unsaturated group, R' is hydrogen, alkyl to C.sub.25, aryl, or R, n is 1 to 4, and the number of olefinic groups in Y is at least 3 when each Y is ##STR3## and otherwise is at least 2. Photosensitive polyamic acids and polyimides can be prepared from the aromatic diamines which can be crosslinked with light to a mask to form patterns on a substrate.

2. 发明授权

US5914408A Olefin polymerization catalysts containing benzothiazole 失效
标题翻译：含有苯并噻唑的烯烃聚合催化剂
公开(公告)号：US5914408A
公开(公告)日：1999-06-22
申请号：US130846
申请日：1998-08-07
申请人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
发明人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
IPC分类号： B01J31/14 , B01J31/22 , C07F7/00 , C07F17/00 , C08F4/642 , C08F4/659 , C08F10/00 , C08F110/02 , B01J31/00
CPC分类号： B01J31/143 , B01J31/14 , B01J31/226 , B01J31/2295 , C07F17/00 , C07F7/006 , C08F10/00 , B01J2531/0236 , B01J2531/46 , B01J2531/48 , C08F2420/04 , C08F4/65908 , C08F4/65912 , C08F4/65916
摘要： A novel metallocene catalyst for the polymerization of olefin (co)polymers is of the general formula:Benzothiazole--E--M--X.sub.m L.sub.nwhere,M is a transition metal of Groups 3-10 of the Periodic Table;E is sulfur or oxygen; E being bond to the transition metal and to the carbon atom between sulfur and nitrogen of the benzothiazole moiety;L is a polymerization-stable anionic ancillary ligand;X is a halogen, alkoxy from C.sub.1 to C.sub.20, siloxy from C.sub.1 to C.sub.20, N(R.sub.1).sub.2, a hydrocarbyl group containing up to about 12 carbon atoms or hydrogen or mixtures thereof; preferably X is halogen, methoxy, ethoxy or siloxy (R.sub.1).sub.3 SiO--, where R.sub.1 is alkyl from C.sub.1 to C.sub.20 ; andm+n equals the valency of the M minus 1.
摘要翻译：用于烯烃（共）聚合物聚合的新型茂金属催化剂具有以下通式：苯并噻唑-E-M-XmL，其中M是周期表第3-10族的过渡金属; E是硫或氧; E键合到过渡金属和苯并噻唑部分的硫和氮之间的碳原子; L是聚合稳定的阴离子辅助配体; X是卤素，C1至C20的烷氧基，C1至C20的甲硅烷氧基，N（R1）2，含有至多约12个碳原子的烃基或氢或其混合物; 优选X是卤素，甲氧基，乙氧基或甲硅烷氧基（R1）3SiO-，其中R1是C1至C20的烷基; 而m + n等于M的化合价减1。

3. 发明授权

US06218486B1 Method of polymerizing vinyl chloride monomer using an organocobalt (III) catalyst 失效
标题翻译：使用有机钴（III）催化剂聚合氯乙烯单体的方法
公开(公告)号：US06218486B1
公开(公告)日：2001-04-17
申请号：US08812511
申请日：1997-03-07
申请人： Sandor Nagy , John Tyrell
发明人： Sandor Nagy , John Tyrell
IPC分类号： C08F216
CPC分类号： C08F14/06 , C08F4/80
摘要： Disclosed is a method of polymerizing vinyl chloride monomer using a catalyst having the general formula where L is a ligand covalently bonded to the cobalt atom, each D is independently selected from donor ligands, R is hydrogen, hydrocarbon from C1 to C30, or hydrohalocarbon from C1 to C30, and X− is an anion. The catalyst is activated by the addition of an acid.
摘要翻译：公开了一种使用具有一般形式的催化剂聚合氯乙烯单体的方法，L是与钴原子共价连接的配体，每个D独立地选自供体配体，R为氢，C1至C30的烃或C1的氢卤化碳至C30，X-为阴离子。通过加入酸活化催化剂。

4. 发明授权

US06462153B1 Method of polymerizing vinyl chloride monomer 失效
标题翻译：聚合氯乙烯单体的方法
公开(公告)号：US06462153B1
公开(公告)日：2002-10-08
申请号：US08627202
申请日：1996-04-03
申请人： Sandor Nagy , John Tyrell
发明人： Sandor Nagy , John Tyrell
IPC分类号： C08F444
CPC分类号： C08F14/06 , C08F4/68
摘要： Disclosed is a catalyst composition and a method of polymerizing vinyl chloride using it. The catalyst composition is a mixture of a vanadyl (V) catalyst having the formula and about 0.5 to about 15 moles of an alkyl aluminum cocatalyst having the formula (R′)mAl(X′)3−m per mole of said catalyst, where R is a group containing 1 to 14 carbon atoms, each X is independently selected from halogen or OR, each R′ is independently selected from alkyl from C1 to C10, each X′ is independently selected from halogen, R1 is alkyl from C1 to C10, haloalkyl from C1 to C10, alkoxyalkyl where each alkyl group is independently selected from C1 to C10, or aryl from C6 to C14, m is 1 or 2, and n is 1 to 100. Also disclosed is a method of polymerizing vinyl chloride comonomer using this catalyst.
摘要翻译：公开了使用它的聚合氯乙烯的催化剂组合物和方法。催化剂组合物是具有下式的氧钒（V）催化剂和约0.5至约15摩尔具有所述催化剂的配方摩尔的烷基铝助催化剂的混合物，其中R是含有1至14个碳原子的基团，每个X是独立地选自卤素或OR，每个R'独立地选自C 1至C 10的烷基，每个X'独立地选自卤素，R 1是C 1至C 10的烷基，C 1至C 10的卤代烷基，各烷基独立地为烷氧基烷基选自C1至C10，或由C6至C14的芳基，m为1或2，n为1至100.还公开了使用该催化剂聚合氯乙烯共聚单体的方法。

5. 发明授权

US6114270A Polymerization-stable anionic ancillary ligand containing alkylimido catalysts and method of using the same 失效
标题翻译：含有烷基亚氨基的催化剂的聚合稳定的阴离子辅助配体及其使用方法
公开(公告)号：US6114270A
公开(公告)日：2000-09-05
申请号：US131132
申请日：1998-08-07
申请人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
发明人： Ramesh Krishnamurti , Sandor Nagy , John Tyrell , Bradley P. Etherton
IPC分类号： B01J31/14 , B01J31/18 , B01J31/22 , C08F4/02 , C08F4/44 , C08F4/60 , C08F4/639 , C08F4/645 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , B01J31/00 , B01J37/00
CPC分类号： B01J31/143 , B01J31/1805 , B01J31/2295 , C08F10/00 , B01J2531/46 , B01J2531/48 , B01J2531/57 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/63912 , Y10S526/943
摘要： Single-site catalyst systems containing alkylimido ligands are disclosed. The catalyst systems comprise a co-catalyst and a Group 3-10 transition metal catalyst. The catalyst includes an alkyl- or arylimido ligand and a polymerization-stable, anionic ligand selected from boraaryl, pyrrolyl, and azaborolinyl. When used to polymerize olefins, the catalyst systems are highly productive, give good comonomer incorporation, and give polymers with narrow molecular weight distributions.
摘要翻译：公开了含有烷基亚氨基配体的单位点催化剂体系。催化剂体系包括助催化剂和3-10族过渡金属催化剂。催化剂包括烷基 - 或芳基亚氨基配位体和选自硼芳基，吡咯基和氮杂硼烷基的聚合稳定的阴离子配体。当用于聚合烯烃时，催化剂体系是高生产率的，提供良好的共聚单体掺入，并得到具有窄分子量分布的聚合物。

6. 发明授权

US6008394A Sulfonyl catalysts and method of using the same 失效
标题翻译：磺酰基催化剂及其使用方法
公开(公告)号：US6008394A
公开(公告)日：1999-12-28
申请号：US130701
申请日：1998-08-07
申请人： Sandor Nagy , John Tyrell , Bradley P. Etherton
发明人： Sandor Nagy , John Tyrell , Bradley P. Etherton
IPC分类号： B01J31/22 , C07F17/00 , C08F4/06 , C08F4/44 , C08F4/602 , C08F4/643 , C08F4/659 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16
CPC分类号： B01J31/14 , B01J31/2295 , C07F17/00 , C08F10/00 , B01J2231/12 , B01J2531/30 , B01J2531/40 , B01J2531/46 , B01J2531/48 , B01J2531/50 , B01J2531/60 , B01J2531/70 , B01J2531/80 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/65912 , Y10S526/943
摘要： A novel metallocene catalyst for the polymerization of olefin (co)polymers is of the general formula:R--SO.sub.2 --L--M--(X).sub.m T.sub.nwherein,M is a metal selected from Groups 3-10;T is a polymerization-stable anionic ancillary ligand;m+n is the valency of M minus 1;R is a C.sub.1 -C.sub.20 alkyl group, a C.sub.6 -C.sub.20 aryl ring or a C.sub.6 -C.sub.20 alkaryl or aralkyl group, optionally substituted with a halogen or an alkoxy group up to 10 carbon atoms;X is a halogen, alkoxy from C.sub.1 to C.sub.20, siloxy from C.sub.1 to C.sub.20, N(R).sub.2, a hydrocarbyl group containing up to about 12 carbon atoms, hydrogen or another univalent anionic ligand, or mixtures thereof;L is T as defined above with the proviso that one of the sites available for substitution is the attachment site of the sulfonyl group; andwherein L and T may be bridged.
摘要翻译：用于烯烃（共）聚合物聚合的新型茂金属催化剂具有以下通式：R-SO2-L-M-（X）mTn其中，M是选自3-10族的金属; T是聚合稳定的阴离子辅助配体; m + n是M的化合价减1; R是任选被卤素或至多10个碳原子的烷氧基取代的C 1 -C 20烷基，C 6 -C 20芳基环或C 6 -C 20烷芳基或芳烷基; X是卤素，C1至C20的烷氧基，C1至C20的甲硅烷氧基，N（R）2，含有至多约12个碳原子的烃基，氢或其它一价阴离子配体，或其混合物; L是如上定义的T，条件是可用于取代的一个位点是磺酰基的连接位点; 并且其中L和T可以桥连。

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