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1. 发明申请

US20090178928A1 Process for Desalting Glycerol Solutions and Recovery of Chemicals 审中-公开
标题翻译：脱盐甘油溶液和化学品回收工艺
公开(公告)号：US20090178928A1
公开(公告)日：2009-07-16
申请号：US12165384
申请日：2008-06-30
申请人： Jeremie Ray GROOS , Ahmad K. Hilaly , Krishnamurthy Mani , Rishi Shukla
发明人： Jeremie Ray GROOS , Ahmad K. Hilaly , Krishnamurthy Mani , Rishi Shukla
IPC分类号： B01D61/44 , B01D61/46
CPC分类号： C11C1/08 , B01D61/42 , B01D61/445 , B01D61/58 , C07C29/76 , C07C67/03 , C10G2300/1011 , C11C3/003 , Y02E50/13 , Y02P30/20 , C07C31/225 , C07C69/52 , C07C69/24
摘要： Processes for desalting glycerol-rich solutions or process streams using electrodialysis are provided. The glycerol-rich process streams are typically byproducts from the production of biodiesel. Following electrodialysis, the resulting aqueous salt solution is placed in a water splitting cell to recover the acid and base components of the salt. These acid and base components, in turn, can be reused in other processes, such as biodiesel production.
摘要翻译：提供了使用电渗析脱盐富含甘油的溶液或工艺流的方法。富含甘油的工艺流通常是来自生物柴油生产的副产物。电渗析后，将所得的盐水溶液置于水分解池中以回收盐的酸和碱组分。这些酸和碱组分又可以用于其他工艺，例如生物柴油生产。

2. 发明授权

US07776369B2 Process for obtaining lignans 失效
标题翻译：获得木酚素的方法
公开(公告)号：US07776369B2
公开(公告)日：2010-08-17
申请号：US12184451
申请日：2008-08-01
申请人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
发明人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
IPC分类号： A61K36/05 , A61K36/00
CPC分类号： C07G1/00 , A61K36/00 , A61K36/55
摘要： Process for obtaining lignan from plant material by extraction with an extraction solvent and separation of the liquid fraction from the plant material. The separated liquid fraction containing the lignan product is subjected to further processing to remove cyanogenic sugars and other impurities. The resulting lignan containing product may be formulated for the treatment of various conditions, such as cancer, diabetes, hypertension, lupus, and atherosclerosis.
摘要翻译：通过用萃取溶剂萃取并从液料中分离液体馏分从植物材料中获得木酚素的方法。将含有木质素产物的分离的液体馏分进行进一步处理以除去氰基糖和其它杂质。所得到的含木酚素的产品可以配制用于治疗各种病症，例如癌症，糖尿病，高血压，狼疮和动脉粥样硬化。

3. 发明授权

US06767565B2 Process for obtaining lignan 失效
标题翻译：获得木酚素的方法
公开(公告)号：US06767565B2
公开(公告)日：2004-07-27
申请号：US10101423
申请日：2002-03-20
申请人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
发明人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
IPC分类号： A61K3578
CPC分类号： C07G1/00 , A61K36/00 , A61K36/55
摘要： Process for obtaining lignan from plant material by extraction with an extraction solvent and separation of the liquid fraction from the plant material. The separated liquid fraction containing the lignan product is subjected to further processing to remove cyanogenic sugars and other impurities. The resulting lignan containing product may be formulated for the treatment of various conditions, such as cancer, diabetes, hypertension, lupus, and atherosclerosis.
摘要翻译：通过用萃取溶剂萃取并从液料中分离液体馏分从植物材料中获得木酚素的方法。将含有木质素产物的分离的液体馏分进行进一步处理以除去氰基糖和其它杂质。所得到的含木酚素的产品可以配制用于治疗各种病症，例如癌症，糖尿病，高血压，狼疮和动脉粥样硬化。

4. 发明申请

US20080317888A1 PROCESS FOR OBTAINING LIGNANS 失效
标题翻译：获取LIGNANS的过程
公开(公告)号：US20080317888A1
公开(公告)日：2008-12-25
申请号：US12184451
申请日：2008-08-01
申请人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
发明人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
IPC分类号： A61K36/55 , C08L97/00
CPC分类号： C07G1/00 , A61K36/00 , A61K36/55
摘要： Process for obtaining lignan from plant material by extraction with an extraction solvent and separation of the liquid fraction from the plant material. The separated liquid fraction containing the lignan product is subjected to further processing to remove cyanogenic sugars and other impurities. The resulting lignan containing product may be formulated for the treatment of various conditions, such as cancer, diabetes, hypertension, lupus, and atherosclerosis.
摘要翻译：通过用萃取溶剂萃取并从液料中分离液体馏分从植物材料中获得木酚素的方法。将含有木质素产物的分离的液体馏分进行进一步处理以除去氰基糖和其它杂质。所得到的含木酚素的产品可以配制用于治疗各种病症，例如癌症，糖尿病，高血压，狼疮和动脉粥样硬化。

5. 发明授权

US07407676B2 Lignan extracts and compositions including the lignan extracts 失效
标题翻译：木质素提取物和包含木质素提取物的组合物
公开(公告)号：US07407676B2
公开(公告)日：2008-08-05
申请号：US10861948
申请日：2004-06-04
申请人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
发明人： Rishi Shukla , Ahmad K. Hilaly , Kevin M. Moore
IPC分类号： A61K36/05 , A61K36/00
CPC分类号： C07G1/00 , A61K36/00 , A61K36/55
摘要： Process for obtaining lignan from plant material by extraction with an extraction solvent and separation of the liquid fraction from the plant material. The separated liquid fraction containing the lignan product is subjected to further processing to remove cyanogenic sugars and other impurities. The resulting lignan containing product may be formulated for the treatment of various conditions, such as cancer, diabetes, hypertension, lupus, and atherosclerosis.
摘要翻译：通过用萃取溶剂萃取并从液料中分离液体馏分从植物材料中获得木酚素的方法。将含有木质素产物的分离的液体馏分进行进一步处理以除去氰基糖和其它杂质。所得到的含木酚素的产品可以配制用于治疗各种病症，例如癌症，糖尿病，高血压，狼疮和动脉粥样硬化。

6. 发明申请

US20100093530A1 METHOD OF PREPARING A COMPOSITION USING ARGENTATION CHROMATOGRAPHY 有权
标题翻译：使用归一化色谱法制备组合物的方法
公开(公告)号：US20100093530A1
公开(公告)日：2010-04-15
申请号：US12639137
申请日：2009-12-16
申请人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
发明人： Thomas P. Binder , Doug Geier , Ahmad K. Hilaly , Robert Duane Sandage , John G. Soper
IPC分类号： B01J20/26
CPC分类号： B01D15/1828 , B01D15/20 , B01D15/362 , B01J20/0233 , B01J20/284 , B01J20/3234 , B01J20/3236 , B01J47/016 , C07C67/56 , C11B3/10 , G01N30/462 , C07C69/587 , C07C69/58
摘要： The present invention is directed to a method of preparing compositions enriched in compounds containing carbon chains of varying degrees of unsaturation using argentation chromatography. The present method utilizes an argentized cationic resin or a conditioned argentized alumina to separate compounds containing saturated or mono-unsaturated carbon chains from compounds having polyunsaturated carbon chains present in a starting composition. The invention is particularly useful for preparing a composition enriched in polyunsaturated fatty acid alkyl esters from mixtures of fatty acid esters in a starting composition derived from vegetable oils. The present invention is also directed to a method of preparing a conditioned argentized alumina adsorbent having increased selectivity for compounds containing one or more polyunsaturated carbon chains.
摘要翻译：本发明涉及使用梯度色谱法制备富集含有不同不饱和度的碳链的化合物的组合物的方法。本方法利用阳离子阳离子树脂或调节的氧化铝将起始组合物中存在的具有多不饱和碳链的化合物与饱和或单不饱和碳链分开。本发明特别可用于在源自植物油的起始组合物中由脂肪酸酯的混合物制备富含多不饱和脂肪酸烷基酯的组合物。本发明还涉及一种制备具有对含有一个或多个多不饱和碳链的化合物具有增加的选择性的调节的氧化铝吸附剂的方法。

7. 发明授权

US07705170B2 Method of preparing fatty acid alkyl esters from waste or recycled fatty acid stock 有权
标题翻译：从废物或再循环脂肪酸原料制备脂肪酸烷基酯的方法
公开(公告)号：US07705170B2
公开(公告)日：2010-04-27
申请号：US11102869
申请日：2005-04-11
申请人： Douglas F. Geier , Ahmad K. Hilaly , John G. Soper
发明人： Douglas F. Geier , Ahmad K. Hilaly , John G. Soper
IPC分类号： C11C1/00
CPC分类号： C11C3/003 , C10L1/026 , C11B13/02 , C11C1/02 , C11C1/08 , C11C1/10 , Y02E50/13 , Y02W30/74
摘要： The present invention is directed to a method or preparing fatty acid alkyl esters from fatty acids contained in co-product streams, or waste or recycled fatty acid stock. The present method utilizes an acidic resin to convert the fatty acid stock into esters. The present method encompasses the use of reactive simulated moving bed chromatography, wherein above about 95 percent of the fatty acid stock is converted to fatty acid alkyl esters. The present method has been optimized to separate the ester product from the raffinate stream formed during the chromatographic process, thereby improving the yield of the esterification and preventing acid hydrolysis of the ester.
摘要翻译：本发明涉及由共同产物流中所含脂肪酸或废物或再循环脂肪酸原料制备脂肪酸烷基酯的方法或方法。本方法利用酸性树脂将脂肪酸原料转化成酯。本方法包括使用反应性模拟移动床层析法，其中高于约95％的脂肪酸原料转化为脂肪酸烷基酯。本发明方法已被优化以将酯产物与色谱过程中形成的萃余液流分离，从而提高酯化产率并防止酯的酸水解。

8. 发明授权

US06479700B2 Method for separating a basic amino acid from fermentation broth 有权
标题翻译：从发酵液中分离出碱性氨基酸的方法
公开(公告)号：US06479700B2
公开(公告)日：2002-11-12
申请号：US09808123
申请日：2001-03-15
申请人： John Soper , Ahmad K. Hilaly , Kevin Moore , Thomas P. Binder
发明人： John Soper , Ahmad K. Hilaly , Kevin Moore , Thomas P. Binder
IPC分类号： C07C22700
CPC分类号： C07C227/40 , C07C229/26
摘要： This invention relates to a method for separating basic amino acids from fermentation broth comprising contacting the broth with strong acid cation exchange resins that have a low degree of cross-linkage and eluting the amino acid. The method described herein results in higher yield and higher purity of lysine, in addition to higher throughput, as compared to conventional processes of purification of lysine from fermentation broth.
摘要翻译：本发明涉及从发酵液中分离碱性氨基酸的方法，包括使肉汤与具有低交联度的氨基酸的强酸性阳离子交换树脂接触。与来自发酵液的赖氨酸的纯化的常规方法相比，本文所述的方法除了产生更高的产量之外还导致更高的产量和更高的赖氨酸纯度。

9. 发明授权

US07767178B2 Regenerating molecular sieve absorbents used for alcohol dehydration 有权
标题翻译：再生用于酒精脱水的分子筛吸附剂
公开(公告)号：US07767178B2
公开(公告)日：2010-08-03
申请号：US11581825
申请日：2006-10-17
申请人： Ahmad K. Hilaly , Joseph R. Beggin
发明人： Ahmad K. Hilaly , Joseph R. Beggin
IPC分类号： B01D53/02
CPC分类号： B01J20/3408 , B01D15/00 , B01J20/18 , B01J20/3458 , B01J20/3483 , B01J29/90 , B01J38/02 , B01J38/04 , C07C29/76 , Y02P20/584 , C07C31/08
摘要： A process for regenerating a molecular sieve absorbent bed used for dehydrating an organic solvent is disclosed. The process is illustrated by regenerating a molecular sieve bed used for dehydrating ethanol, which includes a dehydrating cycle where an ethanol/water vapor mixture is loaded onto the molecular sieve bed at a first temperature to absorb water and recover a substantially dehydrated ethanol vapor effluent. In a regeneration cycle, the bed is subjected to a temperature swing technique whereby a dried gas, such as dried CO2, heated to at a second temperature greater than the first temperature, is passed over the molecular sieve bed, optimally in a counter current directional flow with respect to the dehydrating cycle. The process obviates the need for applying a vacuum pressure swing to regenerate the molecular sieve bed. Water and residual ethanol are removed with the CO2 effluent and can optionally be condensed and combined with a feed input for a subsequent dehydrating cycle.
摘要翻译：公开了一种用于再生用于使有机溶剂脱水的分子筛吸收剂床的方法。该过程通过再生用于脱水乙醇的分子筛床来说明，其包括脱水循环，其中乙醇/水蒸汽混合物在第一温度下加载到分子筛床上以吸收水并回收基本上脱水的乙醇蒸汽流出物。在再生循环中，对床进行温度摆动技术，由此将加热到大于第一温度的第二温度的干燥的CO 2等干燥气体通过分子筛床，最佳地以逆流方向相对于脱水循环流动。该过程消除了施加真空压力摆动以再生分子筛床的需要。用CO 2流出物除去水和残余的乙醇，并且可任选地冷凝并与进料输入物组合以用于随后的脱水循环。

10. 发明授权

US06673945B2 Process for production of high purity tocopherols 失效
标题翻译：生产高纯度生育酚的方法
公开(公告)号：US06673945B2
公开(公告)日：2004-01-06
申请号：US10285700
申请日：2002-11-01
申请人： Thomas P. Binder , Ahmad K. Hilaly
发明人： Thomas P. Binder , Ahmad K. Hilaly
IPC分类号： C07D31172
CPC分类号： C07D311/72
摘要： This invention provides a method of separating tocopherols by using a weakly basic polyvinyl pyridine resin. The resin has the capacity to selectively bind tocopherols, allowing other impurities typically found in a tocopherol production plant stream to separate from the tocopherols. After loading a tocopherol-containing mixture onto a separatory column packed with the resin, the loaded column is eluted with a solvent followed by an alcohol. The eluate is collected in fractions, and the tocopherol-containing fractions are combined and concentrated to yield a purified tocopherol composition. It has been found that the present invention produces highly purified tocopherol compositions (90+%), and is particularly useful for preparing highly purified tocopherol compositions, specifically enriched in &agr;-tocopherol.
摘要翻译：本发明提供了使用弱碱性聚乙烯吡啶树脂分离生育酚的方法。树脂具有选择性结合生育酚的能力，允许通常在生育酚生产植物物流中发现的其它杂质与生育酚分离。将含有生育酚的混合物装载到装有树脂的分离柱上后，用溶剂洗脱负载的柱，然后用醇洗脱。将洗脱液以级分收集，并将含有生育酚的级分合并并浓缩，得到纯化的生育酚组合物。已经发现，本发明产生高度纯化的生育酚组合物（90 +％），并且特别可用于制备特别富含α-生育酚的高度纯化的生育酚组合物。

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