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1. 发明授权

US5972091A Starch replacement composition for corrugating adhesives and the adhesives prepared therewith 失效
标题翻译：用于波纹粘合剂的淀粉替代组合物和用其制备的粘合剂
公开(公告)号：US5972091A
公开(公告)日：1999-10-26
申请号：US10463
申请日：1998-01-21
申请人： J.E. Todd Giesfeldt , Jack R. Wallace , Tammi Brandt-Janel , Roman Skuratowicz
发明人： J.E. Todd Giesfeldt , Jack R. Wallace , Tammi Brandt-Janel , Roman Skuratowicz
IPC分类号： B31F1/00 , C09J103/02 , B32B3/28 , B05D1/26
CPC分类号： C09J103/02 , Y10T156/1016 , Y10T428/24694
摘要： A dry blend pre-mixture composition for use in making corrugating adhesives is comprised of starch and from about 5% to about 20% of ground plant germ. The starch and germ can be derived from various plant sources and in a preferred embodiment the starch is corn starch and the germ is ground corn germ, also known as spent flake. The corrugating adhesives can be prepared by using the pre-mixture as a replacement for starch in a process for making a carrier, no-carrier or carrier-no-carrier adhesive.
摘要翻译：用于制造波纹粘合剂的干混混合预混合物组合物由淀粉和约5％至约20％的地面植物胚芽组成。淀粉和胚芽可以衍生自各种植物来源，在优选的实施方案中，淀粉是玉米淀粉，胚芽是研磨的玉米胚芽，也称为废片。波纹粘合剂可以通过在制备载体，无载体或载体 - 无载体粘合剂的方法中使用预混物作为淀粉的替代物来制备。

2. 发明授权

US08507666B2 Modification of carbohydrates using continuous generation of hydroxyl radicals 有权
标题翻译：使用连续生成羟基自由基改性碳水化合物
公开(公告)号：US08507666B2
公开(公告)日：2013-08-13
申请号：US12862340
申请日：2010-08-24
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C07H1/00 , C07H3/00 , C08B37/00
CPC分类号： D21H19/00 , A23L29/219 , C08B15/00 , C08B31/00 , D21H17/24 , D21H17/25 , D21H17/28 , D21H21/16
摘要： Disclosed herein are methods for modifying carbohydrates using hydroxyl radicals. The hydroxyl radicals may be formed by the photolysis of peroxide in aqueous solution using UV light. Also disclosed are compositions and products comprising carbohydrates modified by the process.
摘要翻译：本文公开了使用羟基自由基来改性碳水化合物的方法。羟基自由基可以通过使用紫外线的水溶液中的过氧化物的光解来形成。还公开了包含通过该方法修饰的碳水化合物的组合物和产品。

3. 发明申请

US20080039615A1 Oxidation of carbohydrate with ultraviolet radiation 有权
标题翻译：用紫外线辐射氧化碳水化合物
公开(公告)号：US20080039615A1
公开(公告)日：2008-02-14
申请号：US11503360
申请日：2006-08-11
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C08B37/06 , C08B37/00 , C08B1/00
CPC分类号： C08B15/02 , C08B31/18 , C08B37/00
摘要： A process for the oxidation of carbohydrate with UV light. The process comprises the steps of providing a carbohydrate, combining the carbohydrate with an oxidant and exposing the combined carbohydrate and oxidant to ultraviolet light. The process occurs at alkaline conditions.
摘要翻译：用UV光氧化碳水化合物的方法。该方法包括提供碳水化合物，将碳水化合物与氧化剂组合并将组合的碳水化合物和氧化剂暴露于紫外光的步骤。该过程发生在碱性条件下。

4. 发明授权

US07057032B2 Low moisture process for extracting hemicellulose 有权
标题翻译：用于提取半纤维素的低水分过程
公开(公告)号：US07057032B2
公开(公告)日：2006-06-06
申请号：US10350610
申请日：2003-01-24
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C08B1/00 , C08B3/28 , C07H1/06 , C07H1/08
CPC分类号： C08B37/0057 , C08B30/10 , C08B37/00 , C08B37/006
摘要： The invention concerns a process for extracting hemicellulose from fiber, such as corn fiber. The process comprises agitating at least fiber, caustic and optional added water at a moisture content from about 10% to about 60% at high speeds in a highly fluidized state. The process substantially instantaneously extracts the hemicellulose from the fiber. Heat may be applied in the process to extract and dry the hemicellulose substantially simultaneously.
摘要翻译：本发明涉及从纤维如玉米纤维中提取半纤维素的方法。该方法包括在高度流化状态下以高速搅拌至少纤维，苛性碱和任选的加入水，其水分含量为约10％至约60％。该方法基本上瞬间从纤维中提取半纤维素。可以在该过程中施加热量以基本上同时提取和干燥半纤维素。

5. 发明授权

US10526627B2 Method for producing high molecular weight reduced viscosity starch pastes 有权
公开(公告)号：US10526627B2
公开(公告)日：2020-01-07
申请号：US12323710
申请日：2008-11-26
申请人： Roman Skuratowicz , Mathew Rice , Aaren Stubberfield , Philip Strong
发明人： Roman Skuratowicz , Mathew Rice , Aaren Stubberfield , Philip Strong
IPC分类号： C12P19/14
摘要： Disclosed herein are methods of making high molecular weight, reduced viscosity starch pastes by enzymatic conversion. The methods provide a process for producing enzyme-thinned starch pastes that have improved molecular weight distributions, i.e., starch pastes having a more mid to high molecular weight content and less low molecular weight sugars than traditional enzyme converted pastes at similar solids and viscosity. In some embodiments, the methods utilize an enzyme capable of producing longer-chain oligosaccharides rather than low-molecular weight sugars. Other embodiments utilize a combination of enzymes to provide low viscosity pastes that are stabilized against setback and retrogradation. Furthermore, the methods may utilize a continuous starch enzyme cooker for the production of the high molecular weight, reduced viscosity starch pastes.

6. 发明申请

US20090142812A1 METHOD FOR PRODUCING HIGH MOLECULAR WEIGHT REDUCED VISCOSITY STARCH PASTES 审中-公开
标题翻译：生产高分子量减少粘度淀粉的方法
公开(公告)号：US20090142812A1
公开(公告)日：2009-06-04
申请号：US12323710
申请日：2008-11-26
申请人： Roman Skuratowicz , Mathew Rice , Aaren Stubberfield , Philip Strong
发明人： Roman Skuratowicz , Mathew Rice , Aaren Stubberfield , Philip Strong
IPC分类号： C12P19/22 , C12P19/00
CPC分类号： C12P19/14
摘要： Disclosed herein are methods of making high molecular weight, reduced viscosity starch pastes by enzymatic conversion. The methods provide a process for producing enzyme-thinned starch pastes that have improved molecular weight distributions, i.e., starch pastes having a more mid to high molecular weight content and less low molecular weight sugars than traditional enzyme converted pastes at similar solids and viscosity. In some embodiments, the methods utilize an enzyme capable of producing longer-chain oligosaccharides rather than low-molecular weight sugars. Other embodiments utilize a combination of enzymes to provide low viscosity pastes that are stabilized against setback and retrogradation. Furthermore, the methods may utilize a continuous starch enzyme cooker for the production of the high molecular weight, reduced viscosity starch pastes.
摘要翻译：本文公开了通过酶促转化制备高分子量，比较粘稠的淀粉糊的方法。该方法提供了生产具有改进的分子量分布的酶 - 稀释的淀粉糊的方法，即具有比传统的酶转化的糊状物具有相似的固体和粘度的具有更高的中等分子量和高分子量含量以及更少的低分子量糖的淀粉糊。在一些实施方案中，该方法利用能够产生较长链寡糖而不是低分子量糖的酶。其它实施方案利用酶的组合来提供稳定的抗粘滞性和降解性的低粘度糊状物。此外，该方法可以利用连续的淀粉酶炊具来生产高分子量，粘度较低的淀粉糊。

7. 发明授权

US07101996B2 Process for preparing purified fractions of hemicellulose and cellulose-hemicellulose complexes from alkali treated fiber and products made by the process 有权
$Process for preparing purified fractions of hemicellulose and cellulose-hemicellulose complexes from alkali treated fiber and products made by the process$
标题翻译：由碱处理的纤维和由该方法制成的产品制备半纤维素和纤维素 - 半纤维素复合物的纯化部分的方法
公开(公告)号：US07101996B2
公开(公告)日：2006-09-05
申请号：US10668951
申请日：2003-09-23
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C08B1/00 , C07H1/00 , C07H1/06 , C07H1/08
CPC分类号： C08B37/0057 , C07H1/06 , C07H1/08 , D21C11/0007
摘要： A process for obtaining purified hemicellulose, cellulose and cellulose-hemicellulose complexes comprising the steps of adding alcohol to caustic liquor from alkali extraction of fiber to precipitate the hemicellulose and the simultaneous, or about simultaneous, density separation of hemicellulose from the caustic liquor. The alcohol transforms the soluble high molecular weight hemicellulose into a light precipitate which floats on top of the caustic liquor solution. The caustic liquor can be subjected to a second separation step whereby the insoluble components (e.g. cellulose and cellulose-hemicellulose complexes) can be removed from the caustic liquor.
摘要翻译：一种获得纯化的半纤维素，纤维素和纤维素 - 半纤维素复合物的方法，包括以下步骤：从碱提取纤维向碱液中加入醇，以沉淀半纤维素，以及同时或大致同时从苛性液中密度分离半纤维素。醇将可溶性高分子量半纤维素转化成漂浮在苛性液溶液顶部的轻质沉淀物。苛性液体可以进行第二分离步骤，由此可以从苛性液体中除去不溶性组分（例如纤维素和纤维素 - 半纤维素络合物）。

8. 发明申请

US20050061204A1 FIBER-BASED PRODUCT 失效
标题翻译：基于纤维的产品
公开(公告)号：US20050061204A1
公开(公告)日：2005-03-24
申请号：US10668950
申请日：2003-09-23
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C08B30/10 , C08L5/14 , C09J103/02 , C08L5/00
CPC分类号： C08L5/14 , C08B30/10 , C08L2666/26 , C09J103/02
摘要： Fiber-based products and adhesives comprising the fiber-based products. The fiber-based products comprise carboxymethyl cellulose, carboxymethylated hemicellulose and carboxymethylated starch. The fiber-based product is obtained by simultaneously performing alkali extraction of hydrocolloid from the fiber and carboxymethylation, with a carboxymethylating agent, thereby converting extracted cellulose to carboxymethyl cellulose and also carboxymethylating some extracted hemicellulose, starch, and hemicellulose-cellulose complexes.
摘要翻译：基于纤维的产品和包含纤维基产品的粘合剂。纤维制品包括羧甲基纤维素，羧甲基化半纤维素和羧甲基淀粉。通过同时从纤维中提取水胶体和羧甲基化用羧甲基化试剂获得纤维基产物，由此将提取的纤维素转化成羧甲基纤维素，并将一些提取的半纤维素，淀粉和半纤维素 - 纤维素复合物进行羧甲基化。

9. 发明授权

US06228158B1 Preblended carrier starches for corrugating adhesives 有权
标题翻译：用于波纹粘合剂的预混载体淀粉
公开(公告)号：US06228158B1
公开(公告)日：2001-05-08
申请号：US09293610
申请日：1999-04-16
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C09J10310
CPC分类号： C09J103/02 , B32B3/28 , C08L2666/02 , C08L2666/54 , C09J103/10 , Y10T428/24694
摘要： A dry preblended carrier starch for corrugating adhesive compositions comprising modified starch and a dry alkali, the modified starch being preferably oxidized starch and the dry alkali being sodium metasilicate or trisodium phosphate. The dry preblended carrier starch for corrugating adhesives has improved viscosity stability over time and temperature fluctuations, eliminates the need for added caustic at end use or at the corrugator and does not require additional silicate compounds in the corrugating adhesive.
摘要翻译：一种用于波纹粘合剂组合物的干燥预混合载体淀粉，其包含改性淀粉和干燥碱，所述改性淀粉优选为氧化淀粉，所述干燥碱为偏硅酸钠或磷酸三钠。用于波纹粘合剂的干预混合载体淀粉具有随时间和温度波动改善的粘度稳定性，消除了在最终用途或在波纹机上添加苛性碱的需要，并且在波纹粘合剂中不需要另外的硅酸盐化合物。

10. 发明授权

US07649090B2 Oxidation of carbohydrate with ultraviolet radiation 有权
标题翻译：用紫外线辐射氧化碳水化合物
公开(公告)号：US07649090B2
公开(公告)日：2010-01-19
申请号：US11503360
申请日：2006-08-11
申请人： Roman Skuratowicz
发明人： Roman Skuratowicz
IPC分类号： C07H1/00 , C07H3/00 , C08B37/00 , C08B31/18 , C08B33/08 , C08B35/08
CPC分类号： C08B15/02 , C08B31/18 , C08B37/00
摘要： A process for the oxidation of carbohydrate with UV light. The process comprises the steps of providing a carbohydrate, combining the carbohydrate with an oxidant and exposing the combined carbohydrate and oxidant to ultraviolet light. The process occurs at alkaline conditions.
摘要翻译：用UV光氧化碳水化合物的方法。该方法包括提供碳水化合物，将碳水化合物与氧化剂组合并将组合的碳水化合物和氧化剂暴露于紫外光的步骤。该过程发生在碱性条件下。

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