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1. 发明授权

US09057145B2 Electrodeposition method with analysis of the electrolytic bath by solid phase extraction 有权
标题翻译：电沉积法通过固相萃取法分析电解槽
公开(公告)号：US09057145B2
公开(公告)日：2015-06-16
申请号：US12312940
申请日：2007-12-10
申请人： Jürgen Barthelmes , Robert Rüther , Florence Lagorce-Broc , Olaf Kurtz , Oleg Sprenger , Marta Sainz-Vila , Thomas Moritz , Josef Gaida
发明人： Jürgen Barthelmes , Robert Rüther , Florence Lagorce-Broc , Olaf Kurtz , Oleg Sprenger , Marta Sainz-Vila , Thomas Moritz , Josef Gaida
IPC分类号： C25D21/12 , C25D21/14
CPC分类号： C25D21/12 , C25D21/14
摘要： A method for electrodepositing a metal layer from an electrolytic bath is described, wherein the concentrations of at least two components of the electrolytic bath are monitored by carrying out the following steps: (a) a sample is taken from the electrolytic bath; (b) the sample is supplied to a column for solid phase extraction, which contains a solid sorbent material; (c) the column is subjected to a washing procedure with a first eluent, wherein the at least two components remain on the column, and undesired components are eluted from the column; (d) the at least two components are eluted from the column by a second eluent; (e) the concentrations of the at least two components in the eluate obtained in step (d) are determined without separating the components from each other. In this method the use of poly(divinyl benzene-co-N-vinyl pyrrolidone) for solid phase extraction is particularly advantageous.
摘要翻译：描述了从电解槽中电沉积金属层的方法，其中通过执行以下步骤监测电解槽的至少两种组分的浓度：（a）从电解浴中取出样品; （b）将样品供给固相萃取柱，其中含有固体吸附剂材料; （c）将柱用第一洗脱液进行洗涤程序，其中至少两种组分保留在柱上，不期望的组分从柱中洗脱出来; （d）所述至少两种组分通过第二种洗脱液从所述柱中洗脱出来; （e）在步骤（d）中获得的洗脱液中的至少两种组分的浓度在不将组分彼此分离的情况下测定。在该方法中，使用聚（二乙烯基苯 - 共-N-乙烯基吡咯烷酮）进行固相萃取是特别有利的。

2. 发明申请

US20100059384A1 Electrodeposition method with analysis of the electrolytic bath by solid Phase Extraction 有权
标题翻译：通过固相萃取法分析电解槽的电沉积方法
公开(公告)号：US20100059384A1
公开(公告)日：2010-03-11
申请号：US12312940
申请日：2007-12-10
申请人： Jürgen Barthelmes , Robert Rüther , Florence Lagorce-Broc , Olaf Kurtz , Oleg Sprenger , Marta Sainz-Vila , Thomas Moritz , Josef Gaida
发明人： Jürgen Barthelmes , Robert Rüther , Florence Lagorce-Broc , Olaf Kurtz , Oleg Sprenger , Marta Sainz-Vila , Thomas Moritz , Josef Gaida
IPC分类号： C25D21/12
CPC分类号： C25D21/12 , C25D21/14
摘要： A method for electrodepositing a metal layer from an electrolytic bath is described, wherein the concentrations of at least two components of the electrolytic bath are monitored by carrying out the following steps: (a) a sample is taken from the electrolytic bath; (b) the sample is supplied to a column for solid phase extraction, which contains a solid sorbent material; (c) the column is subjected to a washing procedure with a first eluent, wherein the at least two components remain on the column, and undesired components are eluted from the column; (d) the at least two components are eluted from the column by a second eluent; (e) the concentrations of the at least two components in the eluate obtained in step (d) are determined without separating the components from each other. In this method the use of poly(divinyl benzene-co-N-vinyl pyrrolidone) for solid phase extraction is particularly advantageous.
摘要翻译：描述了从电解槽中电沉积金属层的方法，其中通过执行以下步骤监测电解槽的至少两种组分的浓度：（a）从电解浴中取出样品; （b）将样品供给固相萃取柱，其中含有固体吸附剂材料; （c）将柱用第一洗脱液进行洗涤程序，其中至少两种组分保留在柱上，不期望的组分从柱中洗脱出来; （d）所述至少两种组分通过第二种洗脱液从所述柱中洗脱出来; （e）在步骤（d）中获得的洗脱液中的至少两种组分的浓度在不将组分彼此分离的情况下测定。在该方法中，使用聚（二乙烯基苯 - 共-N-乙烯基吡咯烷酮）进行固相萃取是特别有利的。

3. 发明申请

US20110189481A1 POST-TREATMENT COMPOSITION FOR INCREASING CORROSION RESISTANCE OF METAL AND METAL ALLOY SURFACES 审中-公开
标题翻译：用于提高金属和金属合金表面耐腐蚀性的后处理组合物
公开(公告)号：US20110189481A1
公开(公告)日：2011-08-04
申请号：US13121479
申请日：2009-10-21
申请人： Jürgen Barthelmes , Michael Danker , Olaf Kurtz , Florence Lagorce-Broc , Robert Rüther
发明人： Jürgen Barthelmes , Michael Danker , Olaf Kurtz , Florence Lagorce-Broc , Robert Rüther
IPC分类号： B32B15/04 , H05K1/03 , C09K3/00 , C23F11/173
CPC分类号： C23C18/12 , H05K3/282 , H05K2201/0162 , Y10T428/294 , Y10T428/31663
摘要： The present invention relates to aqueous post-treatment compositions and an immersion and/or electrolytical process using said compositions for corrosion protection of metal and/or metal alloy surfaces. The aqueous post-treatment compositions comprise at least one polysiloxane betaine compound and at least one phosphorus containing compound.
摘要翻译：本发明涉及含水后处理组合物以及使用所述组合物浸渍和/或电解方法以防止金属和/或金属合金表面的腐蚀。含水后处理组合物包含至少一种聚硅氧烷甜菜碱化合物和至少一种含磷化合物。

4. 发明申请

US20110281124A1 SOLUTION AND PROCESS FOR INCREASING THE SOLDERABILITY AND CORROSION RESISTANCE OF A METAL OR METAL ALLOY SURFACE 有权
标题翻译：提高金属或金属合金表面的焊接性和耐腐蚀性的方法和工艺
公开(公告)号：US20110281124A1
公开(公告)日：2011-11-17
申请号：US13143222
申请日：2010-01-13
申请人： Jürgen Barthelmes , Robert Ruether , Olaf Kurtz , Jana Breitfelder
发明人： Jürgen Barthelmes , Robert Ruether , Olaf Kurtz , Jana Breitfelder
IPC分类号： B32B15/04 , B23K1/20 , H05K1/03 , C09D5/00
CPC分类号： C23C22/58 , C23C22/06 , C23C22/74 , C23F11/1676 , C25D5/48 , H01L21/4835 , H05K3/282 , H05K2203/122 , Y10T428/31678
摘要： Described is a new a solution comprising a phosphorous compound and optionally a solderability-enhancing compound and its use in a process for increasing the solderability and corrosion resistance of a metal or metal alloy surface.
摘要翻译：描述了一种新的溶液，其包含磷化合物和任选的可焊性增强化合物及其在增加金属或金属合金表面的可焊性和耐腐蚀性的方法中的用途。

5. 发明授权

US08491713B2 Solution and process for increasing the solderability and corrosion resistance of a metal or metal alloy surface 有权
标题翻译：提高金属或金属合金表面的可焊性和耐腐蚀性的解决方案和工艺
公开(公告)号：US08491713B2
公开(公告)日：2013-07-23
申请号：US13143222
申请日：2010-01-13
申请人： Jürgen Barthelmes , Robert Ruether , Olaf Kurtz , Jana Breitfelder
发明人： Jürgen Barthelmes , Robert Ruether , Olaf Kurtz , Jana Breitfelder
IPC分类号： C23F11/167 , C23C22/74 , C23C22/58 , C23C22/06 , H05K3/28 , C25D5/48
CPC分类号： C23C22/58 , C23C22/06 , C23C22/74 , C23F11/1676 , C25D5/48 , H01L21/4835 , H05K3/282 , H05K2203/122 , Y10T428/31678
摘要： Described is a new a solution comprising a phosphorous compound and optionally a solderability-enhancing compound and its use in a process for increasing the solderability and corrosion resistance of a metal or metal alloy surface.
摘要翻译：描述了一种新的溶液，其包含磷化合物和任选的可焊性增强化合物及其在增加金属或金属合金表面的可焊性和耐腐蚀性的方法中的用途。

6. 发明申请

US20090250379A1 Process for Manufacturing a Microreactor and Its Use as a Reformer 有权
标题翻译：制造微反应器的工艺及其作为改造者的使用
公开(公告)号：US20090250379A1
公开(公告)日：2009-10-08
申请号：US12085302
申请日：2007-02-22
申请人： Olaf Kurtz , Ralph Herber , Christian Madry , Gerd Schäfer
发明人： Olaf Kurtz , Ralph Herber , Christian Madry , Gerd Schäfer
IPC分类号： F01N7/18 , C23F1/04 , B01J35/02 , C10G35/04
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00804 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , Y10T29/49345
摘要： For manufacturing micro-structured reactors with passageways loaded with catalyst using the pre-coat method, a method is provided which comprises the following method steps: a) producing reactor layers having bonding areas as well as passageway areas in which the passageways are formed, b) applying at least one bonding layer onto the reactor layers in the bonding areas, c) loading the reactor layers in the passageway areas with the catalyst and d) bonding the reactor layers, the bonding layer being applied and masked before the reactor layers are loaded with the catalyst. As a result, it is ensured that the efficiency of the catalyst will not be affected during manufacturing. The reactor may be used as a methane and methanol reformer in particular.
摘要翻译：为了制造具有使用预涂层法的装有催化剂的通道的微结构反应器，提供了一种方法，其包括以下方法步骤：a）制备具有结合区域的反应器层以及形成通道的通道区域，b ）在接合区域中将至少一个粘合层施加到反应器层上，c）用催化剂将反应器层装载在通道区域中，以及d）粘结反应器层，在加载反应器层之前施加和掩蔽粘合层与催化剂。结果确保了在制造时不会影响催化剂的效率。反应器特别可用作甲烷和甲醇重整器。

7. 发明申请

US20080217381A1 Method for Bonding Work pieces and Micro-Structured Component 审中-公开
标题翻译：粘结工件和微结构件的方法
公开(公告)号：US20080217381A1
公开(公告)日：2008-09-11
申请号：US11994583
申请日：2006-06-28
申请人： Heinrich Meyer , Olaf Kurtz , Ralph Herber , Chirstian Madry , Johannes Etzkorn , Thomas Vago
发明人： Heinrich Meyer , Olaf Kurtz , Ralph Herber , Chirstian Madry , Johannes Etzkorn , Thomas Vago
IPC分类号： B23K20/16
CPC分类号： B23K20/023 , F28F2260/00 , F28F2260/02 , F28F2275/04
摘要： For forming very strong bond joints suited for manufacturing micro-structured components consisting of plurality of individual layers, a bonding method is proposed by which a bonding arrangement of the work pieces is formed that comprises at least one metallic bonding layer interposed therein between and by which the bonding arrangement is heated to a bonding temperature below the melting temperature of the at least one bonding layer. In accordance with the invention, the at least one bonding layer is deposited using a chemical or electrolytic method.
摘要翻译：为了形成适合于制造由多个单独层组成的微结构部件的非常牢固的接合接头，提出了一种接合方法，通过该接合方法形成工件的接合装置，其包括插入其间的至少一个金属接合层，由此将接合装置加热到低于至少一个接合层的熔融温度的接合温度。根据本发明，使用化学或电解方法沉积至少一个结合层。

8. 发明申请

US20100326713A1 NI-P LAYER SYSTEM AND PROCESS FOR ITS PREPARATION 有权
标题翻译： NI-P层系统及其制备方法
公开(公告)号：US20100326713A1
公开(公告)日：2010-12-30
申请号：US12919664
申请日：2009-03-05
申请人： Juergen Barthelmes , Robert Ruether , Olaf Kurtz , Michael Danker
发明人： Juergen Barthelmes , Robert Ruether , Olaf Kurtz , Michael Danker
IPC分类号： H05K1/09 , B32B15/04 , C25D5/10
CPC分类号： C23C18/44 , C23C28/021 , C23C28/023 , C25D3/48 , C25D3/562 , C25D5/14 , C25F3/16
摘要： The invention relates to a layer system comprising on a substrate, the surface of which has been electropolished, (i) a Ni layer having a thickness ≦3.0 μm, (ii) a Ni—P layer having a thickness ≦1.0 μm, (iii) a Au layer having a thickness ≦1.0 μm.
摘要翻译：本发明涉及一种层系统，其包括在其表面被电解抛光的基底上，（i）具有厚度为n1E的Ni层为3.0μm，（ii）厚度为n1E的Ni-P层为1.0μm，（iii）厚度为n1E的Au层为1.0μm。

9. 发明申请

US20080196875A1 Micro-Structured Cooler and Use Thereof 有权
公开(公告)号：US20080196875A1
公开(公告)日：2008-08-21
申请号：US11995221
申请日：2006-07-12
申请人： Olaf Kurtz , Ralph Herber , Peter Prechtl , Sven Theisen , Markus Hohn
发明人： Olaf Kurtz , Ralph Herber , Peter Prechtl , Sven Theisen , Markus Hohn
IPC分类号： F28F3/08
CPC分类号： H01L23/473 , F28F3/048 , F28F3/086 , F28F3/12 , H01L2924/0002 , H01L2924/00
摘要： For providing a particularly efficient micro-structured cooler intended more specifically for cooling electronic components, it is proposed to proceed in the following manner to build this cooler: providing a stack of at least two metal foils (1) comprising channels (2) for coolant and one base plate (5) adapted to be brought into thermal contact with the electronic component (4) through a thermal contact surface (6), said metal foils (1) and said base plate (5) being joined together so as to form a single piece of material, said channels (2) having a width b ranging from 100 to 350 μm, a depth t ranging from 30 to 150 μm, a mean spacing s ranging from 30 to 300 μm, residual foil thickness r remaining after formation of the channels (2) in the metal foils (1) ranging from 30 to 300 μm and said base plate (5) having a thickness g ranging from 100 to 1,000 μm, said cooler further having at least one splitting chamber (10) traversing the metal foils (1) approximately in the region of the thermal contact surface (6), said chamber communicating with a respective inlet-side end of all or of the selected channels (2) through channel inlet ports, at least one inlet chamber (20) for admission of coolant into the cooler (3), said chamber communicating with the at least one splitting chamber (10), at least one collecting chamber (11) traversing the metal foils (1) and communicating with a respective outlet-side end of all or selected channels (2) through channel outlet ports and at least one outlet chamber (21) for discharging coolant from said cooler (3), said chamber communicating with said at least one collecting chamber (11), the depth of said channels (2) in a channel layer adjacent said base plate (5) being greater than the depth of the channels (2) in a channel layer located in the stack on the side opposite said base plate (5).

10. 发明授权

US08042726B2 Method for bonding work pieces made of stainless steel, nickel or nickel alloys, using a bonding layer consisting of nickel-phosphorous, method for producing a micro-structured component using such method; micro-structured component obtained by such method 有权
标题翻译：使用由镍 - 磷组成的接合层来接合由不锈钢，镍或镍合金制成的工件的方法，使用这种方法制造微结构部件的方法; 通过这种方法获得的微结构组分
公开(公告)号：US08042726B2
公开(公告)日：2011-10-25
申请号：US12307939
申请日：2007-08-02
申请人： Ralph Herber , Olaf Kurtz , Johannes Etzkorn , Christian Madry , Carsten Schwiekendick , Gerd Schafer
发明人： Ralph Herber , Olaf Kurtz , Johannes Etzkorn , Christian Madry , Carsten Schwiekendick , Gerd Schafer
IPC分类号： B23K31/02 , B23K35/24
CPC分类号： B23K20/233 , B23K20/023 , B23K20/227 , B23K2101/045 , B23K2101/14 , B23K2101/185 , B23K2103/05 , B23K2103/26 , B81C3/001 , B81C2203/035 , F28D9/00 , F28F2260/02 , Y10T428/12646
摘要： To form high performance bonding connections suitable for producing micro-structured components made of a plurality of individual layers, bonding by the steps; providing at least two work pieces; forming a metal bonding layer on at least one side of at least one of said at least two work pieces by chemical or electrolytic metal plating method; the metal bonding layer being a nickel/phosphorous alloy having a prescribed phosphorous content and prescribed thickness; forming a bonding arrangement comprising said work pieces so that there is at least one metal bonding layer between said at least two respective work pieces; heating at a prescribed heating rate to a temperature above the melting temperature of the bonding layer; bonding the two work pieces by applying contact pressure within a prescribed range; and cooling at a prescribed rate.
摘要翻译：为了形成适于生产由多个单独层制成的微结构部件的高性能接合连接，通过该步骤进行接合; 提供至少两个工件; 通过化学或电解金属电镀方法在所述至少两个工件中的至少一个的至少一侧上形成金属粘合层; 金属接合层是具有规定的磷含量和规定厚度的镍/磷合金; 形成包括所述工件的接合装置，使得在所述至少两个相应的工件之间存在至少一个金属结合层; 以规定的加热速度加热到高于接合层的熔融温度的温度; 通过施加规定范围内的接触压力来接合两个工件; 并以规定的速度冷却。

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