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1. 发明申请

US20120310003A1 METHOD FOR PRODUCING CYANOALKENYLCYCLOPROPANECARBOXYLIC ACID SALT 审中-公开
标题翻译：生产氰基烷基环戊烷羧酸盐的方法
公开(公告)号：US20120310003A1
公开(公告)日：2012-12-06
申请号：US13577840
申请日：2011-02-10
申请人： Ichiro Komoto , Toshio Somyo , Masaji Hirota
发明人： Ichiro Komoto , Toshio Somyo , Masaji Hirota
IPC分类号： C07C253/30 , C07C255/31
CPC分类号： C07C253/34 , C07B2200/09 , C07C211/07 , C07C211/35 , C07C253/30 , C07C255/31 , C07C2601/02 , C07C2601/08 , C07C2601/14
摘要： A method for producing a salt of an amine with a cyanoalkenylcyclopropanecarboxylic acid, the method comprising a first step of mixing a carboxylic acid compound represented by formula (2C) and at least one amine selected from the group consisting of primary amines and secondary amines in an organic solvent; a second step of depositing a salt of the amine with a cyanoalkenylcyclopropanecarboxylic acid represented by formula (2) from the mixture obtained in the first step; and a third step of recovering the salt deposited in the second step; wherein, R represents an alkyl group optionally having a substituent or a halogen atom.
摘要翻译：一种用氰基链烯基环丙烷羧酸生产胺盐的方法，该方法包括将式（2C）表示的羧酸化合物与选自伯胺和仲胺中的至少一种胺混合的第一步骤有机溶剂; 第二步是用第一步得到的混合物用式（2）表示的氰基烯基环丙烷羧酸沉淀胺的盐; 以及回收在第二步骤中沉积的盐的第三步骤; 其中，R表示任选具有取代基的烷基或卤素原子。

2. 发明申请

US20110295035A1 METHOD FOR PRODUCING PHENYLACETAMIDE COMPOUND 有权
标题翻译：生产苯乙烯胺化合物的方法
公开(公告)号：US20110295035A1
公开(公告)日：2011-12-01
申请号：US13147823
申请日：2010-02-12
申请人： Hajime Ishida , Masaji Hirota , Yoko Miyanaga , Yuya Mizushima
发明人： Hajime Ishida , Masaji Hirota , Yoko Miyanaga , Yuya Mizushima
IPC分类号： C07C231/06 , C07C235/34
CPC分类号： C07C231/06 , C07C235/34
摘要： A method for producing a phenylacetamide compound represented by formula (1): wherein Q represents a hydrogen atom or a halogen atom, R2 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, R4 represents an alkyl group having 1 to 4 carbon atoms, Ar represents an unsubstituted or substituted phenyl group, R5 represents R4 when R2 is a hydrogen atom, and R5 represents a hydrogen atom when R2 is an alkyl group having 1 to 4 carbon atoms; including reacting a phenylacetamide compound represented by formula (2): wherein Q, R2 and Ar have the same meanings as defined above; with a dialkyl sulfate represented by formula (3): wherein R4 has the same meaning as defined above; in the presence of a base.
摘要翻译：一种由式（1）表示的苯乙酰胺化合物的制备方法：其中Q表示氢原子或卤素原子，R2表示氢原子或碳原子数1〜4的烷基，R4表示1〜4的烷基碳原子，Ar表示未取代或取代的苯基，当R2表示氢原子时，R5表示R4，R2表示碳原子数1〜4的烷基时，R5表示氢原子。包括使由式（2）表示的苯乙酰胺化合物反应：其中Q，R 2和Ar具有与上述相同的含义; 与式（3）表示的二烷基硫酸盐：其中R4具有与上述相同的含义; 在一个基地的存在。

3. 发明申请

US20070078273A1 Process for preparing 5-methyl-2-furfural 审中-公开
标题翻译：制备5-甲基-2-糠醛的方法
公开(公告)号：US20070078273A1
公开(公告)日：2007-04-05
申请号：US11528565
申请日：2006-09-28
申请人： Masaji Hirota
发明人： Masaji Hirota
IPC分类号： C07D307/02
CPC分类号： C07D307/48
摘要： A process for preparing 5-methyl-2-furfural in a high yield by reacting 2-methylfuran, phosgene and N,N-dimethylformamide in a reaction medium comprising a hydrocarbon at a temperature of at least 45° C. and hydrolyzing a reaction mixture.
摘要翻译：通过使2-甲基呋喃，光气和N，N-二甲基甲酰胺在包含烃的反应介质中在至少45℃的温度下反应并水解反应混合物，以高产率制备5-甲基-2-糠醛的方法。

4. 发明申请

US20140221695A1 METHOD FOR PRODUCING 2-(ARYLOXYMETHYL) BENZALDEHYDE COMPOUND 有权
标题翻译： 2-（芳基甲基）苯甲醛化合物的制备方法
公开(公告)号：US20140221695A1
公开(公告)日：2014-08-07
申请号：US14129186
申请日：2012-06-27
申请人： Masaji Hirota , Masashi Takimoto , Tomonori Yamaoka , Yoshio Onogawa
发明人： Masaji Hirota , Masashi Takimoto , Tomonori Yamaoka , Yoshio Onogawa
IPC分类号： C07C45/43
CPC分类号： C07C45/43 , C07C47/575
摘要： A new process capable of producing a 2-(aryloxymethyl)benzaldehyde compound is provided. More particularly, a process for producing a 2-(aryloxymethyl)benzaldehyde compound represented by formula (2) comprising a step of hydrolyzing a compound represented by following formula (1); wherein X1 and X2 each represent independently a chlorine atom, a bromine atom or an iodine atom, Q1, Q2, Q3 and Q4 each represent independently a hydrogen atom or a halogen atom, and Ar represents a phenyl group optionally having a substituent.
摘要翻译：提供了能够生产2-（芳氧基甲基）苯甲醛化合物的新方法。更具体地说，涉及制备由式（2）表示的2-（芳氧基甲基）苯甲醛化合物的方法，包括水解由下式（1）表示的化合物的步骤; 其中X1和X2各自独立地表示氯原子，溴原子或碘原子，Q1，Q2，Q3和Q4各自独立地表示氢原子或卤素原子，Ar表示任选具有取代基的苯基。

5. 发明授权

US08338625B2 Process for production of benzaldehyde compound 有权
标题翻译：苯甲醛化合物生产工艺
公开(公告)号：US08338625B2
公开(公告)日：2012-12-25
申请号：US12997900
申请日：2009-06-09
申请人： Yoshio Onogawa , Kazuyoshi Yamanaka , Masaji Hirota
发明人： Yoshio Onogawa , Kazuyoshi Yamanaka , Masaji Hirota
IPC分类号： C07D317/18
CPC分类号： C07C41/16 , C07C45/52 , C07D317/18 , C07C43/225 , C07C47/575
摘要： A method of producing a corresponding acetal compound which comprises reacting a benzal halide compound represented by formula (1) (wherein, Q represents a hydrogen atom or a halogen atom, X represents a halogen atom, and Ar represents a phenyl group optionally substituted with at least one group selected from the group consisting of alkyl groups having 1 to 4 carbon atoms and halogen atoms.) and an alcohol compound in the presence of at least one alkaline earth metal compound selected from the group consisting of alkaline earth metal oxides, alkaline earth metal hydroxides and alkaline earth metal carbonates.
摘要翻译：一种制备相应的缩醛化合物的方法，其包括使式（1）表示的亚苄基卤化合物（其中，Q表示氢原子或卤素原子，X表示卤素原子，Ar表示任选被至少一个选自具有1-4个碳原子的烷基和卤素原子的基团）和醇化合物在至少一种碱土金属化合物存在下，选自碱土金属氧化物，碱土金属金属氢氧化物和碱土金属碳酸盐。

6. 发明申请

US20110098489A1 PROCESS FOR PRODUCTION OF BENZALDEHYDE COMPOUND 有权
标题翻译：生产苯甲醛的方法
公开(公告)号：US20110098489A1
公开(公告)日：2011-04-28
申请号：US12997900
申请日：2009-06-09
申请人： Yoshio Onogawa , Kazuyoshi Yamanaka , Masaji Hirota
发明人： Yoshio Onogawa , Kazuyoshi Yamanaka , Masaji Hirota
IPC分类号： C07C45/00 , C07D317/22 , C07C41/52
CPC分类号： C07C41/16 , C07C45/52 , C07D317/18 , C07C43/225 , C07C47/575
摘要： A method of producing a corresponding acetal compound which comprises reacting a benzal halide compound represented by formula (1) (wherein, Q represents a hydrogen atom or a halogen atom, X represents a halogen atom, and Ar represents a phenyl group optionally substituted with at least one group selected from the group consisting of alkyl groups having 1 to 4 carbon atoms and halogen atoms.) and an alcohol compound in the presence of at least one alkaline earth metal compound selected from the group consisting of alkaline earth metal oxides, alkaline earth metal hydroxides and alkaline earth metal carbonates.
摘要翻译：一种制备相应的缩醛化合物的方法，其包括使式（1）表示的亚苄基卤化合物（其中，Q表示氢原子或卤素原子，X表示卤素原子，Ar表示任选被至少一个选自具有1-4个碳原子的烷基和卤素原子的基团）和醇化合物在至少一种碱土金属化合物存在下，选自碱土金属氧化物，碱土金属金属氢氧化物和碱土金属碳酸盐。

7. 发明授权

US07491845B2 Process for producing adipic acid 失效
标题翻译：己二酸生产方法
公开(公告)号：US07491845B2
公开(公告)日：2009-02-17
申请号：US11596455
申请日：2004-05-18
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： C07C55/00
CPC分类号： C07C51/313 , B01J23/30 , C07C51/487 , C07C55/14
摘要： It is provided to a process for producing adipic acid which comprises making a wastewater containing hydroxycaproic acid and discharged from the step of oxidizing cyclohexane with molecular oxygen in a liquid phase react with hydrogen peroxide in the presence of a tungsten catalyst in the pH range of 0 to 6.
摘要翻译：提供了一种生产己二酸的方法，其包括制备含有羟基己酸的废水，并且在氧化环己烷的步骤中与分子氧在液相中与在过氧化氢中反应的步骤在钨催化剂存在下在pH范围为0的条件下与过氧化氢反应到6。

8. 发明授权

US08624062B2 Method for producing phenylacetamide compound 有权
标题翻译：苯乙酰胺化合物的制备方法
公开(公告)号：US08624062B2
公开(公告)日：2014-01-07
申请号：US13147823
申请日：2010-02-12
申请人： Hajime Ishida , Masaji Hirota , Yoko Miyanaga , Yuya Mizushima
发明人： Hajime Ishida , Masaji Hirota , Yoko Miyanaga , Yuya Mizushima
IPC分类号： C07C233/05 , C07C231/06
CPC分类号： C07C231/06 , C07C235/34
摘要： A method for producing a phenylacetamide compound represented by formula (1): wherein Q represents a hydrogen atom or a halogen atom, R2 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, R4 represents an alkyl group having 1 to 4 carbon atoms, Ar represents an unsubstituted or substituted phenyl group, R5 represents R4 when R2 is a hydrogen atom, and R5 represents a hydrogen atom when R2 is an alkyl group having 1 to 4 carbon atoms; including reacting a phenylacetamide compound represented by formula (2): wherein Q, R2 and Ar have the same meanings as defined above; with a dialkyl sulfate represented by formula (3): wherein R4 has the same meaning as defined above; in the presence of a base.
摘要翻译：一种由式（1）表示的苯乙酰胺化合物的制备方法：其中Q表示氢原子或卤素原子，R2表示氢原子或碳原子数1〜4的烷基，R4表示1〜4的烷基碳原子，Ar表示未取代或取代的苯基，当R2表示氢原子时，R5表示R4，R2表示碳原子数1〜4的烷基时，R5表示氢原子。包括使由式（2）表示的苯乙酰胺化合物反应：其中Q，R 2和Ar具有与上述相同的含义; 与式（3）表示的二烷基硫酸盐：其中R4具有与上述相同的含义; 在一个基地的存在。

9. 发明申请

US20120101294A1 PROCESS FOR PRODUCING (FLUOROALKYLTHIO) ACETIC ACID ESTER 审中-公开
标题翻译：生产（氟烷基）乙酸酯的方法
公开(公告)号：US20120101294A1
公开(公告)日：2012-04-26
申请号：US13382121
申请日：2010-08-06
申请人： Masaji Hirota , Hiroyuki Miyazaki , Tadayoshi Itoh
发明人： Masaji Hirota , Hiroyuki Miyazaki , Tadayoshi Itoh
IPC分类号： C07C319/12 , C07C315/02
CPC分类号： C07C319/18 , C07C315/02 , C07C315/04 , C07C319/20 , C07C323/52 , C07C317/44
摘要： Disclosed is a process for producing a (fluoroalkylthio)acetic acid ester represented by the formula (3) wherein R, R1 and R2 have the same meanings as defined below, which comprises reacting a thioglycolic acid ester represented by the formula (1) wherein R represents a hydrogen atom or an alkyl group having 1 to 5 carbon atoms, and R1 represents an alkyl group having 1 to 4 carbon atoms, with fluoroolefin represented by the formula (2) wherein R2 represents a fluoroalkyl group having 1 to 5 carbon atoms, in the presence of a radical generator.
摘要翻译：公开了一种由式（3）表示的（氟烷基硫代）乙酸酯的制备方法，其中R 1，R 2和R 2具有如下定义的相同含义，该方法包括使式（1）表示的巯基乙酸酯与式表示氢原子或碳原子数1〜5的烷基，R1表示碳原子数1〜4的烷基，式（2）表示的氟代烯烃，其中，R2表示碳原子数1〜5的氟代烷基，在自由基发生器的存在下。

10. 发明授权

US07074947B2 Process for producing epoxide compound 失效
标题翻译：环氧化合物的制备方法
公开(公告)号：US07074947B2
公开(公告)日：2006-07-11
申请号：US10501956
申请日：2003-01-31
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： C07D301/12 , B01J31/06
CPC分类号： B01J31/34 , B01J23/28 , B01J23/30 , B01J27/16 , B01J27/22 , B01J31/006 , B01J31/0237 , B01J31/0244 , B01J2231/72 , C07D301/12
摘要： A process for producing an epoxide compound, characterized by reacting an olefin compound with hydrogen peroxide in the presence of: a metal oxide catalyst obtained by reacting hydrogen peroxide with at least one member selected from the group consisting of tungsten metal, molybdenum metal, compounds of tungsten and a Group IIIb, IVb, Vb, or VIb element, tungstic acid and salts thereof, compounds of molybdenum and a Group IIIb, IVb, Vb, or VIb element, and molybodic acid and salts thereof; at least one member selected from the group consisting of tertiary amine compounds, tertiary amine oxide compounds, nitrogenous aromatic compounds, and nitrogenous aromatic N-oxide compounds; and a phosphoric acid compound.
摘要翻译：一种制备环氧化合物的方法，其特征在于使烯烃化合物与过氧化氢在以下存在下反应：金属氧化物催化剂，其通过使过氧化氢与至少一种选自钨金属，钼金属，钨和IIIb，IVb，Vb或VIb族元素，钨酸及其盐，钼和IIIb，IVb，Vb或VIb族元素的化合物，以及钼酸及其盐; 选自叔胺化合物，叔胺氧化物化合物，含氮芳族化合物和含氮芳族N-氧化物化合物中的至少一种; 和磷酸化合物。

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