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1. 发明授权

US4248782A Preparation of .epsilon.-caprolactam by catalytic rearrangement of cyclohexanone-oxime 失效
标题翻译：通过催化重排环己酮 - 肟制备ε-己内酰胺
公开(公告)号：US4248782A
公开(公告)日：1981-02-03
申请号：US78031
申请日：1979-09-24
申请人： Hugo Fuchs , Uwe Brand , Peter Horn
发明人： Hugo Fuchs , Uwe Brand , Peter Horn
IPC分类号： C07D201/04
CPC分类号： C07D201/04 , Y02P20/52
摘要： In a process for the preparation of .epsilon.-caprolactam by catalytic rearrangement of cyclohexanone-oxime in the gas phase at from 230.degree. to 450.degree. C. over a supported catalyst, containing boron trioxide, in a fluidized bed, wherein the catalyst is removed from the fluidized bed at the rate at which it becomes spent and is treated, in a fluidized state, with gases containing molecular oxygen at from 600.degree. to 900.degree. C., after which boron trioxide or boric acid is added to the fluidized catalyst, at from 300.degree. to 900.degree. C., before the catalyst is returned to the fluidized bed, the improvement that boron trioxide or boric acid of particle size from 0.05 to 1.5 mm is fed to the fluidized catalyst at one or more points.
摘要翻译：在通过在230℃至450℃的气相中催化重排环己酮 - 肟在含有三氧化硼的载体催化剂的流化床中制备ε-己内酰胺的方法，其中将催化剂从流化床以其流失的速率以流化状态处理含有分子氧的气体在600-900℃，之后将三氧化硼或硼酸加入到流化催化剂中，在在催化剂返回到流化床之前，从300℃升至900℃，改善将粒径为0.05-1.5mm的三氧化硼或硼酸以一个或多个点进料到流化催化剂中。

2. 发明授权

US4257950A Continuous preparation of .epsilon.-caprolactam by Beckmann rearrangement 失效
标题翻译：通过贝克曼重排连续制备ε-己内酰胺
公开(公告)号：US4257950A
公开(公告)日：1981-03-24
申请号：US79329
申请日：1979-09-27
申请人： Peter Horn , Otto-Alfred Grosskinsky , Richard Thoma , Hugo Fuchs
发明人： Peter Horn , Otto-Alfred Grosskinsky , Richard Thoma , Hugo Fuchs
IPC分类号： C07D201/04
CPC分类号： C07D201/04
摘要： A process for the continuous preparation of .epsilon.-caprolactam by Beckmann rearrangement of cyclohexanone-oxime, dissolved in a solvent which is inert toward oleum and is immiscible with oleum and water, at an elevated temperature, with removal of the heat of rearrangement by evaporation of the solvent, wherein oleum containing caprolactam is circulated successively through a conveying zone, a mixing zone, a boiling zone and a separating zone, upstream of the conveying zone oleum is added at the rate at which it is consumed, in the mixing zone cyclohexanone-oxime dissolved in solvent is added under turbulent conditions, in the boiling zone the heat of rearrangement is removed in a conventional manner by evaporating the solvent and recycling the condensate, and in the separating zone the reaction mixture is separated into a solvent phase, from which solvent is withdrawn at the rate at which the phase is formed, and a caprolactam-containing oleum phase, which is removed at the rate at which it is formed.
摘要翻译：通过贝克曼重排环己酮 - 肟连续制备ε-己内酰胺的方法，该方法在升高的温度下溶解在对发烟硫酸是惰性的且与发烟硫酸和水不混溶的溶剂中，通过蒸发除去重排热将其中含有发烟硫酸的己内酰胺在输送区上游的输送区，混合区，沸点区和分离区连续循环的溶剂以其消耗的速率在混合区中加入环己酮 - 在湍流条件下加入溶解在溶剂中的肟，在沸腾区中，以常规方式通过蒸发溶剂并再循环冷凝物来除去重排热，并且在分离区中将反应混合物分离成溶剂相，从其中溶剂以形成相的速率被抽出，含己内酰胺的发烟硫酸相以它是形成的。

3. 发明授权

US4248781A Purification of crude caprolactam 失效
标题翻译：粗己内酰胺的纯化
公开(公告)号：US4248781A
公开(公告)日：1981-02-03
申请号：US78028
申请日：1979-09-24
申请人： Peter Horn , Hugo Fuchs
发明人： Peter Horn , Hugo Fuchs
IPC分类号： C07D201/16
CPC分类号： C07D201/16
摘要： A process for purifying crude caprolactam which has been obtained by rearrangement of cyclohexanone-oxime in the gas phase over a catalyst containing boron trioxide, wherein caprolactam is crystallized out, by cooling, from a melt which contains, per 100 parts by weight of crude caprolactam, from 5 to 30 parts by weight of primary alkanols or fatty acids which have a carbon chain of 6 to 10 carbon atoms and are substituted by alkyl radicals of 1 to 5 carbon atoms, and from 0 to 5 parts by weight of water, and is separated from the mother liquor.
摘要翻译：一种纯化己内酰胺纯化方法，该方法是通过在含有三氧化硼的催化剂上，在气相中重排环己酮 - 肟而得到的，其中己内酰胺通过冷却从含有每100份重量的己内酰胺，5〜30重量份具有碳原子数为6〜10个碳原子并且被1〜5个碳原子的烷基取代的伯烷醇或脂肪酸，0〜5重量份的水，以及与母液分离。

4. 发明授权

US4178317A Manufacture of olefinically unsaturated aliphatic or cycloaliphatic hydrocarbons 失效
标题翻译：制备烯属不饱和脂肪族或脂环族烃
公开(公告)号：US4178317A
公开(公告)日：1979-12-11
申请号：US907678
申请日：1978-05-19
申请人： Peter Horn , Otto-Alfred Grosskinsky , Hugo Fuchs
发明人： Peter Horn , Otto-Alfred Grosskinsky , Hugo Fuchs
IPC分类号： C07C1/20 , B01J23/00 , B01J27/00 , C07B61/00 , C07C1/00 , C07C1/207 , C07C1/213 , C07C11/02 , C07C67/00 , C07C3/00
CPC分类号： C07C1/213 , C07C1/2078 , C07C2101/10 , C07C2101/16 , C07C2521/02 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2523/14 , C07C2527/24 , Y02P20/582
摘要： Olefinically unsaturated aliphatic or cycloaliphatic hydrocarbons are manufactured by bringing alkanecarboxylic acids of 3 to 20 carbon atoms, alkanedicarboxylic acids of 4 to 20 carbon atoms or 5-membered or 6-membered cycloalkanecarboxylic acids or their alkyl, cycloalkyl, aralkyl or phenyl esters, in the gas phase, at from 250.degree. to 800.degree. C., into contact with catalysts in which the active composition consists of boron trioxide, boric acid and/or boron nitride, together with one or more of the oxides of aluminum, silicon, tin, lead, titanium and zirconium.
摘要翻译：通过使3-20个碳原子的链烷羧酸，4-20个碳原子的链烷二羧酸或五元或6-元环烷烃羧酸或它们的烷基，环烷基，芳烷基或苯基酯引入到烯属不饱和脂族或脂环族烃中气相在250℃至800℃下与催化剂接触，其中活性组合物由三氧化硼，硼酸和/或氮化硼组成，以及一种或多种铝，硅，锡，铅，钛和锆。

5. 发明申请

US20060163923A1 Child seat 审中-公开
标题翻译：儿童座椅
公开(公告)号：US20060163923A1
公开(公告)日：2006-07-27
申请号：US10532759
申请日：2003-10-02
申请人： Karl-Heinz Baumann , Michael Fehring , Peter Horn , Rainer Justen
发明人： Karl-Heinz Baumann , Michael Fehring , Peter Horn , Rainer Justen
IPC分类号： A47D1/10
CPC分类号： B60N2/2812 , B60N2/2806 , B60N2/286 , B60N2/2884 , B60N2/2887 , B60R22/1951
摘要： The invention relates to a child seat (1) which can be fastened to a vehicle seat of a motor vehicle by means of a three-point seat belt (14). It is also possible for the child seat also to be connected to the supporting structure of the vehicle via an ISOFIX fastening system (17). The three-point seat belt (14) is equipped with a tightening device. The child seat (1) has its own belt system for securing a child sitting on the child seat. According to the invention, it is proposed that the three-point seat belt (14) be coupled to the belt system of the child seat (1). This coupling makes it possible, during a preventative or crash-active tightening of the three-point seat belt (14), for the belt system of the child seat (1) also to be tightened without a separate tightening device being necessary.
摘要翻译：本发明涉及一种可通过三点式安全带（14）固定在机动车辆的车辆座椅上的儿童座椅（1）。儿童座椅还可以经由ISOFIX紧固系统（17）连接到车辆的支撑结构。三点式安全带（14）配有紧固装置。儿童座椅（1）具有自己的皮带系统，用于固定坐在儿童座椅上的儿童。根据本发明，提出三点式安全带（14）与儿童座椅（1）的皮带系统联接。这种联接使得在三点式安全带（14）的预防或紧急主动紧固期间，也可以在不需要单独的紧固装置的情况下使儿童座椅（1）的皮带系统被紧固。

6. 发明授权

US5760099A Production of rigid or semirigid polyurethane foams and composite elements comprising such polyurethane foams 失效
标题翻译：制备刚性或半刚性聚氨酯泡沫和包含这种聚氨酯泡沫的复合元件
公开(公告)号：US5760099A
公开(公告)日：1998-06-02
申请号：US711452
申请日：1996-09-06
申请人： Peter Horn , Gerhard Lehr , Sarbananda Chakrabarti , Dieter Hertel , Ludwig Jung
发明人： Peter Horn , Gerhard Lehr , Sarbananda Chakrabarti , Dieter Hertel , Ludwig Jung
IPC分类号： C08J9/02 , B32B27/30 , B32B27/40 , C08G18/00 , C08G18/08 , C08G18/40 , C08J9/00 , C08J9/14 , C08L75/00 , C08J9/06
CPC分类号： C08J9/0061 , C08J9/0033 , C08J9/0038 , C08J2375/04 , C08J2471/00
摘要： Rigid polyurethane foams, preferably semirigid polyurethane foams, are produced by reacting an organic and/or modified organic polyisocyanates with relatively high molecular weight polyhydroxyl compounds and, optionally, low molecular weight chain extenders and/or crosslinkers in the presence of water or mixtures of water and physically acting blowing agents, optionally, catalysts, at least one additive selected from the group consisting of sulfonate salts of an acid group-containing alkylene oxide polymer, a phosphonate salt of an acid group-containing alkylene oxide polymer, and mixtures thereof, additional other additives and optionally, auxiliaries. The polyurethane foams produced by this process can be used to produce composite comprising at least one covering layer and at least one layer comprising a rigid or semirigid polyurethane foam produced by the process of the present invention.
摘要翻译：刚性聚氨酯泡沫，优选半刚性聚氨酯泡沫，通过有机和/或改性的有机多异氰酸酯与相对高分子量的多羟基化合物和任选的低分子量增链剂和/或交联剂在水或水的混合物和物理作用的发泡剂，任选的催化剂，至少一种选自含酸基的烯化氧聚合物的磺酸盐，含酸基的烯化氧聚合物的膦酸盐及其混合物的添加剂，另外其他添加剂和任选的助剂。通过该方法生产的聚氨酯泡沫可用于生产包含至少一个覆盖层和至少一层包含通过本发明方法制备的刚性或半刚性聚氨酯泡沫的层的复合材料。

7. 发明授权

US5334620A Production of chlorofluorocarbon-free, urethane-containing moldings having a cellular core and a compacted peripheral zone 失效
标题翻译：生产不含氟碳的含氨基甲酸酯的模制品，其具有多孔芯和压实的周边区
公开(公告)号：US5334620A
公开(公告)日：1994-08-02
申请号：US896295
申请日：1992-06-10
申请人： Peter Horn , Ulrich Mueller , Wolfgang Hoelderich , Ulf Sattler , Rudolf Taddey , Dieter Tintelnot
发明人： Peter Horn , Ulrich Mueller , Wolfgang Hoelderich , Ulf Sattler , Rudolf Taddey , Dieter Tintelnot
IPC分类号： C08J9/00 , C08J9/34 , C08J9/08 , C08J9/12 , C08K3/36
CPC分类号： C08J9/34 , C08J9/0066 , C08J2375/04
摘要： A process for the production of fluorochlorocarbon-free, urethane-containing, soft-elastic, semirigid or rigid moldings having a cellular core and a compacted peripheral zone and an essentially pore-free, smooth surface involves reactinga) an organic and/or modified organic polyisocyanate withb) at least one relatively high-molecular-weight compound containing at least two reactive hydrogen atoms, and, if desired,c) a low-molecular-weight chain extender and/or cross-linking agent,in the presence ofd) a blowing agent,e) a catalyst,f) at least one amorphous, microporous silica gel which preferably has a mean pore diameter with a frequency of occurrence of more than 40% in the range from 0.1 to 10 nm, a pore volume of from 0.15 to 1.8 ml/g and a BET surface area of from 200 to 900 m.sup.2 /g, and, if desired, further additives andg) assistants,in a closed mold with compaction.
摘要翻译：一种生产含氟氯碳化合物，含氨基甲酸酯的软弹性半刚性或刚性模制品的方法，其具有多孔芯和压实的周边区域以及基本上无孔的光滑表面包括使a）有机和/或改性的有机多异氰酸酯，b）至少一种含有至少两个反应性氢原子的相对高分子量化合物，如果需要，c）低分子量增链剂和/或交联剂，在 d）发泡剂，e）催化剂，f）至少一种无定形微孔硅胶，其优选具有在0.1-10nm范围内发生频率大于40％的平均孔径，孔体积为0.15至1.8ml / g，BET表面积为200至900m2 / g，如果需要，还有添加剂和g）辅助剂，在密闭模具中进行压实。

8. 发明授权

US5182354A Transparent, compact polyurethane casting compositions that are sterilizable with superheated steam, process for preparing same, and their use, particularly for medical-technical articles 失效
标题翻译：透明，紧凑的聚氨酯涂料组合物，其不可用超级蒸汽消毒，其制备方法及其使用，特别是医疗技术文章
公开(公告)号：US5182354A
公开(公告)日：1993-01-26
申请号：US507694
申请日：1990-05-07
申请人： Peter Horn , Walter Heckmann , Falko Ramsteiner , Friedrich Gerold
发明人： Peter Horn , Walter Heckmann , Falko Ramsteiner , Friedrich Gerold
IPC分类号： A61L27/00 , A61L27/34 , A61L27/48 , A61L29/00 , A61L31/00 , B01D63/02 , C08G18/10 , C08G18/30 , C08G18/32 , C08G18/48 , C08G18/72 , C08G18/76
CPC分类号： C08G18/7671 , A61L27/34 , A61L27/48 , B01D63/023 , C08G18/10 , C08G18/4829
摘要： The invention relates to transparent, substantially compact polyurethane casting compositions, sterilizable with superheated steam, which are prepared by the reaction of:A) modified diphenylmethane diisocyanates (A) that are liquid at 23.degree. C. and are in turn are obtained by the reaction of1) a diphenylmethane diisocyanate isomer mixture, which in terms of 100 parts by weight comprises 60 to 90 parts by weight of 4,4'-diphenylmethane diisocyanate, 40 to 8 parts by weight of 2,4'-diphenylmethane diisocyanate, and 0 to 5 parts by weight of 2,2'-diphenylmethane diisocyanate with2) at least one polyoxypropylene polyol initiated with glycerine and/or trimethylol propane, having a molecular weight of 350 to 800 with a ratio of NCO:OH groups of 2.5:1 to 15:1, withB) at least one compound having at least two reactive hydrogen atoms in the presence or absence ofC) catalysts,as well as to a process for preparing the polyurethane casting compounds and their use for medical-technical articles.
摘要翻译：本发明涉及透明的，基本上紧凑的聚氨酯流延组合物，其可用过热蒸汽灭菌，其通过以下反应制备：A）在23℃下为液体的改性二苯甲烷二异氰酸酯（A），其又通过反应获得的1）二苯基甲烷二异氰酸酯异构体混合物，其以100重量份计包含60至90重量份的4,4'-二苯基甲烷二异氰酸酯，40至8重量份的2,4'-二苯基甲烷二异氰酸酯和0 至5重量份的2,2'-二苯基甲烷二异氰酸酯与2）至少一种由甘油和/或三羟甲基丙烷引发的聚氧丙烯多元醇，其分子量为350至800，NCO:OH基团的比例为2.5:1 在B存在或不存在下，B）至少一种具有至少两个反应性氢原子的化合物，以及制备聚氨酯浇铸化合物的方法及其在医疗技术领域中的用途 es。

9. 发明授权

US4617225A Sheet-like reinforced material 失效
标题翻译：片状增强材料
公开(公告)号：US4617225A
公开(公告)日：1986-10-14
申请号：US791113
申请日：1985-10-24
申请人： Peter Horn , Edwin Baumann , Matthias Marx , Peter Gerarts
发明人： Peter Horn , Edwin Baumann , Matthias Marx , Peter Gerarts
IPC分类号： B32B5/28 , B32B5/24 , B32B37/10 , B32B38/00 , C08G69/16 , C08J5/24 , B32B3/26 , B32B5/18 , B32B7/04 , B32B27/04
CPC分类号： C08G69/16 , B32B5/24 , Y10T428/24967 , Y10T428/249955 , Y10T428/249981 , Y10T428/249991 , Y10T442/647
摘要： Sheet-like reinforced materials consisting ofA. a core layer comprising a sheet-like textile structure, preferably a glass fiber mat,B. a plastic matrix composed of a nylon which has been polymerized under alkaline conditions and penetrates both the core layer and the surface layer of layers,are produced batchwise by the RIM method or continuously on a double-belt press by impregnating the sheet-line textile structure and the foam sheets with a lactam melt and polymerizing the latter. The reinforced material can be used for the production of finished articles having a satisfactory surface, for example for the automotive or aircraft industry.
摘要翻译：由A组成的片状增强材料，包括片状织物结构的芯层，优选玻璃纤维垫B.由尼龙组成的塑料基质，其在碱性条件下已经聚合并渗透到芯层和通过RIM方法分批生产或在双带压榨机上连续地通过用内酰胺熔体浸渍片状织物结构和泡沫片材并使其聚合而分批生产层。增强材料可以用于生产具有令人满意的表面的成品，例如用于汽车或飞机工业。

10. 发明授权

US4595705A Process for the preparation of optionally cellular polyurethane polyurea molded parts 失效
标题翻译：制备任选细胞聚氨酯聚脲模制件的方法
公开(公告)号：US4595705A
公开(公告)日：1986-06-17
申请号：US700758
申请日：1985-02-13
申请人： Frank Werner , Matthias Marx , Peter Horn , Hans U. Schmidt
发明人： Frank Werner , Matthias Marx , Peter Horn , Hans U. Schmidt
IPC分类号： C08G18/32 , C08G18/40 , C08G18/65 , C08G18/14 , C08G18/30
CPC分类号： C08G18/6529 , C08G18/3221 , C08G18/4009 , C08G18/4018 , C08G2101/0033 , C08G2120/00 , Y10T428/249989
摘要： The invention relates to a one-shot process for the preparation of cellular or noncellular polyurethane polyurea parts having a modulus of flexural elasticity greater than 600 N/mm.sup.2 and densities of from 0.8 to 1.2 g/cm.sup.3 using the reaction injection molding technique, by reacting organic polyisocyanates, a polyol component, aromatic diamines, additional chain extenders and/or cross-linking agents in the presence of catalysts and optionally blowing agents, auxiliaries and/or additives, wherein the polyol component is a mixture containing(i) from 95 to 60 percent by weight of at least one compound selected from the group consisting of polyols, polyether polyamines, polyesteramides, and their mixtures having functionalities of from 2 to 6 and a molecular weight of from 1000 to 8000 and(ii) from 5 to 40 percent by weight of a least one aromatic and/or aromatic-aliphatic polyester polyol having a functionality of from 2 to 3 and a molecular weight of from 254 to 700, wherein the percents by weight are based on the total weight of the polyol component.
摘要翻译：本发明涉及使用反应注射成型技术制备具有大于600N / mm2的弯曲弹性模量和0.8至1.2g / cm 3的密度的细胞或非细胞聚氨酯聚脲部件的一步法，通过使有机多异氰酸酯，多元醇组分，芳族二胺，另外的增链剂和/或交联剂，在催化剂和任选的发泡剂，助剂和/或添加剂的存在下，其中多元醇组分是含有（i）95至 60重量％的至少一种选自多元醇，聚醚多胺，聚酯酰胺及其混合物的至少一种化合物，其官能度为2至6，分子量为1000至8000，（ii）5至40％的至少一种官能度为2至3且分子量为254至700的至少一种芳族和/或芳族 - 脂族聚酯多元醇，其中百分比基于多元醇组分的总重量。

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