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1. 发明授权

US09777089B2 Process, properties, and applications of graft copolymers 有权
公开(公告)号：US09777089B2
公开(公告)日：2017-10-03
申请号：US14971487
申请日：2015-12-16
申请人： Honeywell International Inc. , Centre National de la Recherche Scientifique , Universite de Montpellier
发明人： Alagappan Thenappan , Eric Rainal , Bruno Ameduri , Frederic Boschet , Noureddine Ajellal , Gerald Lopez
IPC分类号： C08F214/24 , C08F259/00 , C08J5/18
CPC分类号： C08F214/24 , C08F259/00 , C08J5/18 , C08J2327/12
摘要： A polymeric molecule having the formula: X—[C(A)2C(B)(B′)]n-Q[CY═C(Z)(Z′)] or [C(A)2=C(B)]n-Q[C(Y)(Y′)—C(Z)(Z′)]—X′, wherein A is either H or F; B and B′ are either H, F, or Cl, and are not necessarily the same; X and X′ are Br, Cl or I (and are not necessarily the same); Y and Y′ are F, Br, Cl or I (and are not necessarily the same); and wherein Z and Z′ are F, Br, Cl or I (and are not necessarily the same); Q is optional and is either oxygen (O) or sulfur (S); and n is at least 1.

2. 发明申请

US20160130379A1 PROCESS, PROPERTIES, AND APPLICATIONS OF GRAFT COPOLYMERS 有权
标题翻译： GRAFT共聚物的工艺，性能和应用
公开(公告)号：US20160130379A1
公开(公告)日：2016-05-12
申请号：US14971487
申请日：2015-12-16
申请人： Honeywell International Inc. , Universite de Montpellier , Centre National de la Recherche Scientifique
发明人： Alagappan Thenappan , Eric Rainal , Bruno Ameduri , Frederic Boschet , Noureddine Ajellal , Gerald Lopez
IPC分类号： C08F214/24
CPC分类号： C08F214/24 , C08F259/00 , C08J5/18 , C08J2327/12
摘要： A polymeric molecule having the formula: X—[C(A)2C(B)(B′)]n-Q[CY═C(Z)(Z′)] or [C(A)2=C(B)]n-Q[C(Y)(Y′)—C(Z)(Z′)]—X′, wherein A is either H or F; B and B′ are either H, F, or Cl, and are not necessarily the same; X and X′ are Br, Cl or I (and are not necessarily the same); Y and Y′ are F, Br, Cl or I (and are not necessarily the same); and wherein Z and Z′ are F, Br, Cl or I (and are not necessarily the same); Q is optional and is either oxygen (O) or sulfur (S); and n is at least 1.
摘要翻译：具有下式的聚合物分子：X- [C（A）2C（B）（B'）] nQ [CY = C（Z）（Z'）]或[C（A）2 = C（B） [C（Y）（Y'）-C（Z）（Z'）] - X'，其中A为H或F; B和B'是H，F或Cl，并不一定相同; X和X'是Br，Cl或I（并不一定相同）; Y和Y'是F，Br，Cl或I（并不一定相同）; 并且其中Z和Z'是F，Br，Cl或I（并且不一定相同）; Q是任选的，并且是氧（O）或硫（S）; 且n至少为1。

3. 发明授权

US09969899B2 Fluoropolymers containing a copolymerized fluoromonomer and a functional hydrocarbon comonomer and articles made from such fluoropolymers 有权
公开(公告)号：US09969899B2
公开(公告)日：2018-05-15
申请号：US14177784
申请日：2014-02-11
申请人： Honeywell International Inc. , Centre National De La Recherche Scientifique
发明人： Alagappan Thenappan , Bruno Ameduri , Gerald Lopez , Eric Rainal , Noureddine Ajellal , Gary Martin
IPC分类号： C09D127/12 , B32B27/08 , C08J7/04 , B32B27/30 , B32B27/32 , B32B27/36 , C08F214/18 , C08J5/18
CPC分类号： C09D127/12 , B32B27/08 , B32B27/304 , B32B27/308 , B32B27/322 , B32B27/36 , B32B2307/412 , B32B2307/714 , B32B2307/7265 , B32B2439/00 , B32B2439/80 , B32B2581/00 , B32B2597/00 , C08F214/18 , C08J5/18 , C08J7/047 , C08J2327/06 , C08J2327/12 , C08J2367/02 , C08J2379/08 , C08J2427/04 , C08J2427/12 , Y10T428/31507 , Y10T428/31544
摘要： Disclosed is a copolymer film that includes a first comonomer including a chlorofluoro olefin and a second comonomer that is selected from the group consisting of itaconic acid, 2,3-dihydropyran, D-glucal, glycerine carbonate vinyl ether, 2-hydroxypropyl acrylate, maleic anhydride, vinylidene chloride, and mixtures thereof.

4. 发明申请

US20150094428A1 SYNTHESIS OF CHLOROTRIFLUOROETHYLENE-BASED BLOCK COPOLYMERS BY IODINE TRANSFER POLYMERIZATION 有权
标题翻译：通过碘转移聚合合成基于氯代三氟乙烯的嵌段共聚物
公开(公告)号：US20150094428A1
公开(公告)日：2015-04-02
申请号：US14448062
申请日：2014-07-31
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Bruno Ameduri , Gerald Lopez
IPC分类号： C08F299/00
CPC分类号： C08F214/242 , C08F2/38 , C08F214/24 , C08F293/005 , C08F2438/00
摘要： Methods for the synthesis of CTFE-based block copolymers through iodine transfer polymerization are disclosed. In an exemplary embodiment, a method includes reacting a fluoromonomer “M” with a chain transfer agent of the formula X—Y or Y—X—Y, wherein X represents a C1-C3 hydrocarbon, a C1-C6 hydrofluorocarbon, C1-C6 hydrochlorofluorocarbon, or C1-C6 fluorocarbon and Y represents iodine or bromine, in the presence of a radical initiator, to form a macro-initiator of the formula: X-poly(M)-Y or Y-poly(M)-X-poly(M)-Y, wherein poly(M) represents a polymer of the fluoromonomer. The method further includes reacting the macro-initiator with chlorotrifluoroethylene (CTFE) in the presence of a radical initiator to form a diblock or a triblock CTFE-based block copolymer of the formula: X-poly(M)-block-poly(CTFE) or PCTFE-block-poly(M)-X-poly(M)-block-PCTFE.
摘要翻译：公开了通过碘转移聚合合成CTFE基嵌段共聚物的方法。在一个示例性实施方案中，一种方法包括使含氟单体“M”与式X-Y或Y-X-Y的链转移剂反应，其中X表示C1-C3烃，C1-C6氢氟烃，C1-C6 氯代氟代烃或C1-C6碳氟化合物，Y代表碘或溴，在自由基引发剂的存在下形成下式的大分子引发剂：X-聚（M）-Y或Y-聚（M）-X- 聚（M）-Y，其中聚（M）表示所述含氟单体的聚合物。该方法还包括在自由基引发剂的存在下使大分子引发剂与氯三氟乙烯（CTFE）反应以形成下式的二嵌段或三嵌段CTFE基嵌段共聚物：X-聚（M） - 嵌段 - 聚（CTFE）或PCTFE-嵌段 - 聚（M）-X-聚（M） - 嵌段-PCFEFE。

5. 发明授权

US09394394B2 Synthesis of chlorotrifluoroethylene-based block copolymers by iodine transfer polymerization 有权
标题翻译：通过碘转移聚合合成三氟氯乙烯基嵌段共聚物
公开(公告)号：US09394394B2
公开(公告)日：2016-07-19
申请号：US14448062
申请日：2014-07-31
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Bruno Ameduri , Gerald Lopez
IPC分类号： C08F2/38 , C08F214/24 , C08F214/08 , C08F214/20 , C08F293/00
CPC分类号： C08F214/242 , C08F2/38 , C08F214/24 , C08F293/005 , C08F2438/00
摘要： Methods for the synthesis of CTFE-based block copolymers through iodine transfer polymerization are disclosed. In an exemplary embodiment, a method includes reacting a fluoromonomer “M” with a chain transfer agent of the formula X—Y or Y—X—Y, wherein X represents a C1-C3 hydrocarbon, a C1-C6 hydrofluorocarbon, C1-C6 hydrochlorofluorocarbon, or C1-C6 fluorocarbon and Y represents iodine or bromine, in the presence of a radical initiator, to form a macro-initiator of the formula: X-poly(M)-Y or Y-poly(M)-X-poly(M)-Y, wherein poly(M) represents a polymer of the fluoromonomer. The method further includes reacting the macro-initiator with chlorotrifluoroethylene (CTFE) in the presence of a radical initiator to form a diblock or a triblock CTFE-based block copolymer of the formula: X-poly(M)-block-poly(CTFE) or PCTFE-block-poly(M)-X-poly(M)-block-PCTFE.
摘要翻译：公开了通过碘转移聚合合成CTFE基嵌段共聚物的方法。在一个示例性实施方案中，一种方法包括使含氟单体“M”与式X-Y或Y-X-Y的链转移剂反应，其中X表示C1-C3烃，C1-C6氢氟烃，C1-C6 氯代氟代烃或C1-C6碳氟化合物，Y代表碘或溴，在自由基引发剂的存在下形成下式的大分子引发剂：X-聚（M）-Y或Y-聚（M）-X- 聚（M）-Y，其中聚（M）表示所述含氟单体的聚合物。该方法还包括在自由基引发剂的存在下使大分子引发剂与氯三氟乙烯（CTFE）反应以形成下式的二嵌段或三嵌段CTFE基嵌段共聚物：X-聚（M） - 嵌段 - 聚（CTFE）或PCTFE-嵌段 - 聚（M）-X-聚（M） - 嵌段-PCFEFE。

6. 发明申请

US20140234630A1 FLUOROPOLYMERS CONTAINING A COPOLYMERIZED FLUOROMONOMER AND A FUNCTIONAL HYDROCARBON COMONOMER AND ARTICLES MADE FROM SUCH FLUOROPOLYMERS 有权
标题翻译：含有共聚氟化物的氟聚合物和功能性烃类化合物以及来自这些氟聚合物的制品
公开(公告)号：US20140234630A1
公开(公告)日：2014-08-21
申请号：US14177784
申请日：2014-02-11
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Bruno Ameduri , Gerald Lopez , Eric Rainal , Noureddine Ajellal , Gary Martin
IPC分类号： C09D127/12
CPC分类号： C09D127/12 , B32B27/08 , B32B27/304 , B32B27/308 , B32B27/322 , B32B27/36 , B32B2307/412 , B32B2307/714 , B32B2307/7265 , B32B2439/00 , B32B2439/80 , B32B2581/00 , B32B2597/00 , C08F214/18 , C08J5/18 , C08J7/047 , C08J2327/06 , C08J2327/12 , C08J2367/02 , C08J2379/08 , C08J2427/04 , C08J2427/12 , Y10T428/31507 , Y10T428/31544
摘要： Disclosed is a copolymer film that includes a first comonomer including a chlorofluoro olefin and a second comonomer that is selected from the group consisting of itaconic acid, 2,3-dihydropyran, D-glucal, glycerine carbonate vinyl ether, 2-hydroxypropyl acrylate, maleic anhydride, vinylidene chloride, and mixtures thereof.
摘要翻译：公开了一种共聚物膜，其包含第一共聚单体，其包含氯氟烯烃和选自衣康酸，2,3-二氢吡喃，D-葡萄糖，甘油碳酸酯乙烯基醚，丙烯酸2-羟丙酯，马来酸酐的第二共聚单体酸酐，偏二氯乙烯及其混合物。

7. 发明授权

US09234062B2 Process, properties, and applications of graft copolymers 有权
标题翻译：接枝共聚物的工艺，性能和应用
公开(公告)号：US09234062B2
公开(公告)日：2016-01-12
申请号：US13713630
申请日：2012-12-13
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Eric Rainal , Bruno Ameduri , Frédéric Boschet , Noureddine Ajellal , Gerald Lopez
IPC分类号： C08F214/24 , C08F259/00 , C08F259/08 , C08F259/02 , C08J5/18
CPC分类号： C08F214/24 , C08F259/00 , C08J5/18 , C08J2327/12
摘要： Fluorinated macromonomers, a PCTFE-g-poly(M) graft copolymer, and moisture barrier films and articles formed therefrom are provided. The PCTFE-g-poly(M) graft copolymers have a PCTFE backbone component and a plurality of pendant groups attached to the PCTFE backbone component.
摘要翻译：提供氟化大分子单体，PCTFE-g-聚（M）接枝共聚物，以及防潮膜和由其形成的制品。 PCTFE-g-聚（M）接枝共聚物具有连接到PCTFE骨架组分的PCTFE骨架组分和多个侧基。

8. 发明申请

US20130184422A1 PROCESS, PROPERTIES, AND APPLICATIONS OF GRAFT COPOLYMERS 有权
标题翻译： GRAFT共聚物的工艺，性能和应用
公开(公告)号：US20130184422A1
公开(公告)日：2013-07-18
申请号：US13713630
申请日：2012-12-13
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Eric Rainal , Bruno Ameduri , Frédéric Boschet , Noureddine Ajellal , Gerald Lopez
IPC分类号： C08F214/24
CPC分类号： C08F214/24 , C08F259/00 , C08J5/18 , C08J2327/12
摘要： Fluorinated macromonomers, a PCTFE-g-poly(M) graft copolymer, and moisture barrier films and articles formed therefrom are provided. The PCTFE-g-poly(M) graft copolymers have a PCTFE backbone component and a plurality of pendant groups attached to the PCTFE backbone component.
摘要翻译：提供氟化大分子单体，PCTFE-g-聚（M）接枝共聚物，以及防潮膜和由其形成的制品。 PCTFE-g-聚（M）接枝共聚物具有连接到PCTFE骨架组分的PCTFE骨架组分和多个侧基。

9. 发明授权

US11654667B2 Flexible substrates with chemical and moisture resistance 有权
公开(公告)号：US11654667B2
公开(公告)日：2023-05-23
申请号：US16864927
申请日：2020-05-01
申请人： HONEYWELL INTERNATIONAL INC.
发明人： Gary M. Skwarek , Carl Altman , Jong Lee , Eric Rainal , Awdhoot Vasant Kerkar , Alagappan Thenappan
IPC分类号： C08J5/18 , B32B27/32 , B32B27/36 , B32B27/34 , B65D75/30 , B32B37/15 , B29C48/00 , B29C48/18 , A61M35/00 , B32B27/08 , A61K9/70 , B29L31/00 , B29K27/00
CPC分类号： B32B27/322 , A61K9/703 , A61M35/00 , B29C48/0019 , B29C48/0021 , B29C48/022 , B29C48/18 , B32B27/08 , B32B27/325 , B32B27/34 , B32B27/36 , B32B37/153 , B65D75/30 , A61K9/7038 , A61K9/7084 , B29K2027/16 , B29L2031/712 , B32B2307/518 , B32B2307/714 , B32B2307/7265 , B32B2439/40 , B32B2439/80 , B32B2535/00
摘要： Flexible packages, transdermal drug delivery devices, and methods for fabricating packages are provided. An exemplary flexible package includes a chemical and moisture resistant layer formed from poly(chlorotrifluoroethylene-co-vinylidene fluoride) (“P(CTFE-co-VDF)”) copolymer. Further, the exemplary flexible package includes a substance to be delivered. The substance is applied to or enclosed by the chemical and moisture resistant layer.

10. 发明授权

US09862811B2 Methods for synthesizing stabilized polymers of chlorotrifluoroethylene and products manufactured using such polymers 有权
公开(公告)号：US09862811B2
公开(公告)日：2018-01-09
申请号：US14804660
申请日：2015-07-21
申请人： Honeywell International Inc.
发明人： Alagappan Thenappan , Eric Rainal
IPC分类号： C08K5/19
CPC分类号： C08K5/19 , C08F14/24 , C08F2/16
摘要： Methods for synthesizing stabilized polymers of chlorotrifluoroethylene and products manufactured using such polymers are disclosed herein. In one exemplary embodiment, a method for synthesizing chlorotrifluoroethylene (CTFE)-based polymers includes reacting, in the presence of an initiator and in a reaction medium at a pH of about 1.5 to about 2.5, one or more monomers comprising CTFE and after an amount of polymerization reaction time has passed, adding a neutralizing agent to the reaction medium to increase the pH of the reaction medium to within a range of about 1.8 to about 6.0.

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