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    • 1. 发明授权
    • Method of producing disazo pigment
    • US06303762B1
    • 2001-10-16
    • US09827098
    • 2001-04-06
    • Hitoshi MakiHideto NoguchiKenji KitamuraMasami Shirao
    • Hitoshi MakiHideto NoguchiKenji KitamuraMasami Shirao
    • C09B6720
    • C09B67/0055C09B41/006
    • Disclosed is a method of producing a disazo pigment, which a coupling reaction is carried out while feeding, into an acidic aqueous solution, a tetrazo aqueous solution containing a tetrazo component of benzidines and a coupler aqueous solution containing a coupling component, wherein the coupling component is a mixture comprising a main component represented by the formula (1): CH3COCH2CONH—X, wherein X represents a phenyl group optionally having one or the same or different plural substituents selected from the group consisting of a methyl group, methoxy group and chlorine atom; a first additional component represented by the formula (2): CH3COCH2CONH—Y, wherein Y represents a phenyl group having a substituent selected from the group consisting of —CONR2 group, —SO2NR2 group and —NHCOR group, and the phenyl group may further have a substituent selected from the group consisting of a methyl group, methoxy group, chlorine atom, —CONR2 group, —SO2NR2 group and —NHCOR group, and wherein Rs may be the same or different mutually, and represent a hydrogen atom, C1 to C4 alkyl group (the alkyl groups may be mutually connected to form a ring) or C1 to C4 alkylene NR′2, further wherein R's represent a hydrogen atom or C1 to C4 alkyl groups which may be mutually different (the alkyl groups may be mutually connected to form a ring); and, a second additional component represented by the formula (3): CH3COCH2CONH—Z, wherein Z represents a phenyl group substituted by any one of a carboxyl group or alkali metal salts thereof, hydroxyl group or sulfonic acid group or alkali metal salts thereof, and said phenyl group may further has a substituent selected from the group consisting of a methyl group, methoxy group, chlorine atom, carboxyl group or alkali metal salts thereof, hydroxyl group or sulfonic acid group or alkali metal salts thereof. According to the method, disazo pigments can be obtained which manifest excellent transparency and flowability of the inks produced therefrom, and excellent flushing property and flushing drain coloration resistance in the pigment production process, or excellent dispersibility when ink is formed under dry condition.
    • 6. 发明申请
    • Method for forming polarization reversal
    • 形成极化反转的方法
    • US20110197432A1
    • 2011-08-18
    • US13066737
    • 2011-04-22
    • Futoshi YamamotoJunichiro IchikawaSatoshi OikawaSunao KurimuraKenji Kitamura
    • Futoshi YamamotoJunichiro IchikawaSatoshi OikawaSunao KurimuraKenji Kitamura
    • H01F7/06
    • G02F1/3558Y10T29/4902
    • A method for forming a ferroelectric spontaneous polarization reversal in a desired region of a ferroelectric substrate includes the steps of forming, for the desired region of the surface of the ferroelectric substrate, an electrode pattern or a mask pattern composed of aggregates of micropatterns, and then applying a given voltage into the desired region. The configuration of the micropatterns can be a stripe-shaped pattern, an ellipse-shaped pattern, a hexagon-shaped pattern, a network pattern, or a double cross shaped pattern. The method can further include the steps of generating many nucleuses by using the electrode pattern or the mask pattern composed of the aggregates of micropatterns, forming another electrode pattern or another mask pattern corresponding to the desired region, and then applying a given voltage into the desired region to generate a ferroelectric spontaneous polarization reversal around the nucleuses.
    • 在铁电基板的所需区域中形成铁电自发极化反转的方法包括以下步骤:对于铁电体基板的表面的期望区域,形成由微图案的聚集体构成的电极图案或掩模图案,然后 将给定电压施加到所需区域。 微图案的构造可以是条形图案,椭圆形图案,六边形图案,网状图案或双十字形图案。 该方法还可以包括通过使用由微图案的聚集体形成的电极图案或掩模图案,形成另一电极图案或对应于期望区域的另一掩模图案,然后将给定电压施加到期望的 区域以产生围绕核的铁电自发极化反转。
    • 8. 发明申请
    • Wavelength conversion element having multi-gratings and light generating apparatus using said element, and wavelength conversion element having cylindrical ferroelectric single crystals and light generating apparatus using said element
    • 具有多光栅的波长转换元件和使用所述元件的发光装置,以及具有圆柱形铁电单晶体的波长转换元件和使用所述元件的发光装置
    • US20070127107A1
    • 2007-06-07
    • US10575535
    • 2004-11-19
    • Kenji KitamuraSunao KurimuraMasaru NakamuraShunji Takekawa
    • Kenji KitamuraSunao KurimuraMasaru NakamuraShunji Takekawa
    • G02B26/00G02F1/00G02F1/01
    • G02F1/37G02F2001/3507G02F2001/3548G02F2202/20
    • A wavelength conversion element having multi-gratings free from damage propagation and a light generating apparatus using it, and a wavelength conversion element having multi-gratings to make a thermal distribution centrosymmetric, and being free from damage propagation, are provided. The wavelength conversion element is realized by comprising a holder and plural prismatic ferroelectric single crystals disposed in the holder, wherein plural prismatic ferroelectric single crystals have at least five planes; the aspect ratios of planes perpendicular to respective longitudinal directions of the plural prismatic ferroelectric single crystals are virtually unity; and each of the plural prismatic ferroelectric single crystals has a domain inversion structure with a predetermined period in the direction perpendicular to the polarization direction thereof, and is arranged in a way that said direction perpendicular to the polarization direction is the same as those of the other crystals. In addition, the element is realized by selecting ferroelectric material from a group comprising lithium niobate, lithium tantalate, impurity-doped lithium niobate, and impurity-doped lithium tantalate, each with virtually stoichiometric composition, and processing it into the cylindrical ferroelectric single crystal with a virtually completely round cross-section.
    • 提供了具有不受损伤传播的多光栅的波长转换元件和使用它的发光装置,以及具有多光栅以实现热分布中心对称,并且没有损伤传播的波长转换元件。 波长转换元件通过包括保持器和设置在保持器中的多个棱柱铁电单晶实现,其中多个棱柱铁电单晶具有至少五个平面; 垂直于多个棱柱铁电单晶的纵向方向的平面的纵横比实际上是一致的; 并且多个棱柱铁电单晶中的每一个具有在垂直于其偏振方向的方向上具有预定周期的畴反转结构,并且以与偏振方向垂直的方向与其他方向相同的方式 晶体。 此外,该元件通过从包含铌酸锂,钽酸锂,杂质掺杂的铌酸锂和杂质掺杂的钽酸锂的组中选择铁电材料来实现,每个具有实质上的化学计量组成,并且将其加工成圆柱形铁电单晶, 一个几乎完全圆形的横截面。