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1. 发明授权

US5659036A Process for the production of 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester, and process for the production of quinacridone from said ester as intermediate 失效
标题翻译：制备2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯的方法，以及由所述酯制备喹吖啶酮的方法，为中间体
公开(公告)号：US5659036A
公开(公告)日：1997-08-19
申请号：US409931
申请日：1995-03-23
申请人： Hitoshi Maki , Shigeki Kato , Yoshimi Kikuchi
发明人： Hitoshi Maki , Shigeki Kato , Yoshimi Kikuchi
IPC分类号： C07B61/00 , C07C227/08 , C07C227/22 , C07C229/32 , C07C229/62 , C07D471/04 , C09B48/00
CPC分类号： C09B48/00 , C07C227/22 , C07C2101/16
摘要： A process for producing 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester having a high purity from 1,4-cyclohexanedione-2,5-di(carboxylic acid alkyl ester) at high yields for a short period of time; a process for producing quinacridone of which the byproduct content is small, from the above 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester; and a process for producing quinacridone of which the particle diameter is adjusted as desired, from the above 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester without adding a step of forming a pigment.
摘要翻译：一种从1,4-环己二酮-2,5-二（羧酸烷基酯）以高产率生产具有高纯度的2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯的方法，的时间由上述2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯制备副产物含量小的喹吖啶酮的方法; 以及根据需要从上述2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯制备其粒径的喹吖啶酮的方法，而不添加形成颜料的步骤。

2. 发明授权

US5622555A Process for the production of dis-azo pigment 失效
标题翻译：偶氮颜料生产工艺
公开(公告)号：US5622555A
公开(公告)日：1997-04-22
申请号：US417112
申请日：1995-04-05
申请人： Yoshio Muramatsu , Ataru Chiba , Hitoshi Maki
发明人： Yoshio Muramatsu , Ataru Chiba , Hitoshi Maki
IPC分类号： C09B67/06 , C09B67/20 , C09B27/00
CPC分类号： C09B67/0003
摘要： A process for the production of a dis-azo pigment having excellent dispersibility, high tinting strength and high masking strength, by a simple method under an improved working environment, which is improved in a drying step and can omit the pulverization step of a conventional process, the present process comprising(a) a first step of forming an aqueous paste or slurry containing a synthesized dis-azo pigment into fine particles under hot air at 100.degree. to 300.degree. C. for a short period of time within 0.5 hour, and at the same time, removing water from the formed fine particles to form a powder, and(b) a second step of keeping the powder under heat at 50.degree. to 150.degree. C. for 0.5 to 10 hours.
摘要翻译：通过在改善的工作环境下的简单方法生产具有优异分散性，高着色强度和高掩蔽强度的偶氮颜料的方法，其在干燥步骤中得到改进并且可以省略常规方法的粉碎步骤本方法包括（a）第一步骤，在100℃至300℃的热空气下，在0.5小时内将短时间内将含有合成的偶氮颜料的含水糊剂或浆料形成微粒;以及同时从形成的细颗粒中除去水以形成粉末，和（b）将粉末在50至150℃下保持0.5至10小时的第二步骤。

3. 发明授权

US07001937B2 Process for producing colored resin composition and utilization thereof 有权
公开(公告)号：US07001937B2
公开(公告)日：2006-02-21
申请号：US10240831
申请日：2002-02-14
申请人： Hitoshi Maki , Masayasu Kawamura , Masashi Koide
发明人： Hitoshi Maki , Masayasu Kawamura , Masashi Koide
IPC分类号： C08J3/22 , C08J3/215 , C08K5/06
CPC分类号： C08J3/215 , C08J3/2056 , C08J2323/02
摘要： A process for the production of a colored resin composition, comprising a step (A) of producing an aqueous slurry of a pigment, a step (B) of producing a melting composition of metallocene type polyolefin containing a dispersant and a solvent, a step (C) of kneading the aqueous slurry obtained in the step (A) with the melting composition obtained in the step (B) and a step (D) of removing the solvent and the water from the kneaded mixture obtained in the step (C), a colored composition obtained in the above process has excellent in pigment dispersibility and high color developing properties, a colored resin molded article obtained from the colored resin composition do not give a physical-properties inhibition of 5% or higher and has a color developing properties.

4. 发明授权

US5472490A Pigment composition, printing ink and coating composition 失效
标题翻译：颜料组成，印刷油墨和涂料组成
公开(公告)号：US5472490A
公开(公告)日：1995-12-05
申请号：US229779
申请日：1994-04-19
申请人： Katsuhiko Sawamura , Shigeki Kato , Hitoshi Maki , Mikio Hayashi
发明人： Katsuhiko Sawamura , Shigeki Kato , Hitoshi Maki , Mikio Hayashi
IPC分类号： C09B67/00 , C09B67/20 , C09B67/22 , C09D7/00 , C09D7/12 , C09D11/02 , C09D11/033 , C09D11/037 , C09B67/50
CPC分类号： C09D11/037 , C09B67/0032 , C09B67/0035 , C09D7/007
摘要： A pigment composition which comprises a phthalocyanine pigment, a phthalocyanine derivative (A) of the formula (1),Pc-(SO.sub.3.sup.-+ NR.sub.1 R.sub.2 R.sub.3 R.sub.4).sub.n(1)and at least one compound (B) selected from the class consisting of a compound of the formula (2),(M.sub.1).sub.j X (2)an aliphatic compound containing carboxylic acid alkali metal salt and an aliphatic compound containing carboxylic acid ammonium salt, and which imparts a printing or a coating with excellent gloss and shows excellent fluidity and stability with time when dispersed in a vehicle for a printing ink or a coating composition.
摘要翻译：一种颜料组合物，其包含酞菁颜料，式（1）的酞菁衍生物（A），Pc-（SO 3 - + NR 1 R 2 R 3 R 4）n（1）和至少一种选自化合物式（2），（M1）jX（2）含有羧酸碱金属盐的脂肪族化合物和含有羧酸铵盐的脂肪族化合物，赋予印刷或涂料优异的光泽度并显示优异的流动性和稳定性随时间分散在用于印刷油墨或涂料组合物的载体中。

5. 发明授权

US5318626A Process for converting 2,9-dimethylquinacridone compound into pigment 失效
标题翻译：将2,9-二甲基喹吖啶酮化合物转化为颜料的方法
公开(公告)号：US5318626A
公开(公告)日：1994-06-07
申请号：US78323
申请日：1993-06-22
申请人： Hitoshi Maki , Shigeki Kato
发明人： Hitoshi Maki , Shigeki Kato
IPC分类号： C09B67/20 , C09B67/10 , C09B67/14 , C09B67/52 , C09B48/00
CPC分类号： C09B67/0017 , C09B67/0014
摘要： A process for converting a 2,9-dimethylquinacridone compound into a pigment, which comprises pouring a solution of a crude 2,9-dimethylquinacridone compound in sulfuric acid into continuously flowing water to form a fine precipitate, recovering said precipitate by filtration, washing it with water, adding it to a lower alcohol having 1 to 4 carbon atoms and heating the resultant mixture to 60.degree.-200.degree. C.
摘要翻译： PCT No.PCT / JP92 / 01462 Sec。 371日期：1993年6月22日 102（e）日期1993年6月22日PCT 1992年11月6日PCT PCT。出版物WO93 / 09186 日本公报1993年5月13日。一种将2,9-二甲基喹吖啶酮化合物转化成颜料的方法，其包括将粗制的2,9-二甲基喹吖啶酮化合物在硫酸中的溶液倒入连续流动的水中形成细小的沉淀物，回收所述通过过滤沉淀，用水洗涤，将其加入到具有1至4个碳原子的低级醇中，并将所得混合物加热至60℃-200℃。

6. 发明授权

US06989055B2 Monoazo lake pigment composition and gravure ink using the same 失效
标题翻译： Monoazo湖颜料组合物和凹版油墨使用相同
公开(公告)号：US06989055B2
公开(公告)日：2006-01-24
申请号：US10634858
申请日：2003-08-06
申请人： Kenji Kitamura , Shigeki Kato , Hitoshi Maki , Shoko Goto , Motoi Shitaka , Osamu Shiromaru
发明人： Kenji Kitamura , Shigeki Kato , Hitoshi Maki , Shoko Goto , Motoi Shitaka , Osamu Shiromaru
IPC分类号： C09B67/08
CPC分类号： C09D11/037 , C09B41/003 , C09B63/005
摘要： A monoazo lake pigment composition containing a monoazo lake pigment obtained from a laked pigment aqueous slurry prepared by conducting coupling of a diazo component obtained by diazotizing an aromatic amine having a soluble group and a coupler component and conducting laking after or simultaneously with the coupling, wherein the laking is carried out in the presence of a water-soluble acrylic polymer in an amount of 0.1 to 40 parts by weight per 100 parts of the above coupler component, and a gravure ink containing the above pigment composition and a gravure ink vehicle.
摘要翻译：一种单偶氮色淀颜料组合物，其含有通过将通过重氮化具有可溶性基团的芳族胺和偶合剂组分获得的重氮组分并在偶合之后或与耦合同时进行的沉淀而制备的浸渍颜料含水浆料中获得的单偶氮颜料，其中在水溶性丙烯酸类聚合物存在下，每100份上述成色剂成分为0.1〜40重量份，含有上述颜料组合物的凹版油墨和凹版油墨载色剂进行浸渍。

7. 发明授权

US5817817A Process for the production of 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester, and process for the production of quinacridone from said ester as intermediate 失效
标题翻译：制备2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯的方法，以及由所述酯制备喹吖啶酮的方法，为中间体
公开(公告)号：US5817817A
公开(公告)日：1998-10-06
申请号：US848179
申请日：1997-04-29
申请人： Hitoshi Maki , Shigeki Kato , Yoshimi Kikuchi
发明人： Hitoshi Maki , Shigeki Kato , Yoshimi Kikuchi
IPC分类号： C07B61/00 , C07C227/08 , C07C227/22 , C07C229/32 , C07C229/62 , C07D471/04 , C09B48/00
CPC分类号： C09B48/00 , C07C227/22 , C07C2101/16
摘要： A process for producing 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester having a high purity from 1,4-cyclohexanedione-2,5-di(carboxylic acid alkyl ester) at high yields for a short period of time; a process for producing quinacridone of which the byproduct content is small, from the above 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester; and a process for producing quinacridone of which the particle diameter is adjusted as desired, from the above 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester without adding a step of forming a pigment.
摘要翻译：一种从1,4-环己二酮-2,5-二（羧酸烷基酯）以高产率生产具有高纯度的2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯的方法，的时间由上述2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯制备副产物含量小的喹吖啶酮的方法; 以及根据需要从上述2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯制备其粒径的喹吖啶酮的方法，而不添加形成颜料的步骤。

8. 发明授权

US5610306A Process for the production of 6,13-dihydroquinacridones and apparatus for use for the production 失效
标题翻译：用于生产6,13-二氢喹吖啶酮的方法和用于生产的装置
公开(公告)号：US5610306A
公开(公告)日：1997-03-11
申请号：US341969
申请日：1994-11-16
申请人： Hitoshi Maki , Shigeki Kato , Shinichi Azuma , Mikio Hayashi , Masatoshi Momose
发明人： Hitoshi Maki , Shigeki Kato , Shinichi Azuma , Mikio Hayashi , Masatoshi Momose
IPC分类号： C09B48/00 , B01J10/02 , B01J19/18 , C07D471/04
CPC分类号： C07D471/04 , B01J10/02 , B01J19/18 , B01J2219/00094 , B01J2219/00132 , B01J2219/00189 , B01J2219/185
摘要： A process for producing highly pure 6,13-dihydroquinacridone, which is a suitable intermediate for effectively producing a quinacridone pigment, for a short period of time at high yields, the process comprising providing a cylindrical reactor, providing an atmosphere free of oxygen in the cylindrical reactor, heating the cylindrical reactor so that the temperature of at least a surface of an inner wall of a cylinder of the cylindrical reactor is in the range of from 250.degree. to 400.degree. C., introducing a powder of 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester or a mixture of 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester with a liquid through a feed port provided in an upper portion of the cylindrical reactor, keeping the powder or the mixture in substantial contact with the inner wall of the cylindrical reactor so that an intramolecular alcohol-elimination reaction of the 2,5-di(arylamino)-3,6-dihydroterephthalic acid dialkyl ester takes place to form 6,13-dihydroquinacridone, and taking out the 6,13-dihydroquinacridone through an outlet provided in a lower portion of the cylindrical reactor.
摘要翻译：一种生产高纯度6,13-二氢喹吖啶酮的方法，该方法是用于有效地制备喹吖啶酮颜料的合适的中间体，其产率高，在短时间内，该方法包括提供圆柱形反应器，在该反应器中提供无氧气氛圆柱形反应器，加热圆柱形反应器，使得圆筒形反应器的圆筒的内壁的至少一个表面的温度在250-400℃的范围内，引入2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯或2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯与液体的混合物，通过设置在圆筒形反应器上部的进料口，保持粉末或混合物与圆柱形反应器的内壁充分接触，从而进行2,5-二（芳基氨基）-3,6-二氢对苯二甲酸二烷基酯的分子内醇消除反应，形成6， 13-d 并通过设置在圆筒形反应器下部的出口取出6,13-二氢喹吖啶酮。

9. 发明授权

US06303762B1 Method of producing disazo pigment 有权
公开(公告)号：US06303762B1
公开(公告)日：2001-10-16
申请号：US09827098
申请日：2001-04-06
申请人： Hitoshi Maki , Hideto Noguchi , Kenji Kitamura , Masami Shirao
发明人： Hitoshi Maki , Hideto Noguchi , Kenji Kitamura , Masami Shirao
IPC分类号： C09B6720
CPC分类号： C09B67/0055 , C09B41/006
摘要： Disclosed is a method of producing a disazo pigment, which a coupling reaction is carried out while feeding, into an acidic aqueous solution, a tetrazo aqueous solution containing a tetrazo component of benzidines and a coupler aqueous solution containing a coupling component, wherein the coupling component is a mixture comprising a main component represented by the formula (1): CH3COCH2CONH—X, wherein X represents a phenyl group optionally having one or the same or different plural substituents selected from the group consisting of a methyl group, methoxy group and chlorine atom; a first additional component represented by the formula (2): CH3COCH2CONH—Y, wherein Y represents a phenyl group having a substituent selected from the group consisting of —CONR2 group, —SO2NR2 group and —NHCOR group, and the phenyl group may further have a substituent selected from the group consisting of a methyl group, methoxy group, chlorine atom, —CONR2 group, —SO2NR2 group and —NHCOR group, and wherein Rs may be the same or different mutually, and represent a hydrogen atom, C1 to C4 alkyl group (the alkyl groups may be mutually connected to form a ring) or C1 to C4 alkylene NR′2, further wherein R's represent a hydrogen atom or C1 to C4 alkyl groups which may be mutually different (the alkyl groups may be mutually connected to form a ring); and, a second additional component represented by the formula (3): CH3COCH2CONH—Z, wherein Z represents a phenyl group substituted by any one of a carboxyl group or alkali metal salts thereof, hydroxyl group or sulfonic acid group or alkali metal salts thereof, and said phenyl group may further has a substituent selected from the group consisting of a methyl group, methoxy group, chlorine atom, carboxyl group or alkali metal salts thereof, hydroxyl group or sulfonic acid group or alkali metal salts thereof. According to the method, disazo pigments can be obtained which manifest excellent transparency and flowability of the inks produced therefrom, and excellent flushing property and flushing drain coloration resistance in the pigment production process, or excellent dispersibility when ink is formed under dry condition.

10. 发明授权

US5808154A Process for the production of an aromatic hydrazo compound 失效
标题翻译：制备芳香族氢化合物的方法
公开(公告)号：US5808154A
公开(公告)日：1998-09-15
申请号：US924606
申请日：1992-07-27
申请人： Hitoshi Maki
发明人： Hitoshi Maki
IPC分类号： C07C241/02 , C07C243/00 , C09B27/00
CPC分类号： C07C241/02
摘要： A process for the production of an aromatic hydrazo compound, which comprises catalytically reducing an aromatic nitro compound with hydrogen in an alkali metal hydroxide aqueous solution and a hydrogen-donating solvent in the presence of a noble metal catalyst and a quinoid compound cocatalyst at a high temperature under a high pressure, the hydrogen-donating solvent being a cyclic hydrocarbon in which hydrogen atoms are attached to its basic skeleton having 1 to 4 aromatic rings and at least one unsaturated carbon-carbon bond remains.
摘要翻译：一种制备芳香族氢化合物的方法，其包括在贵金属催化剂和醌型化合物助催化剂的存在下，在碱金属氢氧化物水溶液和给氢溶剂中用氢气将芳族硝基化合物催化还原在高压下，供氢溶剂是其中氢原子连接到其具有1-4个芳族环和至少一个不饱和碳 - 碳键的基本骨架上的环状烃。

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