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1. 发明授权

US07579414B2 Fine-particled amphoteric aqueous polymer dispersion method for production and use thereof 有权
标题翻译：细颗粒两性水性聚合物分散体的制造和使用方法
公开(公告)号：US07579414B2
公开(公告)日：2009-08-25
申请号：US11569912
申请日：2005-06-03
申请人： Hildegard Kukula , Roland Ettl , Rainer Dyllick-Brenzinger , Bernhard Sturm
发明人： Hildegard Kukula , Roland Ettl , Rainer Dyllick-Brenzinger , Bernhard Sturm
IPC分类号： C08F2/00
CPC分类号： D21H21/16 , C08F212/08 , C08F212/10 , C08F257/02 , C14C11/003 , D21H11/14 , D21H17/37 , D21H17/375 , D21H17/45 , C08F2/18 , C08F220/18
摘要： Finely divided, amphoteric, aqueous polymer dispersions which are obtainable by a two-stage polymerization, a prepolymer being prepared in the first polymerization stage from a monomer mixture comprising (a) from 15 to 40% by weight of at least one (meth)acrylate and/or (meth)acrylamide having in each case a free amino group, protonated amino group and/or quaternized amino group, (b) from 40 to 70% by weight of at least one optionally substituted styrene, (c) from 0 to 25% by weight of acrylonitrile and/or methacrylonitrile, (d) from 0.5 to 5% by weight of at least one ethylenically unsaturated monomer comprising acid groups and (e) from 0 to 30% by weight of at least one nonionic, ethylenically unsaturated monomer differing from (b) and (c), the sum of (a)+(b)+(c)+(d)+(e) being 100% by weight, in a solution polymerization in a solvent partly to completely miscible with water, water then being added to the solution/dispersion of the prepolymer and then at least one nonionic, ethylenically unsaturated monomer being subjected to an emulsion polymerization in the aqueous solution of the prepolymer in a second polymerization stage, processes for the preparation of the polymer dispersions by two-stage polymerization and use of the polymer dispersions as sizes for paper, board and cardboard.
摘要翻译：通过两阶段聚合可得到的细分两性聚合物水分散体，预聚物在第一聚合阶段由单体混合物制备，所述单体混合物包含（a）15-40％重量的至少一种（甲基）丙烯酸酯和/或（甲基）丙烯酰胺，其各自为游离氨基，质子化氨基和/或季铵化氨基，（b）40至70重量％的至少一种任选取代的苯乙烯，（c）0至 25重量％的丙烯腈和/或甲基丙烯腈，（d）0.5至5重量％的至少一种包含酸基的烯键式不饱和单体和（e）0至30重量％的至少一种非离子，烯属不饱和单体与（b）和（c）不同的单体，在溶剂中的溶液聚合中部分地完全混溶的（a）+（b）+（c）+（d）+（e）的总和为100重量％用水，然后将水加入到预聚物的溶液/分散体中，然后加入至少一种非离子的乙烯 lly不饱和单体在第二聚合阶段在预聚物的水溶液中进行乳液聚合，通过两步聚合制备聚合物分散体的方法和使用聚合物分散体作为纸，纸板和纸板的尺寸。

2. 发明申请

US20080039598A1 Fine-Particled Amphoteric Aqueous Polymer Dispersion Method for Production and Use Thereof 有权
标题翻译：用于生产和使用的细颗粒两性水性聚合物分散体方法
公开(公告)号：US20080039598A1
公开(公告)日：2008-02-14
申请号：US11569912
申请日：2005-06-03
申请人： Hildegard Kukula , Roland Ettl , Rainer Dyllick-Brenzinger , Bernhard Sturm
发明人： Hildegard Kukula , Roland Ettl , Rainer Dyllick-Brenzinger , Bernhard Sturm
IPC分类号： C08F2/22
CPC分类号： D21H21/16 , C08F212/08 , C08F212/10 , C08F257/02 , C14C11/003 , D21H11/14 , D21H17/37 , D21H17/375 , D21H17/45 , C08F2/18 , C08F220/18
摘要： Finely divided, amphoteric, aqueous polymer dispersions which are obtainable by a two-stage polymerization, a prepolymer being prepared in the first polymerization stage from a monomer mixture comprising (a) from 15 to 40% by weight of at least one (meth)acrylate and/or (meth)acrylamide having in each case a free amino group, protonated amino group and/or quaternized amino group, (b) from 40 to 70% by weight of at least one optionally substituted styrene, (c) from 0 to 25% by weight of acrylonitrile and/or methacrylonitrile, (d) from 0.5 to 5% by weight of at least one ethylenically unsaturated monomer comprising acid groups and (e) from 0 to 30% by weight of at least one nonionic, ethylenically unsaturated monomer differing from (b) and (c), the sum of (a)+(b)+(c)+(d)+(e) being 100% by weight, in a solution polymerization in a solvent partly to completely miscible with water, water then being added to the solution/dispersion of the prepolymer and then at least one nonionic, ethylenically unsaturated monomer being subjected to an emulsion polymerization in the aqueous solution of the prepolymer in a second polymerization stage, processes for the preparation of the polymer dispersions by two-stage polymerization and use of the polymer dispersions as sizes for paper, board and cardboard.
摘要翻译：通过两阶段聚合可得到的细分两性聚合物水分散体，预聚物在第一聚合阶段由单体混合物制备，所述单体混合物包含（a）15-40％重量的至少一种（甲基）丙烯酸酯和/或（甲基）丙烯酰胺，其各自为游离氨基，质子化氨基和/或季铵化氨基，（b）40至70重量％的至少一种任选取代的苯乙烯，（c）0至 25重量％的丙烯腈和/或甲基丙烯腈，（d）0.5至5重量％的至少一种包含酸基的烯属不饱和单体和（e）0至30重量％的至少一种非离子，烯属不饱和单体与（b）和（c）不同的单体，在溶剂中的溶液聚合中部分地完全混溶的（a）+（b）+（c）+（d）+（e）的总和为100重量％用水，然后将水加入到预聚物的溶液/分散体中，然后加入至少一种非离子的乙烯 lly不饱和单体在第二聚合阶段在预聚物的水溶液中进行乳液聚合，通过两步聚合制备聚合物分散体的方法和使用聚合物分散体作为纸，纸板和纸板的尺寸。

3. 发明授权

US08512520B2 Paper sizing agent 有权
标题翻译：造纸剂
公开(公告)号：US08512520B2
公开(公告)日：2013-08-20
申请号：US11720362
申请日：2005-11-29
申请人： Markus Schmid , Roland Ettl , Klaus Lorenz , Rainer Dyllick-Brenzinger , Andreas Brockmeyer
发明人： Markus Schmid , Roland Ettl , Klaus Lorenz , Rainer Dyllick-Brenzinger , Andreas Brockmeyer
IPC分类号： D21H17/17 , D21H17/29 , D21H17/33 , D21H17/45 , D21H21/16 , D21H21/18 , C08L3/00
CPC分类号： D21H21/16 , D21H17/08 , D21H17/16 , D21H17/17 , D21H17/35
摘要： A paper size which comprises a stable aqueous dispersion of a reactive size, from 5 to 100% by weight, based on the reactive size, of a substantially linear nitrogen-comprising polymer having at least 3 mmol/g of basic nitrogen atoms, and from 1 to 50% by weight of cationic starch having a degree of substitution of at least 0.05 is described. The paper size has a good sizing effect and a stable viscosity.
摘要翻译：一种纸张尺寸，其包含基于反应性大小的反应性大小为5-100重量％的稳定的水性分散体，其具有至少3mmol / g碱性氮原子的基本上线性的含氮聚合物，以及描述1至50重量％的取代度至少为0.05的阳离子淀粉。纸张尺寸具有良好的施胶效果和粘度稳定性。

4. 发明申请

US20100016478A1 PAPER SIZE MIXTURES 审中-公开
标题翻译：纸尺寸混合
公开(公告)号：US20100016478A1
公开(公告)日：2010-01-21
申请号：US12518312
申请日：2007-12-11
申请人： Andreas Brockmeyer , Roland Ettl , Rainer Dyllick-Brenzinger
发明人： Andreas Brockmeyer , Roland Ettl , Rainer Dyllick-Brenzinger
IPC分类号： C08L3/02 , C08F2/16 , C08K5/15 , C08L29/04 , C08L39/06 , C08L33/00 , C08G67/00 , C08L89/00 , C08L33/06 , C08L55/00
CPC分类号： D21H17/34 , C08L3/00 , C08L2666/26 , C09J133/20 , D21H17/17 , D21H17/72 , D21H21/16
摘要： Paper size mixtures comprising a reactive size dispersed in water and a polymer, which are obtainable by mixing (a) an aqueous dispersion of a reactive size whose dispersed particles have a mean particle diameter of less than 500 nm, the dispersion being obtainable by emulsifying at least one reactive size in water in the presence of at least one surfactant, and (b) at least one emulsion polymer and/or at least one water-soluble polymer which does not have a dispersing effect with respect to reactive sizes and/or a water-dispersible polymer, and use of said paper size mixtures for the engine sizing and surface sizing of paper and paper products.
摘要翻译：通过混合（a）具有平均粒径小于500nm的分散颗粒的反应性尺寸的水性分散体可以获得的分散在水中的反应尺寸的聚合物的纸尺寸混合物，所述分散体可通过乳化在在至少一种表面活性剂存在下，在水中至少一种反应性大小，和（b）至少一种乳液聚合物和/或至少一种水溶性聚合物，其对于反应性大小和/或不具有分散作用水分散性聚合物，以及使用所述纸尺寸混合物用于纸和纸产品的发动机尺寸和表面施胶。

5. 发明授权

US07294190B2 Mixtures of solids, consisting of a reactive sizing agent and starch, method for producing said mixtures and use thereof 失效
公开(公告)号：US07294190B2
公开(公告)日：2007-11-13
申请号：US10576678
申请日：2004-10-15
申请人： Rainer Dyllick-Brenzinger , Thomas Kessler , Norbert Guentherberg , Peter Wittmer , Roland Ettl
发明人： Rainer Dyllick-Brenzinger , Thomas Kessler , Norbert Guentherberg , Peter Wittmer , Roland Ettl
IPC分类号： C08L3/02 , C09D103/02 , D21H17/17 , D21H21/16
CPC分类号： D21H21/16 , D21H17/17 , D21H17/28 , D21H17/72 , D21H23/04 , D21H23/22
摘要： Solid mixtures of a reactive size and starch, which are obtainable by mixing at least one reactive size with at least one starch in a melt in the presence of at least one destructuring agent for starch under the action of shear forces at from 65 to 250° C. and cooling the melt to room temperature, are used in the form of aqueous dispersions as process assistants in papermaking.

6. 发明申请

US20060009571A1 Aqueous polymer dispersions containing alkyldiketenes, methods for the production thereof, and their use 失效
标题翻译：含有烷基恶臭酮的聚合物水分散体，其制备方法及其用途
公开(公告)号：US20060009571A1
公开(公告)日：2006-01-12
申请号：US10529782
申请日：2003-10-09
申请人： Rainer Dyllick-Brenzinger , Roland Ettl , Franca Tiarks , Ulrich Riebeling
发明人： Rainer Dyllick-Brenzinger , Roland Ettl , Franca Tiarks , Ulrich Riebeling
IPC分类号： C08G18/63
CPC分类号： D06M13/13 , C08F2/22 , C08F2/44 , C14C11/003 , D21H17/17 , D21H17/72
摘要： Alkyldiketene-containing aqueous polymer dispersions which are obtainable by miniemulsion polymerization of hydrophobic monoethylenically unsaturated monomers in the presence of alkyldiketenes, processes for the preparation of such polymer dispersions and the use of the thus obtainable dispersions as sizes for paper or as water repellents for leather, natural and/or manmade fibers and textiles.
摘要翻译：含有烷基染料的含水聚合物分散体，其可通过疏水性单烯属不饱和单体在烷基二乙烯基酯的存在下的细乳液聚合得到，制备这种聚合物分散体的方法以及由此获得的分散体作为纸张的尺寸或用作皮革的防水剂，天然和/或人造纤维和纺织品。

7. 发明申请

US20060162883A1 Use of polymers containing vinylamine units as promoters for alkyldiketene glueing 审中-公开
标题翻译：含有乙烯胺单元的聚合物用作烷基乙烯基胶粘剂的促进剂
公开(公告)号：US20060162883A1
公开(公告)日：2006-07-27
申请号：US10523995
申请日：2003-07-24
申请人： Simon Champ , Roland Ettl , Rainer Dyllick-Brenzinger
发明人： Simon Champ , Roland Ettl , Rainer Dyllick-Brenzinger
IPC分类号： D21H17/17 , D21H21/16 , D21H23/04
CPC分类号： D21H21/16 , D21H17/17 , D21H23/04
摘要： The invention relates to the use of polymers containing vinylamine units having a K-value (determined in 5% of an aqueous sodium chloride solution and at a temperature of 25%, having a pH-value of 7, and a polymer concentration of 0.5 wt. %) of 30-150 as promoters for mass glueing of paper with alkyldiketenes.
摘要翻译：本发明涉及使用含有K值的乙烯胺单元的聚合物（在5％的氯化钠水溶液中，在25％的温度下测定，pH值为7，聚合物浓度为0.5wt ％）为30-150份，作为纸与烷基二乙烯基胶合的促进剂。

8. 发明授权

US07709052B2 Aqueous polymer dispersions containing alkyldiketenes, methods for the production thereof, and their use 失效
标题翻译：含有烷基恶臭酮的聚合物水分散体，其制备方法及其用途
公开(公告)号：US07709052B2
公开(公告)日：2010-05-04
申请号：US10529782
申请日：2003-10-09
申请人： Rainer Dyllick-Brenzinger , Roland Ettl , Franca Tiarks , Ulrich Riebeling
发明人： Rainer Dyllick-Brenzinger , Roland Ettl , Franca Tiarks , Ulrich Riebeling
IPC分类号： C08F212/00 , C08J3/00 , C08F2/00
CPC分类号： D06M13/13 , C08F2/22 , C08F2/44 , C14C11/003 , D21H17/17 , D21H17/72
摘要： Alkyldiketene-containing aqueous polymer dispersions which are obtainable by miniemulsion polymerization of hydrophobic monoethylenically unsaturated monomers in the presence of alkyldiketenes, processes for the preparation of such polymer dispersions and the use of the thus obtainable dispersions as sizes for paper or as water repellents for leather, natural and/or manmade fibers and textiles.
摘要翻译：含有烷基染料的含水聚合物分散体，其可通过疏水性单烯属不饱和单体在烷基二乙烯基酯的存在下的细乳液聚合得到，制备这种聚合物分散体的方法以及由此获得的分散体作为纸张的尺寸或用作皮革的防水剂，天然和/或人造纤维和纺织品。

9. 发明申请

US20090188054A1 Aqueous polymer dispersions containing alkenyl succinic acid anhydrides, methods for the production thereof, and use of the same 审中-公开
标题翻译：含有烯基琥珀酸酐的聚合物水分散体，其制备方法及其用途
公开(公告)号：US20090188054A1
公开(公告)日：2009-07-30
申请号：US10585339
申请日：2005-01-14
申请人： Rainer Dyllick-Brenzinger , Reinhold J. Leyrer , Andreas Brockmeyer , Markus Schmid , Roland Ettl
发明人： Rainer Dyllick-Brenzinger , Reinhold J. Leyrer , Andreas Brockmeyer , Markus Schmid , Roland Ettl
IPC分类号： C08F220/40 , D06M15/51
CPC分类号： D06M13/13 , C08F2/22 , C08F2/44 , C14C9/00 , D06M13/203 , D21H17/16 , D21H21/16
摘要： Aqueous alkenylsuccinic anhydride-containing polymer dispersions which are obtainable by miniemulsion polymerization of hydrophobic monoethylenically unsaturated monomers in the presence of alkenylsuccinic anhydrides, processes for the preparation of such polymer dispersions by polymerizing hydrophobic monomers by a miniemulsion polymerization method in the presence of at least one alkenylsuccinic anhydride and, if appropriate, an alkyldiketene, and use of the resulting aqueous alkenylsuccinic anhydride-containing polymer dispersions as engine and surface sizes for paper and for imparting water repellency to leather, natural and/or synthetic fibers and textiles.
摘要翻译：含有烯基琥珀酸酐的聚合物分散体，其可通过在烯基琥珀酸酐的存在下的疏水性单烯属不饱和单体的细乳液聚合获得，通过在至少一种烯基琥珀酸存在下通过微乳液聚合法聚合疏水单体来制备这种聚合物分散体的方法酸酐，如果合适的话，可以使用烷基染料，使用得到的含有链烯基琥珀酸酐的聚合物分散液作为纸张的引擎和表面尺寸，并赋予皮革，天然和/或合成纤维和纺织品防水性。

10. 发明申请

US20090178773A1 METHOD FOR PRODUCING AQUEOUS POLYMER DISPERSIONS CONTAINING AT LEAST ONE LIPOPHILIC ACTIVE SUBSTANCE AND THE USE THEREOF 失效
标题翻译：生产含有至少一种活性物质的水性聚合物分散体的方法及其用途
公开(公告)号：US20090178773A1
公开(公告)日：2009-07-16
申请号：US12305976
申请日：2007-06-05
申请人： Andreas Brockmeyer , Roland Ettl , Rainer Dyllick-Brenzinger
发明人： Andreas Brockmeyer , Roland Ettl , Rainer Dyllick-Brenzinger
IPC分类号： D21H21/16 , C08K5/1539 , C08K5/04 , C08K5/42 , C08K5/07 , C08L89/00 , C08L3/00
CPC分类号： C08F2/24 , C08F2/44
摘要： A process for the preparation of aqueous polymer dispersions comprising at least one lipophilic active substance by emulsion polymerization of ethylenically unsaturated monomers in an aqueous medium in the presence of at least one lipophilic active substance, wherein (i) at least one lipophilic active substance which has a water solubility of not more than 5 g/l (determined at 25° C. and 1013 mbar) and a melting point below 130° C. is emulsified in an aqueous solution which comprises at least one dispersion stabilizer with formation of an aqueous dispersion of the active substance having a mean particle size of not more than 1000 nm and (ii) a monomer composition which comprises at least 80% by weight of a neutral, monoethylenically unsaturated monomer emulsifiable in water is subjected to an emulsion polymerization in the aqueous dispersion of the active substance which is obtained according to (i), and use of the dispersions thus obtainable as sizes for paper, board and cardboard, for the treatment and for the stabilization of thermoplastic polymers, for material protection and for crop protection.
摘要翻译：一种制备包含至少一种亲脂性活性物质的含水聚合物分散体的方法，其通过在至少一种亲脂性活性物质存在下，在含水介质中的烯属不饱和单体的乳液聚合反应，其中（i）至少一种亲脂性活性物质，其具有将水溶解度不超过5g / l（在25℃和1013毫巴下测定）和低于130℃的熔点在含有至少一种分散稳定剂的水溶液中乳化，形成水分散体的平均粒径不大于1000nm的活性物质和（ii）包含至少80重量％的在水中可乳化的中性单烯属不饱和单体的单体组合物在水分散体中进行乳液聚合根据（i）获得的活性物质的使用，以及由此获得的分散体作为纸，纸板和纸板的尺寸，用于热塑性聚合物的处理和稳定化，用于材料保护和作物保护。

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