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1. 发明授权

US06313184B1 Expanded polypropylene resin beads and a molded article 有权
标题翻译：膨胀聚丙烯树脂珠和模塑制品
公开(公告)号：US06313184B1
公开(公告)日：2001-11-06
申请号：US09554510
申请日：2000-05-17
申请人： Hidehiro Sasaki , Masakazu Sakaguchi , Mitsuhiro Akiyama , Hisao Tokoro
发明人： Hidehiro Sasaki , Masakazu Sakaguchi , Mitsuhiro Akiyama , Hisao Tokoro
IPC分类号： C08J900
CPC分类号： C08J9/18 , C08J9/16 , C08J2203/06 , C08J2323/12
摘要： Propylene resin beads for molding expansion molded articles having improved high temperature resistance include as base resin metallocene-catalyzed copolymers of propylene with at least one or more of ethylene and ∝-olefins of 4 to 20 carbon atoms. The metallocene-catalyzed propylene copolymers are isotactic random copolymers characterized by a melting point higher than 140° C. to 160° C. and a melt flow rate (MFR) of not higher than 12 g/10 minutes, especially, 0.5 to 12 g/10 minutes. Expansion molded articles produced by expansion molding the expanded beads have a high temperature degree of deflection which is lower than that of metallocene-catalyzed propylene homopolymers and lower than that of Ziegler-Natta-catalyzed random propylene copolymers having the same comonomers and melting point.
摘要翻译：用于模塑具有改进的耐高温性的发泡模塑制品的丙烯树脂珠粒包括丙烯与至少一种或多种乙烯和4-20个碳原子的丙烯的基础树脂金属茂催化的共聚物。茂金属催化的丙烯共聚物是等温无规共聚物，其特征在于熔点高于140℃至160℃，熔体流动速率（MFR）不高于12g / 10分钟，特别是0.5-12g /10分钟。通过膨胀成型发泡珠粒产生的膨胀模制品具有高于茂金属催化的丙烯均聚物的高温度偏转，并且低于具有相同共聚单体和熔点的齐格勒 - 纳塔催化的无规丙烯共聚物。

2. 发明授权

US06077875A Foamed and expanded beads of polypropylene resin for molding 有权
标题翻译：发泡和发泡的聚丙烯树脂珠成型
公开(公告)号：US06077875A
公开(公告)日：2000-06-20
申请号：US274345
申请日：1999-03-23
申请人： Hidehiro Sasaki , Masakazu Sakaguchi , Mitsuhiro Akiyama , Hisao Tokoro
发明人： Hidehiro Sasaki , Masakazu Sakaguchi , Mitsuhiro Akiyama , Hisao Tokoro
IPC分类号： C08J9/18 , C08J9/22 , C08J9/228 , C08J9/232
CPC分类号： C08J9/18 , C08J2201/03 , C08J2203/06 , C08J2323/16
摘要： Disclosed herein are foamed and expanded beads of a polypropylene resin for molding, which comprise an uncrosslinked propylene random copolymer having a melting point of at least 140.degree. C. as a base resin, wherein the time required to attenuate an air pressure within the foamed beads applied by a pressurizing treatment with air from 1.2 kgf/cm.sup.2 (G) to 0.8 kgf/cm.sup.2 (G) under atmospheric pressure at 23.degree. C. is at least 80 minutes, and the CNI value of the foamed beads, which is defined by the following equation (1):CNI=log.sub.10 [Pw.times.Er.div.(2.24.times.D.sup.3 .times.B)](1)wherein Pw is an average weight (mg) per foamed bead, Er is a bulk expansion ratio (time) of the foamed beads, D is a cell diameter (mm) of the foamed beads, and B is a density of the base resin, is smaller than 3.80.
摘要翻译：本文公开了用于模制的聚丙烯树脂的发泡和膨胀珠粒，其包含熔点至少为140℃的未交联的丙烯无规共聚物作为基础树脂，其中减少泡沫颗粒内的空气压力所需的时间通过在大气压下在23℃下通过空气从1.2kgf / cm 2（G）至0.8kgf / cm 2（G）的加压处理施加至少80分钟，并且发泡珠粒的CNI值由以下等式（1）：CNI = log10 [PwxEr DIVIDED（2.24xD3xB）]（1）其中Pw是每个发泡珠粒的平均重量（mg），Er是发泡珠粒的体积膨胀比（时间），D是发泡粒子的孔直径（mm），B是基础树脂的密度，小于3.80。

3. 发明授权

US6051617A Foamed particles of modified polypropylene resin and method of preparing same 失效
标题翻译：改性聚丙烯树脂的发泡颗粒及其制备方法
公开(公告)号：US6051617A
公开(公告)日：2000-04-18
申请号：US904114
申请日：1997-07-31
申请人： Hidehiro Sasaki , Masakazu Sakaguchi , Hisao Tokoro
发明人： Hidehiro Sasaki , Masakazu Sakaguchi , Hisao Tokoro
IPC分类号： C08F255/02 , C08F255/04 , C08J9/18 , C08J9/20 , C08J9/22 , C08J9/224
CPC分类号： C08J9/18 , C08F255/02 , C08F255/04 , C08J2351/08
摘要： A foamed, non-crosslinked resin particle having a bulk density of not greater than 0.045 g/cm.sup.3 and an average cell diameter of at least 200 .mu.m. The non-crosslinked resin includes a polypropylene resin to which a vinyl comonomer is graft-polymerized in such an amount that the weight ratio of the polypropylene resin to the grafted polymer of the vinyl comonomer is in the range of 97:3 to 65:35. The foamed resin particles are produced by grafting a vinyl comonomer to polypropylene resin particles at a temperature of less than 90.degree. C. in the presence of a specific radical polymerization initiator to obtain modified polypropylene resin particles and, then, expanding the modified polypropylene resin particles. The initiator used requires a temperature of not higher than 70.degree. C. for obtaining a half life of 10 hours.
摘要翻译：发泡非交联树脂颗粒，其堆积密度不大于0.045g / cm 3，平均泡孔直径至少为200μm。非交联树脂包括聚乙烯基共聚单体接枝聚合的聚丙烯树脂，其量使得聚丙烯树脂与乙烯基共聚单体的接枝聚合物的重量比在97:3至65:35的范围内。发泡树脂颗粒通过在特定自由基聚合引发剂的存在下，在小于90℃的温度下将乙烯基共聚单体接枝到聚丙烯树脂颗粒上而制备，得到改性聚丙烯树脂颗粒，然后使改性聚丙烯树脂颗粒。使用的引发剂需要不高于70℃的温度以获得10小时的半衰期。

4. 发明授权

US5679450A Expanded polyolefin body having thermosetting resin layer directly bonded thereto 失效
标题翻译：具有与其直接结合的热固性树脂层的发泡聚烯烃体
公开(公告)号：US5679450A
公开(公告)日：1997-10-21
申请号：US498115
申请日：1995-07-05
申请人： Hisao Tokoro , Hidehiro Sasaki , Masakazu Sakaguchi
发明人： Hisao Tokoro , Hidehiro Sasaki , Masakazu Sakaguchi
IPC分类号： B32B5/18 , C08J9/36 , C08L23/02 , C09D167/06 , B32B9/04
CPC分类号： C08J9/365 , B32B5/18 , C08L23/02 , C08L23/06 , C09D167/06 , C08J2323/02 , C08L51/06 , Y10T428/249953 , Y10T428/249955 , Y10T428/249958 , Y10T428/24996 , Y10T428/24998 , Y10T428/254 , Y10T428/31504 , Y10T428/31536 , Y10T428/31587 , Y10T428/31794
摘要： A composite material is disclosed which comprises a shaped, expanded body having a closed cellular structure, and a layer of a thermosetting resin directly bonded to a surface of the shaped body, wherein the shaped body is formed of a mixed thermoplastic resin having a xylene-insoluble content of not greater than 1% by weight and containing at least 50% by weight of a polyolefin resin and at least 2% by weight of a polyene polymer having vinyl group-containing side chains.
摘要翻译：公开了一种复合材料，其包括具有封闭的多孔结构的成形的膨胀体和直接结合到成形体的表面的热固性树脂层，其中，所述成形体由具有二甲苯结构的混合热塑性树脂形成，不溶物含量不大于1重量％，含有至少50重量％的聚烯烃树脂和至少2重量％的含乙烯基侧链的多烯聚合物。

5. 发明授权

US07560498B2 Process of producing foamed molding from expanded polypropylene resin beads and process of producing expanded polypropylene resin beads 有权
标题翻译：由发泡聚丙烯树脂珠制造发泡成型体的方法和生产发泡聚丙烯树脂珠的方法
公开(公告)号：US07560498B2
公开(公告)日：2009-07-14
申请号：US11332342
申请日：2006-01-17
申请人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro
发明人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro
IPC分类号： C08J9/16
CPC分类号： C08J9/224 , C08J9/18 , C08J2323/12
摘要： A process of producing a foamed molding, wherein expanded, substantially non-crosslinked polypropylene-based resin beads are heated in a mold to fuse-bond the beads together into a unitary body. Each of the expanded beads has been surface-modified with an organic peroxide.
摘要翻译：制造发泡模制品的方法，其中将膨胀的基本上未交联的聚丙烯基树脂珠粒在模具中加热，以将珠子熔合在一起成为整体。每个发泡珠粒都用有机过氧化物进行表面改性。

6. 发明授权

US5459169A Uncrosslinked polyethylene particles for the production of expanded particles and uncrosslinked polyethylene expanded particles 失效
公开(公告)号：US5459169A
公开(公告)日：1995-10-17
申请号：US208677
申请日：1994-03-11
申请人： Hisao Tokoro , Kazuo Tsurugai , Hidehiro Sasaki , Masaharu Oikawa
发明人： Hisao Tokoro , Kazuo Tsurugai , Hidehiro Sasaki , Masaharu Oikawa
IPC分类号： C08J9/18 , C08J9/22 , C08L23/06 , C08L23/08 , C08J9/16
CPC分类号： C08L23/0815 , C08J9/18 , C08J2323/06 , C08L2205/02 , C08L2205/03 , C08L23/06
摘要： The present invention relates to uncrosslinked polyethylene particles for the production of expanded particles that can easily and securely produce expanded particles which can be molded without applying a special internal pressure, are excellent in moldability, such as secondary expansion, fusion and dimensional accuracy, and have a high expansion rate and to uncrosslinked polyethylene expanded particles made of said uncrosslinked polyethylene particles. The present uncrosslinked polyethylene particles for the production of expanded particles are resin particles whose base resin is an uncrosslinked polyethylene having a density of over 0.920 g/cm.sup.3 and up to and including 0.940 g/cm.sup.3 and wherein, in the DSC curve that is obtained by using a differential scanning calorimeter in such a manner that after 1 to 10 mg of the resin particles is heated to 200.degree. C. at 10.degree. C./min and then is cooled to room temperature at 10.degree. C./min, heating is again carried out to 200.degree. C. at 10.degree. C./min and during the second heating the measurement for the DSC curve is carried out, q.sub.1 /q.sub.total .gtoreq.0.5 wherein q.sub.1 stands for the quantity of heat absorbed in the range of the DSC curve of from 50.degree. C. to (the melting point-10) .degree. C. in terms of J/g and q.sub.total stands for the total quantity of absorbed heat of the DSC curve of from 50.degree. C. to the temperature at which the melting is completed in terms of J/g is satisfied, and the temperature width at 1/2 of the peak height h of the endothermic peak whose apex is at 115.degree. C. or higher is 5.degree. C. or more. Further, the present uncrosslinked polyethylene expanded particles are obtained by impregnating the above resin particles with an expanding agent, dispersing the resin particles in a dispersing agent in a closed vessel, and discharging the resin particles and the dispersing medium from the vessel at a temperature equal to or over the softening temperature of the resin particles into a low-pressure region.

7. 发明授权

US07671820B2 Luneberg dielectric lens and method of producing same 有权
标题翻译： Luneberg介电透镜及其制造方法
公开(公告)号：US07671820B2
公开(公告)日：2010-03-02
申请号：US11662262
申请日：2005-09-08
申请人： Hisao Tokoro , Kazutoshi Sasaki , Mitsuru Shinohara , Masakazu Sakaguchi , Masatoshi Kuroda , Koichi Kimura , Yoshiyuki Ishibashi
发明人： Hisao Tokoro , Kazutoshi Sasaki , Mitsuru Shinohara , Masakazu Sakaguchi , Masatoshi Kuroda , Koichi Kimura , Yoshiyuki Ishibashi
IPC分类号： H01Q25/00
CPC分类号： C04B38/06 , C04B2111/00939 , H01Q15/08 , H01Q19/062 , C04B14/4637 , C04B26/02
摘要： A hemispherical Luneberg dielectric lens including a hemispherical center layer having a hemispherical outer surface, and a plurality of hemispherical dome-shaped layers each having concentric hemispherical inner and outer surfaces, the outer surfaces of the center layer and dome-shaped layers having different diameters and the inner surfaces of said dome-shaped layers having different diameters. The center layer and dome-shaped layers are successively concentrically fitted into one another and integrated into a hemispherical shape. The center layer is a foam molding of ceramic-containing thermoplastic resin expanded beads, while each of said dome-shaped layers is a foam molding of thermoplastic resin expanded beads containing 0 to 80% by weight of a ceramic. The ceramic content per unit volume of the center and dome-shaped layers decreases from the center layer to the outermost dome-shaped layer, and the standard deviation of the apparent density of each of the center and dome-shaped layers is 0.07 g/cm3 or lower.
摘要翻译：一种半球形Luneberg介质透镜，包括具有半球形外表面的半球形中心层和多个具有同心半球形内表面和外表面的半球形圆顶形层，中心层和圆顶形层的外表面具有不同的直径和所述圆顶形的层的内表面具有不同的直径。中心层和圆顶形的层被相继地同心地装配在一起并整合为半球形。中心层是含有陶瓷的热塑性树脂发泡珠的发泡成型体，而每个所述圆顶形层是含有0至80重量％陶瓷的热塑性树脂发泡珠的发泡成型体。中心层和圆顶形层的单位体积的陶瓷含量从中心层到最外面的圆顶状层减少，中心圆顶形层的表观密度的标准偏差为0.07g / cm 3 或更低。

8. 发明申请

US20080191952A1 Luneberg Dielectric Lens and Method of Producing Same 有权
标题翻译： Luneberg介质透镜及其制作方法
公开(公告)号：US20080191952A1
公开(公告)日：2008-08-14
申请号：US11662262
申请日：2005-09-08
申请人： Hisao Tokoro , Kazutoshi Sasaki , Mitsuru Shinohara , Masakazu Sakaguchi , Masatoshi Kuroda , Koichi Kimura , Yoshiyuki Ishibashi
发明人： Hisao Tokoro , Kazutoshi Sasaki , Mitsuru Shinohara , Masakazu Sakaguchi , Masatoshi Kuroda , Koichi Kimura , Yoshiyuki Ishibashi
IPC分类号： H01Q19/06
CPC分类号： C04B38/06 , C04B2111/00939 , H01Q15/08 , H01Q19/062 , C04B14/4637 , C04B26/02
摘要： A hemispherical Luneberg dielectric lens including a hemispherical center layer having a hemispherical outer surface, and a plurality of hemispherical dome-shaped layers each having concentric hemispherical inner and outer surfaces, the outer surfaces of the center layer and dome-shaped layers having different diameters and the inner surfaces of said dome-shaped layers having different diameters. The center layer and dome-shaped layers are successively concentrically fitted into one another and integrated into a hemispherical shape. The center layer is a foam molding of ceramic-containing thermoplastic resin expanded beads, while each of said dome-shaped layers is a foam molding of thermoplastic resin expanded beads containing 0 to 80% by weight of a ceramic. The ceramic content per unit volume of the center and dome-shaped layers decreases from the center layer to the outermost dome-shaped layer, and the standard deviation of the apparent density of each of the center and dome-shaped layers is 0.07 g/cm3 or lower
摘要翻译：一种半球形Luneberg介质透镜，包括具有半球形外表面的半球形中心层和多个具有同心半球形内表面和外表面的半球形圆顶形层，中心层和圆顶形层的外表面具有不同的直径和所述圆顶形的层的内表面具有不同的直径。中心层和圆顶形的层被相继地同心地装配在一起并整合为半球形。中心层是含有陶瓷的热塑性树脂发泡珠的发泡成型体，而每个所述圆顶形层是含有0至80重量％陶瓷的热塑性树脂发泡珠的发泡成型体。中心层和圆顶形层的单位体积的陶瓷含量从中心层到最外面的圆顶状层减少，中心圆顶形层的表观密度的标准偏差为0.07g / cm 3 或更低

9. 发明授权

US07531116B2 Process of producing foamed molding from expanded polypropylene resin beads 失效
标题翻译：从发泡聚丙烯树脂珠生产发泡成型的方法
公开(公告)号：US07531116B2
公开(公告)日：2009-05-12
申请号：US10493502
申请日：2002-10-31
申请人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro , Mitsuru Shinohara , Tomoo Tokiwa
发明人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro , Mitsuru Shinohara , Tomoo Tokiwa
IPC分类号： B29C44/00
CPC分类号： C08J9/224 , C08J9/18 , C08J2323/12
摘要： A process of producing a foamed molding, wherein expanded, substantially non-crosslinked polypropylene-based resin beads are heated in a mold to fuse-bond the beads together into a unitary body. Each of the expanded beads has been surface-modified with an organic peroxide.
摘要翻译：制造发泡模制品的方法，其中将膨胀的基本上未交联的聚丙烯基树脂珠粒在模具中加热，以将珠子熔合在一起成为整体。每个发泡珠粒都用有机过氧化物进行表面改性。

10. 发明授权

US06956067B2 Expanded polypropylene resin bead and process of producing same 失效
标题翻译：膨胀聚丙烯树脂珠及其生产方法
公开(公告)号：US06956067B2
公开(公告)日：2005-10-18
申请号：US10379569
申请日：2003-03-06
申请人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro
发明人： Hidehiro Sasaki , Akinobu Hira , Keiichi Hashimoto , Hisao Tokoro
IPC分类号： C08J9/224 , C08L23/10 , C08J9/16
CPC分类号： C08J9/224 , C08J2323/10 , C08L23/10 , C08L2203/14 , Y10T428/25 , Y10T428/2991
摘要： Expanded, substantially non-crosslinked polypropylene resin beads capable of producing a high rigidity foamed molding at a relatively low temperature. The beads are produced by a process including a step of dispersing substantially non-crosslinked polypropylene resin particles in a dispersing medium containing an organic peroxide to obtain a dispersion, a step of heating the dispersion to decompose the organic peroxide and to modify the surface of the surface-modified polypropylene resin particles, and a step of expanding the non-crosslinked, surface-modified polypropylene resin particles using a blowing agent.
摘要翻译：膨胀的基本上非交联的聚丙烯树脂珠，其能够在相对低的温度下生产高刚性的发泡成型体。珠粒通过包括将基本上未交联的聚丙烯树脂颗粒分散在含有机过氧化物的分散介质以获得分散体的步骤的方法制备，加热分散体以分解有机过氧化物并改性表面的步骤表面改性聚丙烯树脂颗粒，以及使用发泡剂使未交联的表面改性聚丙烯树脂颗粒膨胀的步骤。

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