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1. 发明授权

US4209461A Process for the production of benzoyl cyanide (I) 失效
标题翻译：苯甲酰氰（I）的制备方法
公开(公告)号：US4209461A
公开(公告)日：1980-06-24
申请号：US965691
申请日：1978-12-01
申请人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
发明人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
IPC分类号： C07B61/00 , B01J31/00 , B01J31/02 , C07C20060101 , C07C63/06 , C07C67/00 , C07C253/00 , C07C253/14 , C07C255/40 , C07C255/56
CPC分类号： C07C253/14
摘要： The process described in Klenk U.S. Pat. No. 4,113,773 is improved by employing alkali metal cyanide in which at least half of the alkali metal cyanide has a particle size below 0.4 mm and the remainder has a particle size below 1.0 mm.
摘要翻译： Klenk美国专利中描述的方法碱金属氰化物其中至少一半的碱金属氰化物的粒度小于0.4mm，其余的粒径小于1.0mm，改善了No.4,113,773。

2. 发明授权

US4144269A Process for the production of benzoyl cyanide (IV) 失效
标题翻译：生产苯甲酰氰（IV）的方法
公开(公告)号：US4144269A
公开(公告)日：1979-03-13
申请号：US802943
申请日：1977-06-02
申请人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
发明人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
IPC分类号： C07B61/00 , B01J31/00 , B01J31/02 , C07C20060101 , C07C51/54 , C07C67/00 , C07C253/00 , C07C253/14 , C07C255/33 , C07C255/40 , C07C255/50 , C07C255/56 , C07C120/00
CPC分类号： C07C253/14
摘要： Benzoyl cyanide is made from benzoyl chloride and an alkali metal cyanide in a two phase system comprising water and an inert organic solvent which has only slight miscibility with water in the presence of a tertiary amine and hydrogen cyanide.
摘要翻译：苯甲酰氰由含有水和惰性有机溶剂的两相体系中的苯甲酰氯和碱金属氰化物制成，其在叔胺和氰化氢的存在下与水仅具有轻微的混溶性。

3. 发明授权

US4113773A Process for the production of benzoyl cyanide (I) 失效
标题翻译：苯甲酰氰（I）的制备方法
公开(公告)号：US4113773A
公开(公告)日：1978-09-12
申请号：US802946
申请日：1977-06-20
申请人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
发明人： Herbert Klenk , Theodor Lussling , Alfred Maierhofer , Heribert Offermanns , Hans Wagner
IPC分类号： C07C255/40 , C07C20060101 , C07C63/06 , C07C67/00 , C07C253/00 , C07C253/14 , C07C255/56
CPC分类号： C07C253/14
摘要： Benzoyl cyanide is made by reacting benzoyl chloride with an alkali cyanide in the presence of a carboxylic acid nitrile and a copper (I) salt at a temperature of about 50.degree. to 160.degree. C.
摘要翻译：在羧酸腈和铜（I）盐存在下，在约50°至160℃的温度下，使苯甲酰氯与碱金属氰化物反应制备苯甲酰氰。

4. 发明授权

US4283337A Process for the purification of tryptophane and derivatives of tryptophane 失效
标题翻译：色氨酸和色氨酸衍生物的纯化方法
公开(公告)号：US4283337A
公开(公告)日：1981-08-11
申请号：US94801
申请日：1979-11-15
申请人： Theodor Lussling , Alfred Maierhofer , Paul Scherberich
发明人： Theodor Lussling , Alfred Maierhofer , Paul Scherberich
IPC分类号： C07D209/20
CPC分类号： C07D209/20
摘要： Tryptophane and tryptophane derivatives are purified by treating them in an inert solvent at a temperature between about 20.degree. C. and the boiling point of the mixture with a salt of dithionous acid. Preferably there is used as solvent a mixture of water and a lower aliphatic carboxylic acid. Normally a single treatment results in a pure, colorless, satisfactory product.
摘要翻译：色氨酸和色氨酸衍生物通过在惰性溶剂中在约20℃和混合物与二硫酸盐的沸点之间的温度下处理来纯化。优选地，作为溶剂使用水和低级脂肪族羧酸的混合物。通常单次处理会产生纯净，无色，令人满意的产品。

5. 发明授权

US3931307A Process for the stabilization of methionine 失效
标题翻译：甲硫氨酸稳定化方法
公开(公告)号：US3931307A
公开(公告)日：1976-01-06
申请号：US420574
申请日：1973-11-30
申请人： Gerd Eikelmann , Rudolf Fahnenstich , Theodor Lussling , Sven-Peter Mannsfeld , Gerhard Pohl , Herbert Tanner , Hans Wagner
发明人： Gerd Eikelmann , Rudolf Fahnenstich , Theodor Lussling , Sven-Peter Mannsfeld , Gerhard Pohl , Herbert Tanner , Hans Wagner
IPC分类号： C07C319/26 , C07C20060101 , C07C67/00 , C07C313/00 , C07C323/58 , C07C149/247
CPC分类号： C07C227/40
摘要： Methionine is stabilized by adjusting the pH to the range from 3 to
摘要翻译：通过将pH调节至3至5的范围来稳定甲硫氨酸。乙内酰脲的来源优选为5-（β-甲基巯基乙基） - 乙内酰脲。

6. 发明授权

US4003983A Process of preparing dicyan 失效
标题翻译：制备二氰的过程
公开(公告)号：US4003983A
公开(公告)日：1977-01-18
申请号：US543367
申请日：1975-01-23
申请人： Johannes Heilos , Werner Heimberger , Theodor Lussling , Wolfgang Weigert
发明人： Johannes Heilos , Werner Heimberger , Theodor Lussling , Wolfgang Weigert
IPC分类号： B01J19/00 , C01C3/00
CPC分类号： C01C3/003 , B01J19/002
摘要： Cyanogen is prepared by passing hydrogen cyanide together with hydrogen peroxide into a solution of copper(II) bromide, chloride, cyanide, nitrate, or sulfate containing ferric ions that is maintained at a temperature between 0.degree. and 100.degree. C.
摘要翻译：通过将氰化氢与过氧化氢一起通入氯化铜（II），氯化物，氰化物，硝酸盐或含有铁离子的硫酸盐溶液中，将其保持在0℃至100℃的温度下制备氰氰。

7. 发明授权

US4550200A Process for obtaining D,L-homocystine (II) 失效
标题翻译：获得D，L-高胱氨酸（II）的方法
公开(公告)号：US4550200A
公开(公告)日：1985-10-29
申请号：US590059
申请日：1984-03-15
申请人： Michael Karrenbauer , Axel Kleemann , Theodor Lussling , Fritz Schafer
发明人： Michael Karrenbauer , Axel Kleemann , Theodor Lussling , Fritz Schafer
IPC分类号： C07C319/24 , C07C67/00 , C07C313/00 , C07C323/58 , C07C149/243
CPC分类号： C07C319/12
摘要： D,L-Homocystine is obtained by introducing molecular oxygen into an aqueous solution of the disodium salt of D,L-homocysteine having a concentration between 0.8 and 1.2 moles/l and an initial pH between 7.0 and 8.0 in the presence of a catalytic amount of iron(III) ions until there is no longer an increase in pH and subsequently adjusting the pH to about 5.3 with stirring.
摘要翻译：通过将分子氧引入浓度在0.8和1.2摩尔/升之间的D，L-高半胱氨酸的二钠盐水溶液中，并且在催化量存在下将初始pH值介于7.0和8.0之间，得到D，L-高等胱氨酸的铁（III）离子，直到pH不再增加，随后在搅拌下将pH调节至约5.3。

8. 发明授权

US4136108A Process for the production of malononitrile 失效
标题翻译：生产马鞭草的方法
公开(公告)号：US4136108A
公开(公告)日：1979-01-23
申请号：US294925
申请日：1972-10-04
申请人： Theodor Lussling , Ferdinand Theissen , Wolfgang Weigert
发明人： Theodor Lussling , Ferdinand Theissen , Wolfgang Weigert
IPC分类号： C07C121/22 , C07C120/00
CPC分类号： C07C255/00
摘要： Malononitrile is prepared by the short time high temperature reaction of gaseous acetonitrile and cyanogen chloride in the molar ratio of acetonitrile to cyanogen halide of above 1 characterized in that the well mixed reaction components are reacted at an average temperature below 800.degree. C. and the reaction is quenched to condense acetonitrile and malononitrile by introducing a cooling medium into the reaction system.

9. 发明授权

US4038276A Process for the production of finely divided solid cyanuric chloride 失效
标题翻译：生产精细分散固体氰基氯化物的方法
公开(公告)号：US4038276A
公开(公告)日：1977-07-26
申请号：US716353
申请日：1976-08-20
申请人： Friedhelm Geiger , Werner Heimberger , Theodor Lussling
发明人： Friedhelm Geiger , Werner Heimberger , Theodor Lussling
IPC分类号： C07D251/28
CPC分类号： C07D251/28
摘要： Finely divided solid cyanuric chloride is produced by feeding a jet of liquid cyanuric chloride into a separatory container, cooling the liquid cyanuric chloride with recycling inert gases to such an extent that the cyanuric chloride is separated in crystalline form, washing the thereby warmed cyanuric chloride vapor or dust containing gases free of cyanuric chloride in countercurrent flow with an inert liquid that is a good solvent for cyanuric chloride in a washing column connected to the outlet side of the separatory column, thus simultaneously cooling the gases, and subsequently again returning the gases to the separatory container, while the temperature of the cyanuric chloride containing washing liquid which has increased in the washing process is again brought to the original temperature by leading it in the cycle over a heat exchanger and spraying the inside of the pipe connected to the separatory container and leading to the washing column constantly with the washing liquid while dividing a partial stream of the cyanuric chloride containing washing liquid in a distillation column into pure liquid cyanuric chloride which is recycled into the separatory column and into pure washing liquid which is recycled into the washing column.

10. 发明授权

US4550199A Process for obtaining D,L-homocystine (I) 失效
标题翻译：获得D，L-高胆固醇（I）的方法
公开(公告)号：US4550199A
公开(公告)日：1985-10-29
申请号：US590058
申请日：1984-03-15
申请人： Michael Karrenbauer , Axel Kleemann , Theodor Lussling , Fritz Schafer
发明人： Michael Karrenbauer , Axel Kleemann , Theodor Lussling , Fritz Schafer
IPC分类号： C07C319/24 , C07C67/00 , C07C313/00 , C07C323/58 , C07C149/243
CPC分类号： C07C319/24
摘要： D,L-Homocystine is obtained by treating an aqueous solution of the disodium salt of D,L-homocysteine having a concentration between 0.4 and 1.6 moles/l and an initial pH between 7.0 and 8.0 under vigorous stirring with at least the equivalent amount of an aqueous solution of hydrogen peroxide and after the end of the oxidation adjusting the pH to about 5.3. The hydrogen peroxide solution can be employed with a concentration between 20 and 60 weight percent.
摘要翻译： D，L-高密半胱氨酸通过在剧烈搅拌下处理浓度为0.4〜1.6摩尔/升的D，L-高半胱氨酸的二钠盐水溶液，并在至少等量的过氧化氢水溶液，氧化结束后将pH调节至约5.3。过氧化氢溶液可以使用浓度在20至60重量％之间。

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