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1. 发明申请

US20160000077A1 2-Mercaptobenzothiazole Manganese Zinc, Preparation Method Therefor And Application Thereof 有权
标题翻译： 2-巯基苯并噻唑锰锌，其制备方法及应用
公开(公告)号：US20160000077A1
公开(公告)日：2016-01-07
申请号：US14653654
申请日：2013-11-30
申请人： HENAN XINXIANG ACADEMY OF AGRICULTURE SCIENCES
发明人： Zhenjun Wang , Xu Zhang , Limin Wang , Hongyan Liu , Senxiang Cheng , Mengjiao Li
IPC分类号： A01N43/78 , C07D277/72
CPC分类号： C07D277/72 , A01N43/78 , A01N59/16 , C07D277/70 , Y02A50/359 , A01N2300/00
摘要： The present invention belongs to the technical field of agricultural fungicides and discloses a 2-mercaptobenzothiazole manganese zinc, preparation method therefor and application thereof. The chemical structure of the 2-mercaptobenzothiazole manganese zinc is shown as the above formula. Wherein m, n and n′ are positive integers, m=2(n+n′), n≧n′, n:n′=1:1˜9:1. Materials are prepared according to the stoichiometric ratio of the target products; 2-mercaptobenzothiazole is dissolved in sodium hydroxide solution. The aqueous solution of water-soluble manganese salts and water-soluble zinc salts solution are successively added to 2-mercaptobenzothiazole sodium solution under stirring, followed by stirring for mixing well, then the solution being allowed to stand, filtered and washed with water to obtain filter cake, and then dried in vacuum to obtain 2-mercaptobenzothiazole manganese zinc. The present 2-mercaptobenzothiazole manganese zinc may be used as an agricultural fungicide. The present invention coordinates the surface of solid particles of 2-mercaptobenzothiazole manganese with zinc to form a stable clathrate of 2-mercaptobenzothiazole manganese and zinc. Tests show that the clathrate has excellent effect for controlling a plurality of diseases including apple alternaria leaf spot, pear scab, apple ring rot, apple anthracnose and the like.
摘要翻译：本发明属于农药杀菌剂的技术领域，公开了2-巯基苯并噻唑锰锌，其制备方法及应用。 2-巯基苯并噻唑锰锌的化学结构如上式所示。其中m，n和n'为正整数，m = 2（n + n'），n≥n'，n：n'= 1：1〜9：1。材料根据目标产品的化学计量比制备; 将2-巯基苯并噻唑溶解在氢氧化钠溶液中。将水溶性锰盐和水溶性锌盐溶液的水溶液在搅拌下依次加入到2-巯基苯并噻唑钠溶液中，搅拌均匀，然后静置，过滤并用水洗涤，得到滤饼，然后真空干燥，得到2-巯基苯并噻唑锰锌。本发明的2-巯基苯并噻唑锰锌可用作农业杀真菌剂。本发明用锌与2-巯基苯并噻唑锰的固体颗粒表面配位，形成稳定的2-巯基苯并噻唑锰和锌的包合物。试验结果表明，包合物对苹果叶斑病，梨痂病，苹果腐烂，苹果炭疽病等多种疾病的控制效果优异。

2. 发明授权

US09499501B2 2-Mercaptobenzothiazole manganese zinc, preparation method therefor and application thereof 有权
标题翻译： 2-巯基苯并噻唑锰锌，其制备方法及其应用
公开(公告)号：US09499501B2
公开(公告)日：2016-11-22
申请号：US14653654
申请日：2013-11-30
申请人： Henan Xinxiang Academy of Agriculture Sciences
发明人： Zhenjun Wang , Xu Zhang , Limin Wang , Hongyan Liu , Senxiang Cheng , Mengjiao Li
IPC分类号： C07D277/72 , C07D277/70 , A01N43/78 , A01N59/16
CPC分类号： C07D277/72 , A01N43/78 , A01N59/16 , C07D277/70 , Y02A50/359 , A01N2300/00
摘要： The present invention belongs to the technical field of agricultural fungicides and discloses a 2-mercaptobenzothiazole manganese zinc, preparation method therefor and application thereof. The chemical structure of the 2-mercaptobenzothiazole manganese zinc is shown as the above formula. Wherein m, n and n′ are positive integers, m=2(n+n′), n≧n′, n:n′=1:1˜9:1. Materials are prepared according to the stoichiometric ratio of the target products; 2-mercaptobenzothiazole is dissolved in sodium hydroxide solution. The aqueous solution of water-soluble manganese salts and water-soluble zinc salts solution are successively added to 2-mercaptobenzothiazole sodium solution under stirring, followed by stirring for mixing well, then the solution being allowed to stand, filtered and washed with water to obtain filter cake, and then dried in vacuum to obtain 2-mercaptobenzothiazole manganese zinc. The present 2-mercaptobenzothiazole manganese zinc may be used as an agricultural fungicide. The present invention coordinates the surface of solid particles of 2-mercaptobenzothiazole manganese with zinc to form a stable clathrate of 2-mercaptobenzothiazole manganese and zinc. Tests show that the clathrate has excellent effect for controlling a plurality of diseases including apple alternaria leaf spot, pear scab, apple ring rot, apple anthracnose and the like.
摘要翻译：本发明属于农药杀菌剂的技术领域，公开了2-巯基苯并噻唑锰锌，其制备方法及应用。 2-巯基苯并噻唑锰锌的化学结构如上式所示。其中m，n和n'为正整数，m = 2（n + n'），n≥n'，n：n'= 1：1〜9：1。材料根据目标产品的化学计量比制备; 将2-巯基苯并噻唑溶解在氢氧化钠溶液中。将水溶性锰盐和水溶性锌盐溶液的水溶液在搅拌下依次加入到2-巯基苯并噻唑钠溶液中，搅拌均匀，然后静置，过滤并用水洗涤，得到滤饼，然后真空干燥，得到2-巯基苯并噻唑锰锌。本发明的2-巯基苯并噻唑锰锌可用作农业杀真菌剂。本发明用锌与2-巯基苯并噻唑锰的固体颗粒表面配位，形成稳定的2-巯基苯并噻唑锰和锌的包合物。试验结果表明，包合物对苹果叶斑病，梨痂病，苹果腐烂，苹果炭疽病等多种疾病的控制效果优异。

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