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1. 发明授权

US5494941A Preparation of chlorofluorocarbon-free flexible polyurethane foams using diphenylmethane diisocyanate-based polyisocyanate mixtures containing urethane groups, and modified polyisocyanate mixtures of the type 失效
标题翻译：使用含有氨基甲酸酯基团的二苯基甲烷二异氰酸酯基聚异氰酸酯混合物和类型的改性多异氰酸酯混合物制备不含氟氯化碳的柔性聚氨酯泡沫体
公开(公告)号：US5494941A
公开(公告)日：1996-02-27
申请号：US15746
申请日：1993-02-10
申请人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
发明人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
IPC分类号： C08G18/10 , C08G18/12 , C08G18/40 , C08G18/48 , C08G18/65 , C08G18/72 , C08G18/76 , C08G101/00 , C08J9/02 , C08G18/00
CPC分类号： C08G18/7664 , C08G18/12 , C08G18/409 , C08G18/4812 , C08G2101/0008 , C08G2101/0041 , C08G2101/0083
摘要： The invention relates to a process for the preparation of CFC-free, flexible polyurethane foams or molded foams by reactingA) liquid polyisocyanate mixtures containing bonded urethane groups and having a content of NCO groups of from 20 to 30% by weight, these mixtures themselves being prepared by reacting a mixture of diphenylmethane diisocyanates and polyphenyl-polymethylene polyisocyanates (crude diphenylmethane diisocyanate) with a polyether-polyol mixture, having a hydroxyl number of from 120 to 25, of at least one polyoxypropylene glycol and at least one trifunctional polyoxypropylene-polyoxyethylene glycol having a content of ethylene oxide units of from 90 to 10% by weight or by reacting 4,4'-diphenylmethane diisocyanate (diphenylmethyl diisocyanate) or an diphenylmethane diisocyanate isomer mixture with said polyether-polyol mixture to give an NCO-containing quasi-prepolymer and diluting this quasi-prepolymer with crude diphenylmethane diisocyanate, withB) relatively high-molecular-weight polyhydroxyl compounds.
摘要翻译：本发明涉及一种制备无CFC的柔性聚氨酯泡沫或模制泡沫的方法，其通过使A）含有键合的氨基甲酸酯基团的液体多异氰酸酯混合物并且具有20至30重量％的NCO基团的含量，这些混合物本身通过使二苯基甲烷二异氰酸酯和聚苯基多亚甲基多异氰酸酯（粗二苯基甲烷二异氰酸酯）与羟基数为120至25的聚醚 - 多元醇混合物的混合物与至少一种聚氧丙烯二醇和至少一种三官能聚氧丙烯 - 聚氧乙烯乙二醇的含量为90〜10重量％的环氧乙烷单元，或通过使4,4'-二苯基甲烷二异氰酸酯（二苯基甲基二异氰酸酯）或二苯基甲烷二异氰酸酯异构体混合物与所述聚醚 - 多元醇混合物反应，得到含NCO的准 - 预聚物，并用粗二苯基甲烷二异氰酸酯稀释该准预聚物，B）相对较高小重量多羟基化合物。

2. 发明授权

US5597885A Preparation of chlorofluorocarbon-free flexible polyurethane foams using diphenylmethane diisocyanate-based polyisocyanate mixtures containing urethane groups, and modified polyisocyanate mixtures 失效
标题翻译：使用含有氨基甲酸酯基团的二苯基甲烷二异氰酸酯基聚异氰酸酯混合物和改性多异氰酸酯混合物制备不含氯氟烃的柔性聚氨酯泡沫体
公开(公告)号：US5597885A
公开(公告)日：1997-01-28
申请号：US430926
申请日：1995-06-07
申请人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
发明人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
IPC分类号： C08G18/12 , C08G18/48 , C08G18/10
CPC分类号： C08G18/4812 , C08G18/12 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： The invention relates to a process for the preparation of CFC-free, flexible polyurethane foams or molded foams by reactingA) liquid polyisocyanate mixtures containing bonded urethane groups and having a content of NCO groups of from 20 to 30% by weight, these mixtures themselves being prepared by reacting a mixture of diphenylmethane diisocyanates and polyphenyl-polymethylene polyisocyanates (crude diphenylmethane diisocyanate) with a polyether-polyol mixture, having a hydroxyl number of from 120 to 25, of at least one polyoxypropylene glycol and at least one trifunctional polyoxypropylene-polyoxyethylene glycol having a content of ethylene oxide units of from 90 to 10% by weight or by reacting 4,4'-diphenylmethane diisocyanate (diphenylmethyl diisocyanate) or an diphenylmethane diisocyanate isomer mixture with said polyether-polyol mixture to give an NCO-containing quasi-prepolymer and diluting this quasi-prepolymer with crude diphenylmethane diisocyanate, withB) relatively high-molecular-weight polyhydroxyl compounds.
摘要翻译：本发明涉及一种制备无CFC的柔性聚氨酯泡沫或模制泡沫的方法，其通过使A）含有键合的氨基甲酸酯基团的液体多异氰酸酯混合物并且具有20至30重量％的NCO基团的含量，这些混合物本身通过使二苯基甲烷二异氰酸酯和聚苯基 - 多亚甲基多异氰酸酯（粗二苯基甲烷二异氰酸酯）与羟基数为120至25的聚醚 - 多元醇混合物的混合物与至少一种聚氧丙烯二醇和至少一种三官能聚氧丙烯 - 聚氧乙烯乙二醇的含量为90〜10重量％的环氧乙烷单元，或通过使4,4'-二苯基甲烷二异氰酸酯（二苯基甲基二异氰酸酯）或二苯基甲烷二异氰酸酯异构体混合物与所述聚醚 - 多元醇混合物反应，得到含NCO的准 - 预聚物，并用粗二苯基甲烷二异氰酸酯稀释该准预聚物，B）相对较高小重量多羟基化合物。

3. 发明授权

US5596063A Preparation of chlorofluorocarbon-free flexible polyurethane foams using diphenylmethane diisocyanate-based polyisocyanate mixtures containing urethane groups, and modified polyisocyanate mixtures of this type 失效
标题翻译：使用含有氨基甲酸酯基团的二苯基甲烷二异氰酸酯基聚异氰酸酯混合物和该类型的改性多异氰酸酯混合物制备不含氟氯化碳的柔性聚氨酯泡沫体
公开(公告)号：US5596063A
公开(公告)日：1997-01-21
申请号：US430924
申请日：1995-06-08
申请人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
发明人： Heinz-Dieter Lutter , Bernd Bruchmann , Claudia Spang , Roland Minges , Dietrich Scherzer , Michael Lugmayr , Ruth Zschiesche
IPC分类号： C08G18/12 , C08G18/48 , C08G18/10
CPC分类号： C08G18/4812 , C08G18/12 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： The invention relates to a process for the preparation of CFC-free, flexible polyurethane foams or molded foams by reactingA) liquid polyisocyanate mixtures containing bonded urethane groups and having a content of NCO groups of from 20 to 30% by weight, these mixtures themselves being prepared by reacting a mixture of diphenylmethane diisocyanates and polyphenyl-polymethylene polyisocyanates (crude diphenylmethane diisocyanate) with a polyether-polyol mixture, having a hydroxyl number of from 120 to 25, of at least one polyoxypropylene glycol and at least one trifunctional polyoxypropylene-polyoxyethylene glycol having a content of ethylene oxide units of from 90 to 10% by weight or by reacting 4,4'-diphenylmethane diisocyanate (diphenylmethyl diisocyanate) or an diphenylmethane diisocyanate isomer mixture with said polyether-polyol mixture to give an NCO-containing quasi-prepolymer and diluting this quasi-prepolymer with crude diphenylmethane diisocyanate, withB) relatively high-molecular-weight polyhydroxyl compounds.
摘要翻译：本发明涉及一种制备无CFC的柔性聚氨酯泡沫或模制泡沫的方法，其通过使A）含有键合的氨基甲酸酯基团的液体多异氰酸酯混合物并且具有20至30重量％的NCO基团的含量，这些混合物本身通过使二苯基甲烷二异氰酸酯和聚苯基 - 多亚甲基多异氰酸酯（粗二苯基甲烷二异氰酸酯）与羟基数为120至25的聚醚 - 多元醇混合物的混合物与至少一种聚氧丙烯二醇和至少一种三官能聚氧丙烯 - 聚氧乙烯乙二醇的含量为90〜10重量％的环氧乙烷单元，或通过使4,4'-二苯基甲烷二异氰酸酯（二苯基甲基二异氰酸酯）或二苯基甲烷二异氰酸酯异构体混合物与所述聚醚 - 多元醇混合物反应，得到含NCO的准 - 预聚物，并用粗二苯基甲烷二异氰酸酯稀释该准预聚物，B）相对较高小重量多羟基化合物。

4. 发明授权

US5786402A Production of polyurethane foams in the presence of aminoalkyl- or aminophenylimidazoles as catalyst, and the use of these catalysts for the preparation of polyisocyanate polyaddition products 失效
标题翻译：在作为催化剂的氨基烷基 - 或氨基苯基咪唑存在下制备聚氨酯泡沫，以及这些催化剂用于制备多异氰酸酯加成产物
公开(公告)号：US5786402A
公开(公告)日：1998-07-28
申请号：US415290
申请日：1995-04-03
申请人： Bernd Bruchmann , Ruth Zschiesche , Heinz-Dieter Lutter , Claudia Spang , Werner Hinz
发明人： Bernd Bruchmann , Ruth Zschiesche , Heinz-Dieter Lutter , Claudia Spang , Werner Hinz
IPC分类号： C08J9/02 , C08G18/18 , C08G18/20 , C08J9/12
CPC分类号： C08G18/2027 , C08G18/1825 , C08G2101/00 , C08G2290/00
摘要： The invention relates to a process for the production of (flexible) polyurethane foams having reduced odor and reduced fogging values by reacting a) modified or unmodified organic polyisocyanates with b) relatively high-molecular-weight polyhydroxyl compounds and, if desired,c) low-molecular-weight chain extenders and/or crosslinking agents, in the presence of d) blowing agents, e) catalysts from the group consisting of aminoalkyl- and aminophenylimidazoles of the formula ##STR1## and, if desired, f) additives, and to the use of the aminoalkyl- and aminophenylimidazoles of the formula (I) and/or (II) as catalysts for the preparation of polyisocyanate polyaddition products.
摘要翻译：本发明涉及通过使a）改性或未改性的有机多异氰酸酯与b）相对高分子量的多羟基化合物和如果需要的话c）低的，生产具有降低的气味和降低雾化值的（柔性）聚氨酯泡沫的方法 - 分子量增链剂和/或交联剂，在d）发泡剂的存在下，e）由下式的氨基烷基 - 和氨基苯基咪唑组成的组中的催化剂：（I）＆lt; IMAGE＆gt;（II）如果需要，f）添加剂，以及使用式（I）和/或（II）的氨基烷基 - 和氨基苯基咪唑作为制备多异氰酸酯加聚产物的催化剂。

5. 发明授权

US5534185A Process for the preparation of fluorochlorohydrocarbon-free low density polyurethane soft foams and soft elastic polyurethane molding foams and polyisocyanate mixtures modified with urethane groups and diphenylmethane-diisocyanate base 失效
标题翻译：用于制备氟氯烃无低密度聚氨酯软泡沫和柔性弹性聚氨酯成型泡沫和用氨基甲酸酯基团和二苯基甲烷二异氰酸酯基改性的多异氰酸酯混合物的方法
公开(公告)号：US5534185A
公开(公告)日：1996-07-09
申请号：US310591
申请日：1994-09-21
申请人： Werner Hinz , Ruth Zschiesche , Heinz-Dieter Lutter , Bernd Bruchmann
发明人： Werner Hinz , Ruth Zschiesche , Heinz-Dieter Lutter , Bernd Bruchmann
IPC分类号： C08G18/10 , C08G18/48 , C08G18/76 , C08G18/80 , C08G18/70 , C07C249/00 , C08G18/00
CPC分类号： C08G18/8035 , C08G18/10 , C08G18/4837 , C08G18/7664 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , Y10S521/914
摘要： Method for preparation of fluorochlorohydrocarbon-free (FCHC-free) low-density polyurethane soft-foam materials and soft-elastic polyurethane soft-foam materials as well as polyisocyanate mixtures modified with urethane groups, and based on diphenylmethane-diisocyanate, which are applicable thereto.
摘要翻译：用于制备氟氯化碳（FCHC）的低密度聚氨酯软泡沫材料和软弹性聚氨酯软泡沫材料以及用氨基甲酸酯基改性的多异氰酸酯混合物和基于二苯基甲烷二异氰酸酯的方法，其适用于。

6. 发明授权

US6096238A Preparation of CFC-free, highly resilient, flexible polyurethane foams, and diphenylmethane diisocyanate-based polyisocyanate mixtures modified by means of urethane groups which can be used for this purpose 失效
标题翻译：制备无CFC，高弹性，柔性聚氨酯泡沫和通过可用于此目的的氨基甲酸酯基团改性的二苯基甲烷二异氰酸酯基多异氰酸酯混合物
公开(公告)号：US6096238A
公开(公告)日：2000-08-01
申请号：US944704
申请日：1997-10-06
申请人： Heinz-Dieter Lutter , Ruth Zschiesche , Jurgen Mertes , Bernd Bruchmann , Klaus Pittrich , Peter Brandt
发明人： Heinz-Dieter Lutter , Ruth Zschiesche , Jurgen Mertes , Bernd Bruchmann , Klaus Pittrich , Peter Brandt
IPC分类号： C08J9/02 , C08G18/00 , C08G18/08 , C08G18/10 , C08G18/40 , C08G18/48 , C08G18/72 , C08G18/76 , C08G101/00 , C08J9/14
CPC分类号： C08G18/7664 , C08G18/10 , C08G18/409 , C08G18/4812 , C08G18/4829 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： The present invention relates to a process for the preparation of CFC-free, flexible polyurethane (molded) foams by reactingA) liquid polyisocyanate mixtures containing bonded urethane groups having a content of NCO groups of from 22 to 30% by weight which are themselves prepared by reacting a mixture of diphenylmethane diisocyanates and polyphenyl-polymethylene polyisocyanates having a content of diphenylmethane diisocyanate isomers of from 55 to 99% by weight, based on the total weight, with at least one trifunctional polyoxypropylene-polyol having a hydroxyl number of from 20 to 60, withB) relatively high-molecular-weight polyhydroxyl compounds and, if desired,C) low-molecular-weight chain extenders and/or crosslinking agents,in the presence ofD) blowing agents,E) catalysts and, if desired,F) auxiliaries and/or additives,and to the polyisocyanate mixtures (A) modified by means of urethane groups which can be used according to the invention.
摘要翻译：本发明涉及一种制备无CFC的柔性聚氨酯（模制）泡沫的方法，其方法是使A）含有NCO基团含量为22-30％重量的结合氨基甲酸酯基团的液体多异氰酸酯混合物本身制备通过使二苯基甲烷二异氰酸酯和聚苯基 - 多亚甲基多异氰酸酯的混合物与二苯基甲烷二异氰酸酯异构体的含量相对于总重量为55-99重量％与至少一种羟基数为20〜20的三官能聚氧丙烯 - 多元醇反应， 60，B）相对高分子量的多羟基化合物，如果需要，C）低分子量增链剂和/或交联剂，在D）发泡剂，E）催化剂存在下，如果需要， F）助剂和/或添加剂，以及通过可根据本发明使用的氨基甲酸酯基团改性的多异氰酸酯混合物（A）。

7. 发明授权

US5374667A Process for the preparation of fluorochlorohydrocarbon-free, low-density polyurethan soft foams and soft elastic polyurethan molding foams and polyisocyanate mixtures modified with urethan groups on diphenylmethane-diisocyanate base 失效
标题翻译：用于制备氟代氯代烃，低密度聚氨酯软泡沫和柔性弹性聚氨酯成型泡沫的方法和在二苯基甲烷二异氰酸酯基础上用氨基甲酸酯基团改性的多异氰酸酯混合物
公开(公告)号：US5374667A
公开(公告)日：1994-12-20
申请号：US24589
申请日：1993-03-01
申请人： Werner Hinz , Ruth Zschiesche , Heinz-Dieter Lutter , Bernd Bruchmann
发明人： Werner Hinz , Ruth Zschiesche , Heinz-Dieter Lutter , Bernd Bruchmann
IPC分类号： C08G18/10 , C08G18/48 , C08G18/76 , C08G18/80 , C08G18/00
CPC分类号： C08G18/8035 , C08G18/10 , C08G18/4837 , C08G18/7664 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , Y10S521/914
摘要： The invention provides a method for the preparation of fluorochlorohydrocarbon(FCHC)-free polyurethane soft (molded) foam materials with low density, by reactingA) liquid polyisocyanate mixtures containing bound urethane groups, containing 22 to 30 weight percent of NCO groups, which in turn are prepared by reacting a mixture of diphenylmethane-diisocyanate and polyphenyl-polymethylene-polyisocyanates (raw MDI) with at least one polyoxypropylene-polyoxyethylene-polyol with a functionality between 2.5 and 3.5, a hydroxyl number between 50 and 90 and a polymerized ethylene oxide group concentration ranging from more than 30 to less than 50 weight percent, relative to the weight of the polymerized ethylene oxide and 1,2 propylene oxide groups, or by reacting of 4,4'diphenylmethane-diisocyanate (MDI) or and MDI-isomeric mixture with the above-named polyoxypropylene-polyoxyethylene-polyol to an NCO-group-containing quasi-prepolymer, and diluting this quasi-prepolymer with raw-MDI, withB) higher-molecular polyhydroxyl compounds and, if appropriateC) low-molecular chain lengthening and/or cross-linkage-promoting materialsD) propellants,E) catalysts as well as if appropriate,F) auxiliary materials and/or additives, as well as the polyisocyanate mixtures modified with urethane groups (A) which are utilizable in accordance with the process of the invention.
摘要翻译：本发明提供了一种通过使含有22-30％（重量）NCO基团的结合的氨基甲酸酯基团的液体多异氰酸酯混合物反应来制备低密度的氟氯烃（FCHC） - 软质（模塑）泡沫材料的方法，通过使二苯基甲烷 - 二异氰酸酯和聚苯基 - 多亚甲基多异氰酸酯（原MDI）与至少一种官能度在2.5和3.5之间，羟基数在50和90之间的聚氧化丙烯 - 聚氧乙烯 - 多元醇与聚合的环氧乙烷相对于聚合的环氧乙烷和1,2-环氧丙烷基团的重量，或通过4,4'-二苯基甲烷二异氰酸酯（MDI）或MDI异构体（MDI）的反应，组浓度范围从大于30至小于50重量％与上述聚氧丙烯 - 聚氧乙烯 - 多元醇的混合物与含有NCO基的准预聚物混合，并用B-MDI稀释该准预聚物，B）高分子量多羟基化合物，如果合适C）低分子链延长和/或交联促进材料D）推进剂，E）催化剂以及适当的F）辅助材料和/或添加剂，以及用氨基甲酸酯基团（A）改性的多异氰酸酯混合物，其可根据本发明的方法使用。

8. 发明授权

US5739173A Preparation of flame-resistant soft polyurethane foams of reduced smoke density, and melamine/expandable graphite/polyether-polyol dispersions for this purpose 失效
标题翻译：减少烟雾密度的阻燃软质聚氨酯泡沫的制备和用于此目的的三聚氰胺/可膨胀石墨/聚醚 - 多元醇分散体
公开(公告)号：US5739173A
公开(公告)日：1998-04-14
申请号：US531114
申请日：1995-09-20
申请人： Heinz-Dieter Lutter , Ruth Zschiesche , Hans-Jurgen Gabbert , Volker Hasse , Karl Fimmel
发明人： Heinz-Dieter Lutter , Ruth Zschiesche , Hans-Jurgen Gabbert , Volker Hasse , Karl Fimmel
IPC分类号： C08L75/04 , C08G18/38 , C08G18/48 , C08G18/65 , C08K3/04 , C08K3/32 , C08K5/3492 , C08K13/02 , C08G18/14
CPC分类号： C08K5/34922 , C08G18/3851 , C08G18/657 , C08K13/02 , C08K3/04 , C08K3/32 , C08G2101/0008 , C08G2101/0058
摘要： A process for the preparation of flame-resistant soft polyurethane foams which produce less smoke in the event of fire involves reacting a) an organic polyisocyanate and/or a modified organic polyisocyanate with b) a high-molecular-weight compound containing at least two reactive hydrogen atoms and, if desired, c) a chain extender and/or crosslinking agent, in the presence of d) a mixture of flameproofing agents which contains: di) melamine dii) expandable graphite and, if desired, diii) at least one further flameproofing agent, preferably a modified or unmodified ammonium polyphosphate, e) a blowing agent, f) a catalyst and, if desired, g) assistants and/or additives, and melamine/expandable graphite/polyether-polyol dispersions which are suitable for this purpose.
摘要翻译：一种制备耐火软质聚氨酯泡沫的方法，其在火灾的情况下产生较少的烟，包括使有机多异氰酸酯和/或改性的有机多异氰酸酯与b）高分子量化合物反应，所述高分子量化合物含有至少两个反应性氢原子，如果需要，c）扩链剂和/或交联剂，在d）一种防火剂的混合物的存在下，所述防火剂包含：二）三聚氰胺二）可膨胀石墨，如果需要，diii）至少另外一种防火剂，优选改性或未改性的多磷酸铵，e）发泡剂，f）催化剂，如果需要，g）助剂和/或添加剂以及适用于该目的的三聚氰胺/可膨胀石墨/聚醚 - 多元醇分散体。

9. 发明授权

US5476969A Highly reactive polyoxyalkylene-polyols containing tertiary amino groups in bonded form, their preparation, and their use for the preparation of polyisocyanate polyaddition products 失效
标题翻译：含有结合形式的叔氨基的高反应性聚氧化烯多元醇，其制备方法及其用于制备多异氰酸酯加聚物的用途
公开(公告)号：US5476969A
公开(公告)日：1995-12-19
申请号：US952376
申请日：1992-09-28
申请人： Werner Hinz , Stefan Adams , Ulrich Koehler , Christian Maletzko , Klaus Vorspohl , Ruth Zschiesche
发明人： Werner Hinz , Stefan Adams , Ulrich Koehler , Christian Maletzko , Klaus Vorspohl , Ruth Zschiesche
IPC分类号： C08G18/50 , C08G65/26 , C07C217/42
CPC分类号： C08G18/5021 , C08G65/2624 , C08G2101/0008 , C08G2101/0016 , C08G2101/0025 , C08G2101/0033 , C08G2101/0041
摘要： The invention relates to highly reactive polyoxyalkylene-polyols prepared by oxyalkylation of an initiator molecule containing, in bonded form, at least 2 reactive hydrogen atoms and at least one tertiary amino group bonded via a spacer bridge, which preferably comprises an alkylene radical having at least 3 carbon atoms, by means of at least one alkylene oxide, preferably ethylene oxide and/or 1,2-propylene oxide, to a process for the preparation of these polyoxyalkylene-polyols, and to their use for the production of compact or cellular, preferably flexible polyisocyanate polyaddition products.
摘要翻译：本发明涉及通过包含键合形式的至少2个反应性氢原子和至少一个通过间隔桥连接的叔氨基的引发剂分子的烷氧基化制备的高反应性聚氧化烯多元醇，其优选包含至少具有至少 3个碳原子，通过至少一种烯化氧，优选环氧乙烷和/或1,2-环氧丙烷与制备这些聚氧化烯 - 多元醇的方法，以及它们用于生产紧密或细胞的，优选柔性聚异氰酸酯加成产物。

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