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1. 发明授权

US5872252A Compression of ethylenically unsaturated monomers 失效
标题翻译：烯属不饱和单体的压缩
公开(公告)号：US5872252A
公开(公告)日：1999-02-16
申请号：US867041
申请日：1997-06-02
申请人： Heinz Friedrich Sutoris , Alexander Aumuller , Andreas Koch , Andreas Deckers , Eckard Schauss , Roger Klimesch , Arend Jouke Kingma , Wilhelm Weber
发明人： Heinz Friedrich Sutoris , Alexander Aumuller , Andreas Koch , Andreas Deckers , Eckard Schauss , Roger Klimesch , Arend Jouke Kingma , Wilhelm Weber
IPC分类号： C08F2/34 , C07B63/04 , C07C7/20 , C07C11/04 , C08F2/38 , C08F2/40 , C08F10/00 , C08F210/02 , C07D251/00
CPC分类号： C08F10/00 , C07B63/04 , C07C11/04 , C07C7/20 , C08F2/40 , C08F210/02
摘要： A process for compressing ethylenically unsaturated monomers at a pressure of 200-5000 bar in the absence of a polymerization initiator comprises carrying out compression in the presence of a sterically hindered amine derivative.
摘要翻译：在不存在聚合引发剂的情况下，在200-5000巴的压力下压制烯属不饱和单体的方法包括在空间位阻胺衍生物的存在下进行压缩。

2. 发明授权

US5914379A Compression of ethylenically unsaturated monomers 有权
公开(公告)号：US5914379A
公开(公告)日：1999-06-22
申请号：US174247
申请日：1998-10-16
申请人： Heinz Friedrich Sutoris , Alexander Aumuller , Andreas Koch , Andreas Deckers , Eckard Schauss , Roger Klimesch , Arend Jouke Kingma , Wilhelm Weber
发明人： Heinz Friedrich Sutoris , Alexander Aumuller , Andreas Koch , Andreas Deckers , Eckard Schauss , Roger Klimesch , Arend Jouke Kingma , Wilhelm Weber
IPC分类号： C08F2/34 , C07B63/04 , C07C7/20 , C07C11/04 , C08F2/38 , C08F2/40 , C08F10/00 , C08F210/02 , C08F10/02
CPC分类号： C08F10/00 , C07B63/04 , C07C11/04 , C07C7/20 , C08F2/40 , C08F210/02
摘要： A process for compressing ethylenically unsaturated monomers at a pressure of 200-5000 bar in the absence of a polymerization initiator comprises carrying out compression in the presence of a sterically hindered amine derivative.

3. 发明授权

US06458904B1 Catalyst for the (co)polymerization of alk-1-enes 有权
标题翻译：烷-1-烯的（共）聚合的催化剂
公开(公告)号：US06458904B1
公开(公告)日：2002-10-01
申请号：US09485767
申请日：2000-02-17
申请人： Andrei Gonioukh , Andreas Deckers , Eckard Schauss , Roger Klimesch , Wilhelm Weber
发明人： Andrei Gonioukh , Andreas Deckers , Eckard Schauss , Roger Klimesch , Wilhelm Weber
IPC分类号： C08F464
CPC分类号： C08F10/00 , C08F4/63908 , C08F4/63916 , C08F4/63922 , C08F110/02 , C08F210/16 , Y10S526/943 , C08F4/63912 , C08F2500/12 , C08F2500/03
摘要： A catalyst composition suitable for the (co)polymerization of alk-1-enes is obtainable by mixing a metallocene complex with a C3-C20-alk-1-ene in an inert solvent, reacting the resulting mixture in a controlled manner with a compound capable of forming metallocenium ions and diluting the resulting mixture with an inert nonpolar, essentially aliphatic solvent, and also, if desired, applying the catalyst composition to a particulate support material.
摘要翻译：适用于烯-1-烯的（共）聚合的催化剂组合物可通过在惰性溶剂中将茂金属配合物与C 3 -C 20烷-1-烯进行混合而获得，将所得混合物以控制的方式与化合物能够形成金属茂离子并用惰性非极性基本上脂族的溶剂稀释所得混合物，并且如果需要，将催化剂组合物施加到颗粒状载体材料上。

4. 发明授权

US06444607B1 Catalyst solution for the polymerization of &agr;-olefins 失效
标题翻译：用于α-烯烃聚合的催化剂溶液
公开(公告)号：US06444607B1
公开(公告)日：2002-09-03
申请号：US09423113
申请日：1999-11-02
申请人： Andrei Gonioukh , Eckard Schauss , Roger Klimesch , Andreas Deckers , Wilhelm Weber
发明人： Andrei Gonioukh , Eckard Schauss , Roger Klimesch , Andreas Deckers , Wilhelm Weber
IPC分类号： B01J3138
CPC分类号： C08F10/00 , C08F4/6592 , C08F4/65925 , C08F4/65927 , C08F110/02 , Y10S526/943 , C08F4/65908 , C08F2500/12 , C08F2500/03 , C08F2500/23
摘要： A catalyst solution for polymerizing &agr;-olefins is obtainable by reacting a metallocene compound with an activator compound which can react with the metallocene compound so as to displace a ligand from the central atom and stabilize the resulting cationic complex by a non-coordinating anion as an ion pair, adding one or more &agr;-olefins in a molar ratio of metallocene compound: &agr;-olefins of from 1:1 und 1:100 and mixing with at least 10 parts by volume of an aliphatic hydrocarbon.
摘要翻译：用于聚合α-烯烃的催化剂溶液可通过使茂金属化合物与可与金属茂化合物反应的活化剂化合物反应以使配位体从中心原子置换并通过非配位阴离子稳定得到的阳离子络合物得到离子对，加入一种或多种摩尔比为1：1和1：100的茂金属化合物：α-烯烃的α-烯烃，并与至少10体积份的脂族烃混合。

5. 发明授权

US5880233A Process for the preparation of ethylene/(meth)acrylic acid copolymers 失效
标题翻译：制备乙烯/（甲基）丙烯酸共聚物的方法
公开(公告)号：US5880233A
公开(公告)日：1999-03-09
申请号：US957321
申请日：1997-11-06
申请人： Andreas Deckers , Eckard Schauss , Roger Klimesch , Wilhelm Weber
发明人： Andreas Deckers , Eckard Schauss , Roger Klimesch , Wilhelm Weber
IPC分类号： C08F2/00 , C08F4/38 , C08F210/02
CPC分类号： C08F210/02
摘要： Copolymers of ethylene with .alpha.,.beta.-unsaturated carboxylic acids are prepared at from 50.degree. to 250.degree. C. and from 500 to 5000 bar in a stirred autoclave having a length/diameter ratio greater than 5:1 by a process in which the monomer mixtures are fed into the autoclave in at least two part-streams, the first part-stream being passed into the autoclave at the beginning of the autoclave pipe and the second part-stream being introduced at a position which is a distance away from the beginning which corresponds to 25-50% of the total length and the amount of the .alpha.,.beta.-unsaturated carboxylic acids in the first part-stream is from 20 to 90% less than the average amount in the further part-streams and a peroxide polymerization initiator having a lower decomposition temperature, or a mixture of peroxide polymerization initiators having a lower average decomposition temperature, than that of the initiators in the further part-streams is passed in with the first part-stream.
摘要翻译：乙烯与α，β-不饱和羧酸的共聚物在50至250℃和500至5000巴的条件下通过一种方法制备，所述搅拌高压釜的长度/直径比大于5:1，其中单体将混合物以至少两部分流进料到高压釜中，第一部分物流在高压釜管道的开始处被送入高压釜中，并且将第二部分物流引入远离开始位置的位置其对应于总长度的25-50％，并且第一部分流中的α，β-不饱和羧酸的量比另外的部分流中的平均量少20至90％，并且过氧化物聚合具有较低分解温度的引发剂或具有较低平均分解温度的过氧化物聚合引发剂的混合物比其它部分流中的引发剂的引发剂与第一部分流一起进入。

6. 发明授权

US06348547B1 Oxidized metallocene-polyolefin waxes 失效
标题翻译：氧化茂金属 - 聚烯烃蜡
公开(公告)号：US06348547B1
公开(公告)日：2002-02-19
申请号：US09171824
申请日：1998-10-27
申请人： Andreas Deckers , Arend Jouke Kingma , Ulrich Moll , Wilhelm Weber
发明人： Andreas Deckers , Arend Jouke Kingma , Ulrich Moll , Wilhelm Weber
IPC分类号： C08F806
CPC分类号： C09G1/08 , A23B7/16 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F8/06 , C08F10/02 , C08F110/02 , C08L23/30 , C08F2500/02 , C08F2500/23
摘要： Oxidized waxes are obtainable by oxidation of polyolefins obtainable by means of metallocene catalysis and having a molecular weight Mw in the range from 1000 to 40,000 g/mol.
摘要翻译：通过氧化可通过茂金属催化并且分子量Mw在1000至40,000g / mol范围内的聚烯烃获得氧化蜡。

7. 发明授权

US06350827B1 Pressurization of ethylenically unsaturated monomers 失效
标题翻译：烯属不饱和单体的加压
公开(公告)号：US06350827B1
公开(公告)日：2002-02-26
申请号：US09452451
申请日：1999-12-02
申请人： Heinz Friedrich Sutoris , Andreas Deckers , Wilhelm Weber
发明人： Heinz Friedrich Sutoris , Andreas Deckers , Wilhelm Weber
IPC分类号： C08F240
CPC分类号： C07C7/20 , C08F2/40 , C08F10/00 , C08F2/42
摘要： Disclosed is a process for pressurizing ethylenically unsaturated monomers to 200-5000 bar in the absence of a polymerization initiator, which comprises effecting said pressurizing in the presence of nitroxyl compounds of the formula I where R1 and R2 are singly C1-C4-alkyl or combine with the joining carbon atom to form a 5- or 6-membered saturated hydrocarbon ring, R3 is C1-C4-alkyl, and R4 is hydrogen or C1-C12-alkyl. Also disclosed are a process for preparing copolymers by such pressurization and subsequent polymerization and copolymers obtainable thereby.
摘要翻译：公开了一种在不存在聚合引发剂的情况下将烯属不饱和单体加压至200-5000巴的方法，其包括在式I的硝酰基化合物存在下进行所述加压，其中R 1和R 2是单C1-C4烷基或与连接碳原子以形成5-或6-元饱和烃环，R 3为C 1 -C 4 - 烷基，R 4为氢或C 1 -C 12 - 烷基。还公开了通过这种加压和随后的聚合和共聚物制备共聚物的方法从而获得。

8. 发明授权

US06509103B1 Method for coating reactors for high pressure polymerization of 1-olefins 失效
标题翻译：用于1-烯烃高压聚合反应器的涂布方法
公开(公告)号：US06509103B1
公开(公告)日：2003-01-21
申请号：US09869147
申请日：2001-06-26
申请人： Stephan Hüffer , Andreas Deckers , Wilhelm Weber , Roger Klimesch , Dieter Littmann , Jürgen Sturm , Götz Lerch
发明人： Stephan Hüffer , Andreas Deckers , Wilhelm Weber , Roger Klimesch , Dieter Littmann , Jürgen Sturm , Götz Lerch
IPC分类号： B05D722
CPC分类号： F28F19/02 , C23C18/1616 , C23C18/1662 , C23C18/36 , Y10T428/12556 , Y10T428/12944 , Y10T428/31678
摘要： A process for coating a reactor, which comprises depositing a metal layer or a metal/polymer dispersion layer on the internal surface of the reactor in an electroless manner by bringing the surfaces into contact with a metal electrolyte solution which, besides the metal electrolyte, comprises a reducing agent and optionally a halogenated polymer to be deposited in dispersed form.
摘要翻译：一种用于涂覆反应器的方法，其包括通过使金属电解质溶液与金属电解质溶液接触而以化学方式沉积在反应器内表面上的金属层或金属/聚合物分散层还原剂和任选的以分散形式沉积的卤化聚合物。

9. 发明授权

US06562915B2 Method for carrying out radical ethylene high-pressure polymerization while preventing undesired polymer deposits 有权
标题翻译：进行自由基乙烯高压聚合同时防止不期望的聚合物沉积物的方法
公开(公告)号：US06562915B2
公开(公告)日：2003-05-13
申请号：US10182563
申请日：2002-07-31
申请人： Frank-Olaf Mähling , Andreas Deckers , Dieter Littmann , Heinz Friedrich Sutoris , Kaspar Evertz
发明人： Frank-Olaf Mähling , Andreas Deckers , Dieter Littmann , Heinz Friedrich Sutoris , Kaspar Evertz
IPC分类号： C08F240
CPC分类号： C08F297/08 , C08F110/02 , C08F2/40 , C08F2/00 , C08F4/34 , C08F2/005 , C08F2500/26
摘要： In a process for the polymerization or copolymerization of ethylenically unsaturated monomers in the presence of polymerization initiators which decompose to form free radicals in a continuously operated polymerization apparatus comprising a fresh gas feed line, a precompressor, a postcompressor, a reactor, a pressure maintenance valve, a high-pressure circuit having a high-pressure product separator and a high-pressure circulation gas return line, a product valve and a low-pressure circuit having a low-pressure product separator and a low-pressure circulation gas return line, nitrogen monoxide or oxygen is introduced as inhibitor into the high-pressure circuit, into the low-pressure circuit and/or the precompressor.
摘要翻译：在用于在连续操作的聚合装置中分解形成自由基的聚合引发剂存在下烯键式不饱和单体的聚合或共聚的方法中，所述聚合引发剂包括新鲜气体进料管线，预压缩机，后压缩机，反应器，压力维持阀具有高压产品分离器和高压循环气体返回管路的高压回路，具有低压产品分离器和低压循环气体返回管路的产品阀和低压回路，氮气将一氧化碳或氧气作为抑制剂引入高压回路中，进入低压回路和/或预压缩机。

10. 发明授权

US5932684A Preparation of keto-functional polyethylene waxes 失效
标题翻译：酮官能聚乙烯蜡的制备
公开(公告)号：US5932684A
公开(公告)日：1999-08-03
申请号：US948070
申请日：1997-10-09
申请人： Andreas Deckers , Eckard Schauss
发明人： Andreas Deckers , Eckard Schauss
IPC分类号： C08F210/02 , C07C45/00
CPC分类号： C08F210/02
摘要： A process for preparing keto-functional polyethylene waxes having a molecular weight of from 150 to 1000 g/mol by telomerization of ethylene with aldehydes at from 500 to 5000 bar and from 100 to 280.degree. C., wherein ethylene and aldehyde are employed in a molar ration of from 5:1 to 50:1.
摘要翻译：通过乙烯与500-5000巴和100-280℃的醛的聚合来制备分子量为150-1000g / mol的酮官能聚乙烯蜡的方法，其中乙烯和醛用于摩尔比为5：1至50：1。

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