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1. 发明授权

US4308180A Sulfide resin for rubber 失效
标题翻译：橡胶硫化树脂
公开(公告)号：US4308180A
公开(公告)日：1981-12-29
申请号：US131788
申请日：1980-03-19
申请人： Haruki Okamura , Tetsuo Yamaguchi , Tamaki Ishii
发明人： Haruki Okamura , Tetsuo Yamaguchi , Tamaki Ishii
IPC分类号： C08L7/00 , C08G8/00 , C08G8/04 , C08G8/20 , C08G8/24 , C08G8/28 , C08G75/16 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L61/06 , C08L61/10 , C08L81/00 , C08L101/00 , C08G14/04
CPC分类号： C08G75/16 , C08G8/04 , C08G8/24 , C08G8/28 , C08L21/00 , C08L7/00 , C08L9/06 , C08K5/17 , C08K5/315 , C08K5/353
摘要： A rubber composition comprising vulcanizable natural or synthetic rubber and a sulfide resin produced by (1) reacting a component (A) with a componet (B), followed by reacting with a component (D), or (2) reacting a component (A) with a component (B), followed by reacting with a component (C) and a component (D) simultaneously or sequentially, and if desired reacting the resulting phenol resin with an acylating agent, the component (A) being a phenol compound of the following formula, and/or an acylated compound thereof, ##STR1## wherein R.sub.1 and R.sub.2 are each a hydrogen atom, a hydroxyl, carboxyl, amino, C.sub.1 -C.sub.18 alkyl, C.sub.3 -C.sub.10 cycloalkyl, C.sub.3 -C.sub.10 cycloalkenyl or C.sub.7 -C.sub.12 aralkyl group or a phenyl group unsubstituted or substituted with at least one C.sub.1 -C.sub.3 alkyl group, the component (B) being a sulfur chloride or sulfur, the component (C) being an aldehyde, and the component (D) being at lest one hydroxyaryl compound of the following formula, and/or an acylated compound thereof, ##STR2## wherein R.sub.3 is a --OR.sub.6,--NHR.sub.6, --COOR.sub.6, --OCOR.sub.6, phenyl group unsubstituted or substituted with at least one C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.18 alkyl, C.sub.3 -C.sub.10 cycloalkyl, C.sub.3 -C.sub.10 cycloalkenyl or C.sub.7 -C.sub.12 aralkyl group, and R.sub.4 and R.sub.5 are each a hydrogen atom, --OR.sub.6, --NHR.sub.6,--COOR.sub.6, --0COR.sub.6, phenyl group unsubstituted or substituted with at least one C.sub.1-C.sub.3 alkyl, C.sub.1 -C.sub.18 alkyl, C.sub.3 -C.sub.10 cycloalkyl, C.sub.3 -C.sub.10 cycloalkenyl or C.sub.7 -C.sub.12 aralkyl group in which R.sub.6 is a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group.
摘要翻译：（1）将组分（A）与组分（B）反应，然后与组分（D）反应，或（2）使组分（A）与组分（A）反应，制备包含可硫化天然或合成橡胶的橡胶组合物和硫化物树脂）与组分（B）反应，随后与组分（C）和组分（D）同时或相继反应，如果需要，使所得酚醛树脂与酰化剂反应，组分（A）为下式，和/或其酰化化合物，其中R 1和R 2各自为氢原子，羟基，羧基，氨基，C 1 -C 18烷基，C 3 -C 10环烷基，C 3 -C 10环烯基或C 7 -C 12 芳烷基或未被取代或被至少一个C 1 -C 3烷基取代的苯基，所述组分（B）为硫化氯或硫，组分（C）为醛，组分（D）为至少一个下式的羟基芳基化合物和/或其酰化化合物，其中R 1， 3是-OR 6，-NHR 6，-COOR 6，-OCOR 6，未被取代或被至少一个C 1 -C 3烷基，C 1 -C 18烷基，C 3 -C 10环烷基，C 3 -C 10环烯基或C 7 -C 12芳烷基取代的苯基，并且R 4和R 5各自为氢原子，-OR 6，-NHR 6，-COOR 6，-COR 6，未被取代或被至少一个C 1 -C 3烷基，C 1 -C 18烷基，C 3 -C 10环烷基，C 3 -C 10环烯基或其中R 6为氢原子或C 1 -C 4烷基的C 7 -C 12芳烷基。

2. 发明授权

US4739080A Purification of hydroxyphenylpropionic acid ester 失效
标题翻译：羟基苯丙酸酯的纯化
公开(公告)号：US4739080A
公开(公告)日：1988-04-19
申请号：US868742
申请日：1986-05-30
申请人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
发明人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
IPC分类号： C07D493/10 , C08K5/1575 , C07D319/04
CPC分类号： C07D493/10
摘要： Method for the purification of 3,9-bis{2-[3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propionyloxy]-1,1-dimethylethyl} -2,4,8,10-tetraoxaspiro[5.5]undecane, to form crystals having a crystalline structure which, when subjected to Cu-K.sub..alpha. X-ray diffraction, show sharp X-ray diffraction peaks at angles of diffraction, to 2.theta.=2.8.degree., 2.theta.=8.7.degree. and 2.theta.=11.7.degree., by recrystallizing the ester at a temperature lower than 40.degree. C. using as a recrystallization solvent, A C.sub.5 -C.sub.10 alicyclic hydrocarbon, which may contain a limited amount of certain other solvents, or using a mixed solvent of a C.sub.5 -C.sub.10 aliphatic hydrocarbon and at least one other certain solvent in a certain weight ratio.
摘要翻译：纯化3,9-双{2- [3-（3-叔丁基-4-羟基-5-甲基苯基）丙酰氧基] -1,1-二甲基乙基} -2,4,8,10-四氧杂螺环 [5.5]十一烷，以形成具有晶体结构的晶体，当经受Cu-Kαα射线衍射时，衍射角呈现尖锐的X射线衍射峰，为2θ= 2.8°，2θ= 8.7° 和2θ= 11.7°，通过在低于40℃的温度下使酯重结晶，使用可能含有有限量的某些其它溶剂的A C5-C10脂环族烃，或使用混合溶剂一种C 5 -C 10脂族烃和至少一种其它特定溶剂。

3. 发明授权

US4603159A Phenolic compounds and stabilizers containing the same 失效
标题翻译：酚类化合物和含有它的稳定剂
公开(公告)号：US4603159A
公开(公告)日：1986-07-29
申请号：US706165
申请日：1985-02-27
申请人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shinoya
发明人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shinoya
IPC分类号： C08K5/134 , C08K5/372 , C08K5/378 , C08K5/37
CPC分类号： C08K5/1345 , C08K5/372 , C08K5/378
摘要： Synthetic resins, such as polyolefins, are stabilized with phenolic compounds of the formula ##STR1## where n is 1 to 4 and A is ##STR2## where R.sub.1 is C.sub.1 -C.sub.3 alkyl.
摘要翻译：合成树脂，如聚烯烃，用式为“IMAGE”的酚类化合物进行稳定化，其中n为1至4，A为“IMA”，其中R 1为C 1 -C 3烷基。

4. 发明授权

US4725634A Stabilizer for synthetic resins 失效
标题翻译：合成树脂稳定剂
公开(公告)号：US4725634A
公开(公告)日：1988-02-16
申请号：US852716
申请日：1986-04-16
申请人： Tamaki Ishii , Shinichi Yachigo , Haruki Okamura , Yuzo Maegawa , Eizo Okino , Yukoh Takahashi , Hiroki Yamamoto
发明人： Tamaki Ishii , Shinichi Yachigo , Haruki Okamura , Yuzo Maegawa , Eizo Okino , Yukoh Takahashi , Hiroki Yamamoto
IPC分类号： C08K5/34 , C08K5/00 , C08K5/3412 , C08K5/3432 , C08K5/3435 , C08L1/00 , C08L7/00 , C08L21/00 , C08L23/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L67/00 , C08L77/00 , C08L101/00 , C08K5/54
CPC分类号： C08K5/3435
摘要： A stabilizer for synthetic resins containing as an effective ingredient a hindered piperidine compound represented by the general formula: ##STR1## wherein R.sub.1 represents a C.sub.1 -C.sub.18 alkyl group, R.sub.2 represents a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group, n represents an integer of 1 to 12, and C.sub.n H.sub.2n represents a straight-chain or branched alkylene group.
摘要翻译：含有作为有效成分的由通式表示的受阻哌啶化合物的合成树脂稳定剂：其中R1表示C1-C18烷基，R2表示氢原子或C1-C4烷基，n表示整数为1〜12，C n H 2n为直链或支链亚烷基。

5. 发明授权

US4719257A Polyolefin resin composition 失效
标题翻译：聚烯烃树脂组合物
公开(公告)号：US4719257A
公开(公告)日：1988-01-12
申请号：US848114
申请日：1986-04-04
申请人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shionoya
发明人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shionoya
IPC分类号： C08L23/02 , C08K5/1575 , C08L7/00 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L77/00 , C08L101/00 , C08K5/59
CPC分类号： C08K5/1575
摘要： Polyolefin resins are thermally stabilized and are also stabilized against yellowing from nitrogen oxide gases by incorporating 3,9-bis[2- 3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propionyloxy -1,1-dimethylethyl]-2,4,8,10-tetraoxaspiro[5.5]undecane.
摘要翻译：聚烯烃树脂是热稳定的，并且通过加入3,9-双[2-3-（3-叔丁基-4-羟基-5-甲基苯基）丙酰氧基-1,1-二甲基乙基] -2,4,8,10-四氧杂螺[5.5]十一烷。

6. 发明授权

US4754045A Method for producing hydroxyphenylpropionic acid ester 失效
标题翻译：羟基苯丙酸酯的制备方法
公开(公告)号：US4754045A
公开(公告)日：1988-06-28
申请号：US868100
申请日：1986-05-29
申请人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
发明人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
IPC分类号： B01J23/02 , B01J31/12 , C07B61/00 , C07D493/10 , C07D319/00
CPC分类号： C07D493/10
摘要： Method for producing 3,9-bis{2-[3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propionyloxy]-1,1-dimethylethyl}-2,4,8,10-tetraoxaspiro[5.5]undecane by ester exchange of a 3-(3-tert-butyl-4-hydroxy-5-methylphenyl)-propionic acid ester with 3,9-bis(2-hydroxy-1,1-dimethylethyl)-2,4,8,10-tetraoxaspiro[5.5]-undecane at a temperature of 170.degree.-250.degree. C. using a calcium compound as a catalyst in an amount of 0.05-1.5 moles per mole of the 3,9-bis(2-hydroxy-1,1-dimethylethyl)-2,4,8,10-tetraoxaspiro[5.5]-undecane.
摘要翻译：制备3,9-双{2- [3-（3-叔丁基-4-羟基-5-甲基苯基）丙酰氧基] -1,1-二甲基乙基} -2,4,8,10-四氧杂螺[5.5 （3-叔丁基-4-羟基-5-甲基苯基） - 丙酸酯与3,9-双（2-羟基-1,1-二甲基乙基）-2,4， 8,10-四氧杂螺[5.5] - 十一碳烷，温度为170-250℃，使用钙化合物作为催化剂，其用量为0.05-1.5摩尔/摩尔3,9-双（2-羟基 - 1,1-二甲基乙基）-2,4,8,10-四氧杂螺[5.5] - 十一烷。

7. 发明授权

US4721792A N,N',N",N'"-tetrakis(substituted benzyl)-acetylenecarbamide derivatives 失效
标题翻译： N，N'，N“，N”' - 四（取代苄基） - 乙酰甲酰胺衍生物
公开(公告)号：US4721792A
公开(公告)日：1988-01-26
申请号：US825559
申请日：1986-01-30
申请人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
发明人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
IPC分类号： C07D487/04 , C08K5/3445 , C08K5/3472 , C09K15/22 , C07D235/00
CPC分类号： C07D487/04 , C08K5/3445
摘要： There are provided acetylenecarbamide derivatives of the formula: ##STR1## wherein A represents ##STR2## in which R.sub.1 represents a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group, and R.sub.2 represents a C.sub.2 -C.sub.9 alkyl group. These derivatives are useful as stabilizers for polymeric organic substances susceptible to thermal and oxygen-induced degradation.
摘要翻译：提供下式的乙炔卡巴酰胺衍生物：其中A代表“IMAGE”，其中R1代表氢原子或C1-C4烷基，R2代表C2-C9烷基。这些衍生物可用作对热和氧诱导的降解敏感的聚合物有机物质的稳定剂。

8. 发明授权

US4670489A Piperidine derivatives, their production and use as stabilizers 失效
标题翻译：哌啶衍生物，其生产和用作稳定剂
公开(公告)号：US4670489A
公开(公告)日：1987-06-02
申请号：US805298
申请日：1985-12-05
申请人： Yukoh Takahashi , Tatsuo Kaneoya , Eizo Okino , Yuzo Maegawa , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
发明人： Yukoh Takahashi , Tatsuo Kaneoya , Eizo Okino , Yuzo Maegawa , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
IPC分类号： C07D211/46 , C08K5/00 , C08K5/34 , C08K5/3412 , C08K5/3432 , C08K5/3435 , C08L1/00 , C08L7/00 , C08L21/00 , C08L23/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L67/00 , C08L77/00 , C08L101/00 , C09K15/30 , C07D401/12
CPC分类号： C07D211/46 , C09K15/30
摘要： The present invention relates to a piperidine derivative represented by the general formula (I), ##STR1## wherein R.sub.1 is a uni- or divalent carboxylic acid residue, R.sub.2 is a hydrogen atom or a C.sub.1 -C.sub.3 alkyl or C.sub.1 -C.sub.18 acyl group, l is an integer of 1 to 3 and n is 1 or 2,its production and a stabilizer for organic substances containing it as an effective ingredient.
摘要翻译：本发明涉及由通式（I）表示的哌啶衍生物，其中R 1为单或二价羧酸残基，R 2为氢原子或C 1 -C 3烷基或C 1 -C 18 酰基，l为1〜3的整数，n为1或2，其生产和含有有机物质的稳定剂作为有效成分。

9. 发明授权

US4576734A Stabilizer for synthetic resins 失效
标题翻译：合成树脂稳定剂
公开(公告)号：US4576734A
公开(公告)日：1986-03-18
申请号：US712230
申请日：1985-03-15
申请人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Masahisa Shionoya , Haruki Okamura
发明人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Masahisa Shionoya , Haruki Okamura
IPC分类号： C08K5/00 , C08K5/1575 , C08K5/37 , C08K5/372 , C08K5/378 , C08L7/00 , C08L21/00 , C08L23/00 , C08L51/00 , C08L51/02 , C08L101/00 , C09K15/14 , C08K5/11
CPC分类号： C08K5/372 , C08K5/1575 , C08K5/378
摘要： A stabilizer for synthetic resins containing as an effective component a mixture comprising a phenol type compound (I) represented by the formula (I), ##STR1## wherein R.sub.1 represents a C.sub.1 -C.sub.3 alkyl group, and at least one sulfur type compound (II) selected from the group consisting of compounds represented by the formula (II-1), ##STR2## wherein R.sub.2 represents a C.sub.4 -C.sub.20 alkyl group, and compounds represented by the formula (II-2), ##STR3## wherein R.sub.3 represents a C.sub.3 -C.sub.18 alkyl group, and R.sub.4 and R.sub.5 independently represent a hydrogen atom or a C.sub.1 -C.sub.6 alkyl group, the weight ratio of phenol type compound (I) to sulfur type one (II) being 1 to 0.5-15.
摘要翻译：含有由式（I）表示的酚型化合物（I），其中R 1表示C 1 -C 3烷基的混合物作为有效成分的合成树脂稳定剂，和选自由式（II-1）表示的化合物，其中R 2表示C 4 -C 20烷基的化合物，II-1所示的至少一种硫型化合物（II）式（II-2），其中R 3表示C 3 -C 18烷基，R 4和R 5独立地表示氢原子或C 1 -C 6烷基的化合物（II-2），苯酚型化合物（I）的硫型（II）为1〜0.5〜15。

10. 发明授权

US4721744A Stabilized polyurethane compositions 失效
标题翻译：稳定的聚氨酯组合物
公开(公告)号：US4721744A
公开(公告)日：1988-01-26
申请号：US846050
申请日：1986-03-31
申请人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shionoya
发明人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shionoya
IPC分类号： C08G18/00 , C08K5/14 , C08K5/1575 , C08K5/18 , C08K5/3435 , C08K5/3447 , C08K5/3492 , C08L67/00 , C08L75/00 , C08L75/04 , C08K5/34 , C08K5/49
CPC分类号： C08K5/3435 , C08K5/1575 , C08K5/3492
摘要： Polyurethanes are stabilized against yellowing by incorporating a phenolic type compound represented by the general formula (I) ##STR1## wherein R.sub.1 represents a C.sub.1 -C.sub.3 alkyl group and at least one member selected from a benzotriazole type light stabilizer and a hindered amine type stabilizer.
摘要翻译：通过加入由通式（I）表示的酚类化合物，其中R1表示C1-C3烷基和选自苯并三唑型光稳定剂和受阻胺中的至少一种，聚氨酯稳定防黄变型稳定剂。

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