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1. 发明授权

US5506286A Method for stabilizing an organic material using a hindered piperidine compound 失效
标题翻译：使用受阻哌啶化合物稳定有机材料的方法
公开(公告)号：US5506286A
公开(公告)日：1996-04-09
申请号：US305365
申请日：1994-09-13
申请人： Kenji Kimura , Motohiko Samizo , Shinya Tanaka , Yukihiro Honda , Manji Sasaki , Shinichi Yachigo
发明人： Kenji Kimura , Motohiko Samizo , Shinya Tanaka , Yukihiro Honda , Manji Sasaki , Shinichi Yachigo
IPC分类号： C07D211/58 , C07B61/00 , C07D211/94 , C08K5/3432 , C08K5/3435 , C08L101/00 , C09K15/22
CPC分类号： C08K5/3435
摘要： A hindered piperidine compound represented by the formula of ##STR1## wherein R.sup.1 is a 2,2,6,6-tetramethyl-4-piperidyl group of which the N-position is substituted or not, a hydrogen atom, a C.sub.1 -C.sub.18 alkyl group which may contain a cyclic portion, or a C.sub.7 -C.sub.18 arylalkyl group, R.sup.2 is a hydrogen atom, a C.sub.1 -C.sub.10 alkyl group which may contain a cyclic portion, a C.sub.1 -C.sub.18 alkyloxy group which may contain a cyclic portion, or a hydroxyl group, and n is an integer of 2 to 8, effectively stabilizes organic materials having a property to deteriorate by the action of light. A method for producing the compound represented by the above formula is also disclosed.
摘要翻译：由下式表示的受阻哌啶化合物，其中R1是其N-取代的2,2,6,6-四甲基-4-哌啶基，氢原子，C 1 -C 18烷基可以含有环状部分的基团，或C 7〜C 18芳烷基，R 2为氢原子，可含有环状部分的C 1〜C 10烷基，可含有环状部分的C 1 -C 18烷氧基，或羟基，n为2〜8的整数，有效地使通过光的作用使具有劣化性的有机材料稳定化。还公开了由上式表示的化合物的制备方法。

2. 发明授权

US5214084A Stabilized polypropylene resin composition 失效
标题翻译：稳定的聚丙烯树脂组合物
公开(公告)号：US5214084A
公开(公告)日：1993-05-25
申请号：US933936
申请日：1992-08-24
申请人： Tamaki Ishii , Shinichi Yachigo
发明人： Tamaki Ishii , Shinichi Yachigo
IPC分类号： C08K3/00 , C08K5/13 , C08K5/134 , C08K5/20 , C08K5/3435 , C08K5/3492 , C08K5/372 , C08K5/526 , C08K5/527 , C08L23/10 , C08L23/16
CPC分类号： C08K5/526 , C08K3/0033 , C08K5/13 , C08K5/1345 , C08K5/20 , C08K5/3435 , C08K5/34926 , C08K5/372 , C08K5/527 , C08L23/10 , C08L23/16
摘要： A polypropylene resin containing an .alpha.-olefinic copolymer rubber and an inorganic filler is stabilized by incorporating therein the following 6 components:(A) a hindered phenolic compound having a molecular weight of not less than 500,(B) a high-molecular hindered piperidine compound such as poly[{6-(1,1,3,3-tetramethylbutyl)amino-1,3,5-triazine-2,4-diyl}{(2,2,6,6-tetramethyl-4-piperidyl)-imino}hexamethylene{(2,2,6,6-tetramethyl-4-piperidyl)imino}],(C) a low-molecular hindered piperidine compound such as 2-methyl-2-(2,2,6,6-tetramethyl-4-piperidyl)amino-N-(2,2,6,6-tetramethyl-4-piperidyl)propionamide,(D) a benzoate compound such as 2,4-di-t-butylphenyl 3,5-di-t-butyl-4-hydroxybenzoate,(E) a phosphorous compound such as bis(2,4-di-t-butylphenyl) pentaerythritol diphosphite, and(F) an amide compound such as ethylene-bisstearylamide. This composition may also contain a sulfur compound such as dialkyl thiodipropionate and pentaerythritol tetrakis(3-alkylthiopropionate). The composition disclosed is stable not only against heat and oxidation but also against light.
摘要翻译：含有α-烯烃共聚物橡胶和无机填料的聚丙烯树脂通过在其中加入以下6种成分而稳定化：（A）分子量不小于500的受阻酚类化合物，（B）高分子受阻哌啶化合物如聚[{6-（1,1,3,3-四甲基丁基）氨基-1,3,5-三嗪-2,4-二基} {（2,2,6,6-四甲基-4-哌啶基） - 亚氨基}六亚甲基{（2,2,6,6-四甲基-4-哌啶基）亚氨基}]，（C）低分子受阻哌啶化合物如2-甲基-2-（2,2,6， 6-二甲基-4-哌啶基）氨基-N-（2,2,6,6-四甲基-4-哌啶基）丙酰胺，（D）苯甲酸酯化合物如2,4-二叔丁基苯基3,5 - 二叔丁基-4-羟基苯甲酸酯，（E）磷化合物如双（2,4-二叔丁基苯基）季戊四醇二亚磷酸酯，和（F）酰胺化合物如乙烯 - 双硬脂酰胺。该组合物还可以含有硫化合物如硫代二丙酸二烷基酯和季戊四醇四（3-烷基硫代丙酸酯）。所公开的组合物不仅耐热和氧化而且对光也是稳定的。

3. 发明授权

US4985479A Stabilized polyolefin composition 失效
标题翻译：稳定的聚烯烃组合物
公开(公告)号：US4985479A
公开(公告)日：1991-01-15
申请号：US329764
申请日：1989-03-28
申请人： Hideo Nagasaki , Shinichi Yachigo , Takeshi Takata , Hiroki Yamamoto , Yukoh Takahashi
发明人： Hideo Nagasaki , Shinichi Yachigo , Takeshi Takata , Hiroki Yamamoto , Yukoh Takahashi
IPC分类号： C08K5/134 , C08K5/3435 , C08K5/3492 , C08K5/526 , C08K5/527 , C08K5/5393
CPC分类号： C08K5/527 , C08K5/1345 , C08K5/3435 , C08K5/34926 , C08K5/526 , C08K5/5393
摘要： A stabilized polyolefin composition having improved weathering resistance is provided, whereby the following four components are incorporated into a polyolefin:(A) a hindered piperidine compound having a molecular weight of more than 750, such as poly-{[6-morpholino-1,3,5-triazine-2,4-diyl][2,2,6,6-tetramethyl-4-piperidyl)imino]hexamethylene[2,2,6,6-tetramethyl-4-piperidyl)imino]},(B) a hindered piperidine compound having a molecular weight of less than 500, such as bis(2,2,6,6-tetramethyl-4-piperidyl) sebacate,(C) a benzoate compound such as 2,4-di-t-butylphenyl 3,5-di-t-butyl-4-hydroxybenzoate, and(D) a phosphorus-containing compound such as bis(2,4-di-t-butylphenyl) pentaerythritol diphosphite.
摘要翻译：提供了具有改善的耐候性的稳定的聚烯烃组合物，由此将以下四种组分引入聚烯烃中：（A）分子量大于750的受阻哌啶化合物，例如聚{{6-吗啉代-1，亚氨基]亚己基[2,2,6,6-四甲基-4-哌啶基]亚氨基]}，（B）分子量小于500的受阻哌啶化合物，例如双（2,2,6,6-四甲基-4-哌啶基）癸二酸酯，（C）苯甲酸酯化合物如2,4-二 - 3,5-二叔丁基-4-羟基苯甲酸叔丁基苯酯和（D）含磷化合物如双（2,4-二叔丁基苯基）季戊四醇二亚磷酸酯。

4. 发明授权

US4829112A Polyolefin resin composition 失效
标题翻译：聚烯烃树脂组合物
公开(公告)号：US4829112A
公开(公告)日：1989-05-09
申请号：US129937
申请日：1987-12-03
申请人： Tamaki Ishii , Shinichi Yachigo , Taisuke Okita , Manji Sasaki , Chinehito Ebina
发明人： Tamaki Ishii , Shinichi Yachigo , Taisuke Okita , Manji Sasaki , Chinehito Ebina
IPC分类号： C08L23/00 , C08K5/00 , C08K5/1575 , C08K5/49 , C08K5/52 , C08K5/524 , C08K5/53
CPC分类号： C08K5/1575 , C08K5/524
摘要： A thermally stable polyolefin resin improved in thermal processing by the incorporation therein of a phenolic compound represented by the general formula: ##STR1## wherein R.sub.1 represents a hydrogen atom or a C.sub.1 -C.sub.3 alkyl group, and a phosphite or phosphonite compound of 0.1 to 15 times by weight based on the phenolic compound.
摘要翻译：热稳定性聚烯烃树脂通过掺入由下列通式表示的酚类化合物而改善热处理：其中R 1表示氢原子或C 1 -C 3烷基，亚磷酸酯或亚膦酸酯化合物为0.1至15 基于酚类化合物的重量。

5. 发明授权

US4739080A Purification of hydroxyphenylpropionic acid ester 失效
标题翻译：羟基苯丙酸酯的纯化
公开(公告)号：US4739080A
公开(公告)日：1988-04-19
申请号：US868742
申请日：1986-05-30
申请人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
发明人： Manji Sasaki , Chinehito Ebina , Haruki Okamura , Shinichi Yachigo , Tamaki Ishii
IPC分类号： C07D493/10 , C08K5/1575 , C07D319/04
CPC分类号： C07D493/10
摘要： Method for the purification of 3,9-bis{2-[3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propionyloxy]-1,1-dimethylethyl} -2,4,8,10-tetraoxaspiro[5.5]undecane, to form crystals having a crystalline structure which, when subjected to Cu-K.sub..alpha. X-ray diffraction, show sharp X-ray diffraction peaks at angles of diffraction, to 2.theta.=2.8.degree., 2.theta.=8.7.degree. and 2.theta.=11.7.degree., by recrystallizing the ester at a temperature lower than 40.degree. C. using as a recrystallization solvent, A C.sub.5 -C.sub.10 alicyclic hydrocarbon, which may contain a limited amount of certain other solvents, or using a mixed solvent of a C.sub.5 -C.sub.10 aliphatic hydrocarbon and at least one other certain solvent in a certain weight ratio.
摘要翻译：纯化3,9-双{2- [3-（3-叔丁基-4-羟基-5-甲基苯基）丙酰氧基] -1,1-二甲基乙基} -2,4,8,10-四氧杂螺环 [5.5]十一烷，以形成具有晶体结构的晶体，当经受Cu-Kαα射线衍射时，衍射角呈现尖锐的X射线衍射峰，为2θ= 2.8°，2θ= 8.7° 和2θ= 11.7°，通过在低于40℃的温度下使酯重结晶，使用可能含有有限量的某些其它溶剂的A C5-C10脂环族烃，或使用混合溶剂一种C 5 -C 10脂族烃和至少一种其它特定溶剂。

6. 发明授权

US4603159A Phenolic compounds and stabilizers containing the same 失效
标题翻译：酚类化合物和含有它的稳定剂
公开(公告)号：US4603159A
公开(公告)日：1986-07-29
申请号：US706165
申请日：1985-02-27
申请人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shinoya
发明人： Tamaki Ishii , Shinichi Yachigo , Manji Sasaki , Haruki Okamura , Masahisa Shinoya
IPC分类号： C08K5/134 , C08K5/372 , C08K5/378 , C08K5/37
CPC分类号： C08K5/1345 , C08K5/372 , C08K5/378
摘要： Synthetic resins, such as polyolefins, are stabilized with phenolic compounds of the formula ##STR1## where n is 1 to 4 and A is ##STR2## where R.sub.1 is C.sub.1 -C.sub.3 alkyl.
摘要翻译：合成树脂，如聚烯烃，用式为“IMAGE”的酚类化合物进行稳定化，其中n为1至4，A为“IMA”，其中R 1为C 1 -C 3烷基。

7. 发明授权

US4507417A Stabilizers for synthetic resins 失效
标题翻译：合成树脂稳定剂
公开(公告)号：US4507417A
公开(公告)日：1985-03-26
申请号：US542518
申请日：1983-10-17
申请人： Tamaki Ishii , Shinichi Yachigo , Yukoh Takahashi
发明人： Tamaki Ishii , Shinichi Yachigo , Yukoh Takahashi
IPC分类号： C08L23/00 , C08K5/00 , C08K5/34 , C08K5/3477 , C08K5/36 , C08K5/372 , C08K5/378 , C08L7/00 , C08L21/00 , C08L51/00 , C08L51/02 , C08L77/00 , C08L101/00
CPC分类号： C08K5/378 , C08K5/3477 , C08K5/372
摘要： A novel stabilizing mixture composed of 1 1,3,5-tris 2-[3-(3-t-butyl-4-hydroxy-5-methyl-phenyl)-propionyloxyl] ethyl isocyanuric acid (I) and at least one sulfur-containing compound (II) selected from compounds represented by the general formulas (II-1) and (II-2): ##STR1## wherein R.sub.1 is an alkyl group having 4 to 20 carbon atoms, and ##STR2## wherein R.sub.2 is an alkyl group having 3 to 18 carbon atoms, and R.sub.3 and R.sub.4 each independently is a hydrogen atom or an alkyl group having 1 to 6 carbon atoms, is useful as a stabilizer for synthetic resins.
摘要翻译：由1,3,5-三2- [3-（3-叔丁基-4-羟基-5-甲基 - 苯基） - 丙酰氧基]乙基异氰脲酸（I）和至少一种硫（II-1）和（II-2）表示的化合物：其中R 1是具有4至20个碳原子的烷基和（II-2）其中R2是具有3至18个碳原子的烷基，R3和R4各自独立地是氢原子或具有1至6个碳原子的烷基，可用作合成树脂的稳定剂。

8. 发明授权

US5300568A Thermoplastic resin composition 失效
标题翻译：热塑性树脂组合物
公开(公告)号：US5300568A
公开(公告)日：1994-04-05
申请号：US667408
申请日：1991-04-08
申请人： Hiroomi Abe , Takeshi Fujii , Masashi Yamamoto , Shinichi Yachigo , Hideo Nagasaki , Naoki Inui
发明人： Hiroomi Abe , Takeshi Fujii , Masashi Yamamoto , Shinichi Yachigo , Hideo Nagasaki , Naoki Inui
IPC分类号： C08K5/32 , C08K5/34 , C08L21/00 , C08L23/00 , C08L23/04 , C08L25/00 , C08L51/06 , C08L71/12 , C08L53/00
CPC分类号： C08L23/04 , C08K5/32 , C08K5/34 , C08L71/12 , Y10S525/905
摘要： A thermoplastic resin composition which comprises 100 parts by weight of a composition comprising 95-5% by weight of at least one polyolefin-resin (A) selected from homopolymers of ethylene or .alpha.-olefin or copolymers thereof and these homopolymers or copolymers modified with a polyfunctional compound (E) and/or an unsaturated monomer (L) and 5-95% by weight of at least one polyphenylene-ether-resin (B) selected from polyphenylene ether, modified polyphenylene ether with the above (E) and/or (L) and a composition comprising the polyphenylene or modified polyphenylene ether and an aromatic vinyl polymer resin (M) and 0.001-10 parts by weight of a dinitrodiamine (D) of the following formula (I). ##STR1## (wherein X represents a divalent chain aliphatic group, a cyclic aliphatic group or an aromatic group which may contain a halogen or an oxygen atom, R.sup.1 represents a hydrogen atom, a chain aliphatic group, a cyclic aliphatic group or an aromatic group and when both of X and R.sup.1 are chain aliphatic groups, the nitrogen atoms may further bond each other to form a ring through X and R.sup.1 ; R.sup.2 and R.sup.3 are independently a hydrogen atom or an alkyl group of 1-12 carbon atoms and R.sup.2 and R.sup.3 may bond to form a ring).
摘要翻译： PCT No.PCT / JP90 / 00759 Sec。 371日期：1991年4月8日 102（e）日期1991年4月8日PCT Filed 1990年6月11日PCT公布。 WO91 / 19762 PCT出版物日本1991年12月26日。一种热塑性树脂组合物，其包含100重量份的组合物，其包含95-5重量％的至少一种选自乙烯或（α-）α-烯烃或共聚物的均聚物的聚烯烃树脂（A）和由多官能化合物（E）和/或不饱和单体（L）改性的这些均聚物或共聚物和5-95重量％的至少一种选自聚苯醚，改性聚苯醚的聚苯醚树脂（B）与上述（E）和/或（L）和包含聚亚苯基或改性聚苯醚和芳族乙烯基聚合物树脂（M）的组合物和0.001-10重量份下式（I）的二硝基二胺（D））。（*化学结构*）（I）（其中X表示可以含有卤素或氧原子的二价链脂肪族基团，环状脂肪族基团或芳香族基团，R 1表示氢原子，链状脂肪族基团，环状脂族基团或芳香族基团，当X和R 1均为链状脂族基团时，氮原子可以进一步通过X和R 1彼此键合形成环; R2和R3独立地为氢原子或1- 12个碳原子，R2和R3可以键合形成环）。

9. 发明授权

US5109055A Rubber composition having excellent dynamic properties 失效
标题翻译：橡胶组合物具有优异的动态性能
公开(公告)号：US5109055A
公开(公告)日：1992-04-28
申请号：US548560
申请日：1990-07-05
申请人： Hideo Nagasaki , Naoki Inui , Shinichi Yachigo
发明人： Hideo Nagasaki , Naoki Inui , Shinichi Yachigo
IPC分类号： C08K5/08 , C08K5/32 , C08K5/3415
CPC分类号： C08K5/32 , C08K5/08 , C08K5/3415
摘要： A rubber composition comprising a base rubber, carbon black and a dinitrodiamine compound represented by the formula [I], ##STR1## wherein X is a divalent aliphatic, alicyclic or aromatic group which may contain halogen or oxygen in the group, R.sup.1 is hydrogen or an aliphatic, alicyclic or aromatic group, provided that two nitrogen atoms linking through X may further link through R.sup.1 when both X and R.sup.1 are the aliphatic groups, and R.sup.2 and R.sup.3 independently of one another are each hydrogen or an alkyl of 1 to 12 carbon atoms, provided that R.sup.2 and R.sup.3 may conjointly form a ring,is improved in its scorching without deterioration in its dynamic properties by incorporating thereto the following components (A) or (B):(A) N-(cyclohexylthio)phthalimide and a bismaleimide compound, or(B) 2,3,5,6-tetrachloro-1,4-benzoquinone.

10. 发明授权

US5045581A Butadiene polymer composition containing phenolic compound and phosphorus-containing compound 失效
标题翻译：丁二烯聚合物组合物含有酚类化合物和含磷化合物
公开(公告)号：US5045581A
公开(公告)日：1991-09-03
申请号：US287287
申请日：1988-12-21
申请人： Takeshi Takata , Shinichi Yachigo , Manji Sasaki , Kikumitsu Inoue , Shinya Tanaka
发明人： Takeshi Takata , Shinichi Yachigo , Manji Sasaki , Kikumitsu Inoue , Shinya Tanaka
IPC分类号： C08K5/13 , C08K5/134 , C08K5/49 , C08K5/52 , C08K5/526 , C08L9/00 , C08L53/00 , C08L53/02
CPC分类号： C08K5/134 , C08K5/526
摘要： A butadiene polymer composition containing a phenolic compound represented by the formula: ##STR1## wherein R.sub.1 is an alkyl having 1 to 4 carbon atoms, R.sub.2 and R.sub.3 are each independently a group represented by --C(CH.sub.3).sub.2 --R' in which R' is an alkyl having 1 to 5 carbon atoms or phenyl, and R.sub.4 is hydrogen or methyl, and a phosphorus-containing compound represented by the formula: ##STR2## wherein R.sub.5 and R.sub.6 are each independently an alkyl having 1 to 9 carbon atoms.The composition is stable against the thermal deterioration and discoloration in the absence of oxygen as well as against the exposure to oxides of nitrogen gas.
摘要翻译：一种丁二烯聚合物组合物，其含有由下式表示的酚类化合物：其中R 1是具有1至4个碳原子的烷基，R 2和R 3各自独立地是由-C（CH 3）2 -R'表示的基团，其中R '是具有1至5个碳原子的烷基或苯基，R4是氢或甲基，以及由下式表示的含磷化合物：其中R 5和R 6各自独立地为具有1至9个碳原子的烷基。该组合物对于在不存在氧气的情况下的热劣化和变色以及暴露于氮气的氧化物是稳定的。

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